3-BROMOBENZENESULFONAMIDE
Uses Application- Product Name
- 3-BROMOBENZENESULFONAMIDE
- CAS No.
- 89599-01-9
- Chemical Name
- 3-BROMOBENZENESULFONAMIDE
- Synonyms
- TCMDC-123819;BUTTPARK 95\57-08;3-BROMOBENZENESULFON;m-bromobenzenesulfonamide;3-BROMOBENZENESULFONAMIDE;3-BROMOBENZENESULPHONAMIDE;Benzenesulfonamide, 3-bromo-;3-BROMOBENZENE-1-SULFONAMIDE;3-Bromobenzene-1-Sulphonamide;3-Bromobenzenesulfonamide,97%
- CBNumber
- CB3366169
- Molecular Formula
- C6H6BrNO2S
- Formula Weight
- 236.09
- MOL File
- 89599-01-9.mol
3-BROMOBENZENESULFONAMIDE Property
- Melting point:
- 151-156 °C(lit.)
- Boiling point:
- 375.8±44.0 °C(Predicted)
- Density
- 1.754±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- pka
- 9.81±0.60(Predicted)
- color
- White to Light yellow
- CAS DataBase Reference
- 89599-01-9(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 563609
- Product name
- 3-Bromobenzenesulfonamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $57.6
- Updated
- 2023/06/20
- Product number
- B5734
- Product name
- 3-Bromobenzenesulfonamide
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $42
- Updated
- 2025/07/31
- Product number
- B5734
- Product name
- 3-Bromobenzenesulfonamide
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $123
- Updated
- 2025/07/31
- Product number
- B682623
- Product name
- 3-Bromobenzenesulfonamide
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B682623
- Product name
- 3-Bromobenzenesulfonamide
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
3-BROMOBENZENESULFONAMIDE Chemical Properties,Usage,Production
Uses
3-Bromobenzenesulfonamide is an amine derivative that can be used as a pharmaceutical intermediate.
Application
3-Bromobenzenesulfonamide can be used as a pharmaceutical synthesis intermediate. It can be prepared by reacting 3-bromobenzenesulfonyl chloride with ammonia, or by preparing it in one step from the diazonium salt of m-bromobenzene tetrafluoride.
Chemical Properties
white powder
Synthesis
2905-24-0
89599-01-9
Under ice bath conditions, 3-bromobenzenesulfonyl chloride (4.073 g, 15.94 mmol) was dissolved in dichloromethane (67 mL) and 25% ammonia solution (3.7 mL, 57.15 mmol) was slowly added. The reaction mixture was stirred at ice bath temperature for 0.5 hr, then brought to room temperature and continued stirring for 6 hr. Upon completion of the reaction, the precipitated solid was collected by filtration, washed with water and dried under vacuum in the presence of phosphorus pentoxide to afford 3-bromobenzenesulfonamide (3.270 g, 87% yield) in white crystalline form. NMR hydrogen spectrum (DMSO-d6) δ: 7.97 (t, J = 1.9 Hz, 1H), 7.84-7.80 (m, 2H), 7.54 (t, J = 7.9 Hz, 1H), 7.50 (bs, 2H). Liquid chromatography-mass spectrometry (ESI) m/z: 235.98 [M-H]-.
References
[1] Patent: WO2016/129983, 2016, A1. Location in patent: Page/Page column 18; 19
[2] Justus Liebigs Annalen der Chemie, 1875, vol. 177, p. 82
[3] ACS Medicinal Chemistry Letters, 2011, vol. 2, # 8, p. 603 - 607
[4] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 9, p. 2222 - 2225
3-BROMOBENZENESULFONAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-BROMOBENZENESULFONAMIDE manufacturers
- Product
- 3-BROMOBENZENESULFONAMIDE 89599-01-9
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.9%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-07-12
- Product
- 3-BROMOBENZENESULFONAMIDE 89599-01-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-02