4-BROMO-2-METHYLTHIAZOLE

Product Name: 4-BROMO-2-METHYLTHIAZOLE
CAS No.: 298694-30-1
Chemical Name: 4-BROMO-2-METHYLTHIAZOLE
Synonyms: 4-Bromo-2-methyl-1,3-thiazole;4-BROMO-2-METHYLTHIAZOLE;Thiazole, 4-bromo-2-methyl-;4-Bromo-2-methylthiazole 98%;4-Bromo-2-(methyl-d3)-thiazole
CBNumber: CB3282173
Molecular Formula: C4H4BrNS
Formula Weight: 178.05
MOL File: 298694-30-1.mol

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4-BROMO-2-METHYLTHIAZOLE Property

Boiling point:: 199.2±13.0 °C(Predicted)
Density: 1.702±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Store in freezer, under -20°C
pka: 0.66±0.10(Predicted)
form: liquid
color: Colourless

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Safety

Hazard Codes: Xi
Risk Statements: 41
Safety Statements: 26-39
Hazard Note: Irritant
HS Code: 2934100090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B697783
Product name: 4-Bromo-2-methylthiazole
Packaging: 1g
Price: $345
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB157500
Product name: 4-Bromo-2-methylthiazole
Packaging: 1g
Price: $400
Updated: 2021/12/16

AK Scientific

Product number: X4179
Product name: 4-Bromo-2-methylthiazole
Packaging: 1g
Price: $181
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB157500
Product name: 4-Bromo-2-methylthiazole
Packaging: 500mg
Price: $265
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB157500
Product name: 4-Bromo-2-methylthiazole
Packaging: 50mg
Price: $55
Updated: 2021/12/16

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4-BROMO-2-METHYLTHIAZOLE Chemical Properties,Usage,Production

Synthesis

616-42-2

298694-30-1

General procedure for the synthesis of 2-methyl-4-bromothiazole from dimethyl sulfite: 2,4-dibromothiazole (2.4 g, 9.8 mmol) was dissolved in anhydrous THF (50 mL), and the resulting solution was stirred at -78 °C under argon protection. Slowly n-butyllithium (4.2 mL, 6 mmol, 2.5 M hexane solution) was added and stirring was continued for 1 hour. Subsequently, a solution of dimethyl sulfate (2.7 mL) in THF (5 mL) was added dropwise. The reaction mixture was stirred at -78 °C for 4 h before slowly warming to room temperature and continuing to stir overnight. Upon completion of the reaction, the reaction mixture was diluted with saturated aqueous sodium bicarbonate solution (50 mL). The aqueous layer was extracted with ether, the organic phases were combined, washed with brine, dried over magnesium sulfate and concentrated by rotary evaporation. Finally, purification by silica gel column chromatography afforded 2-methyl-4-bromothiazole as a yellow oil (0.956 g, 55% yield).

References

[1] Patent: WO2007/14922, 2007, A1. Location in patent: Page/Page column 121-122

4-BROMO-2-METHYLTHIAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-2-METHYLTHIAZOLE Suppliers

Canada 1 China 91 Germany 2 India 3 United Kingdom 4 United States 12 Global 113

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View Lastest Price from 4-BROMO-2-METHYLTHIAZOLE manufacturers

Career Henan Chemical Co

Product: 4-BROMO-2-METHYLTHIAZOLE 298694-30-1
Price: US $1.00/g
Min. Order: 1g
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-07

298694-30-1, 4-BROMO-2-METHYLTHIAZOLERelated Search:

4-Bromo-2-methylethylaminopyridine-d11 4-Bromo-2-methoxypyridine-d6 4-Bromo-2-methylpyridine-d6 4-Bromo-2-methoxythiazole-d4 ETHYL 2-BROMO-4-METHYLTHIAZOLE-5-CARBOX&,ETHYL 2-BROMO-4-METHYLTHIAZOLE-5-CARBOXYLATE Methyl 5-bromo-4-methylthiazole-2-carboxylate 5-Bromo-2-methylthiazole 2-BROMO-4-METHYLTHIAZOLE-5-CARBOXYLIC ACID,2-BROMO-4-METHYLTHIAZOLE-5-CARBOXYLIC A& 2-BROMO-4-METHYLTHIAZOLE 2-BROMO-4-METHYLTHIAZOLE ,97% 4-BROMO-2-FORMYLTHIAZOLE 2-AMINO-5-BROMO-4-METHYLTHIAZOLE HYDROCHLORIDE 5-Bromo-4-methyl-thiazol-2-amine 4-BROMO-2-METHYLTHIAZOLE (4-BROMO-THIAZOL-2-YL)-METHANOL 4-BROMO-1,3-THIAZOLE-2-CARBOXYLIC ACID ETHYL 4-BROMOTHIAZOLE-2-CARBOXYLATE 4-Bromo-2-(2-hydroxyprop-2-yl)-1,3-thiazole

4-BROMO-2-METHYLTHIAZOLE

4-Bromo-2-methyl-1,3-thiazole

4-Bromo-2-(methyl-d3)-thiazole

Thiazole, 4-bromo-2-methyl-

4-Bromo-2-methylthiazole 98%

298694-30-1