Uses Application
ChemicalBook > CAS DataBase List > 3-BROMOBENZENESULFONAMIDE

3-BROMOBENZENESULFONAMIDE

Uses Application
Product Name
3-BROMOBENZENESULFONAMIDE
CAS No.
89599-01-9
Chemical Name
3-BROMOBENZENESULFONAMIDE
Synonyms
TCMDC-123819;BUTTPARK 95\57-08;3-BROMOBENZENESULFON;m-bromobenzenesulfonamide;3-BROMOBENZENESULFONAMIDE;3-BROMOBENZENESULPHONAMIDE;Benzenesulfonamide, 3-bromo-;3-BROMOBENZENE-1-SULFONAMIDE;3-Bromobenzene-1-Sulphonamide;3-Bromobenzenesulfonamide,97%
CBNumber
CB3366169
Molecular Formula
C6H6BrNO2S
Formula Weight
236.09
MOL File
89599-01-9.mol
More
Less

3-BROMOBENZENESULFONAMIDE Property

Melting point:
151-156 °C(lit.)
Boiling point:
375.8±44.0 °C(Predicted)
Density 
1.754±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
pka
9.81±0.60(Predicted)
color 
White to Light yellow
CAS DataBase Reference
89599-01-9(CAS DataBase Reference)
More
Less

Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
37/39-26
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29350090
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
563609
Product name
3-Bromobenzenesulfonamide
Purity
97%
Packaging
1g
Price
$57.6
Updated
2023/06/20
TCI Chemical
Product number
B5734
Product name
3-Bromobenzenesulfonamide
Purity
>98.0%(GC)
Packaging
5g
Price
$42
Updated
2025/07/31
TCI Chemical
Product number
B5734
Product name
3-Bromobenzenesulfonamide
Purity
>98.0%(GC)
Packaging
25g
Price
$123
Updated
2025/07/31
TRC
Product number
B682623
Product name
3-Bromobenzenesulfonamide
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
B682623
Product name
3-Bromobenzenesulfonamide
Packaging
500mg
Price
$65
Updated
2021/12/16
More
Less

3-BROMOBENZENESULFONAMIDE Chemical Properties,Usage,Production

Uses

3-Bromobenzenesulfonamide is an amine derivative that can be used as a pharmaceutical intermediate.

Application

3-Bromobenzenesulfonamide can be used as a pharmaceutical synthesis intermediate. It can be prepared by reacting 3-bromobenzenesulfonyl chloride with ammonia, or by preparing it in one step from the diazonium salt of m-bromobenzene tetrafluoride.

Chemical Properties

white powder

Synthesis

2905-24-0

89599-01-9

Under ice bath conditions, 3-bromobenzenesulfonyl chloride (4.073 g, 15.94 mmol) was dissolved in dichloromethane (67 mL) and 25% ammonia solution (3.7 mL, 57.15 mmol) was slowly added. The reaction mixture was stirred at ice bath temperature for 0.5 hr, then brought to room temperature and continued stirring for 6 hr. Upon completion of the reaction, the precipitated solid was collected by filtration, washed with water and dried under vacuum in the presence of phosphorus pentoxide to afford 3-bromobenzenesulfonamide (3.270 g, 87% yield) in white crystalline form. NMR hydrogen spectrum (DMSO-d6) δ: 7.97 (t, J = 1.9 Hz, 1H), 7.84-7.80 (m, 2H), 7.54 (t, J = 7.9 Hz, 1H), 7.50 (bs, 2H). Liquid chromatography-mass spectrometry (ESI) m/z: 235.98 [M-H]-.

References

[1] Patent: WO2016/129983, 2016, A1. Location in patent: Page/Page column 18; 19
[2] Justus Liebigs Annalen der Chemie, 1875, vol. 177, p. 82
[3] ACS Medicinal Chemistry Letters, 2011, vol. 2, # 8, p. 603 - 607
[4] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 9, p. 2222 - 2225

3-BROMOBENZENESULFONAMIDE Preparation Products And Raw materials

Raw materials

Copper(II) chloride Sodium nitrite Diethyl ether Acetic acid 3-Bromoaniline sulfur dioxide Ammonia

Preparation Products

More
Less

3-BROMOBENZENESULFONAMIDE Suppliers

Americas 1 Belgium 4 China 106 Europe 1 France 1 Germany 4 India 6 Japan 1 Switzerland 2 The Netherlands 1 Ukraine 1 United Kingdom 13 United States 36 Global 177
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
Advantage
61
Wuhan Chemwish Technology Co., Ltd
Tel
86-027-67849912
Fax
86-027-87531808
Email
sales@chemwish.com
Country
China
ProdList
35896
Advantage
56
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
ProdList
18207
Advantage
66
Jia Xing Isenchem Co.,Ltd
Tel
0573-85285100 18627885956
Fax
0573-85285100
Email
isenchem@163.com
Country
China
ProdList
9310
Advantage
66
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
Advantage
59
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11035
Advantage
64
Nanjing Chemlin Chemical Co., Ltd
Tel
025-83697070
Fax
+86-25-83453306
Email
info@chemlin.com.cn
Country
China
ProdList
16075
Advantage
64
China DongFan Chemical Co.,LTD
Tel
86-0571-85151182
Fax
86-0571-85151182
Country
China
ProdList
5691
Advantage
66
Sinopharm Chemical Reagent Co,Ltd.
Tel
86-21-63210123
Fax
86-21-63290778 86-21-63218885
Email
sj_scrc@sinopharm.com
Country
China
ProdList
9815
Advantage
79
Shanghai Sunway Pharmaceutical Technology Co., Ltd
Tel
18270980682
Fax
021 51613951
Email
mlcheng@sunwaypharm.cn
Country
China
ProdList
8669
Advantage
57
Tianjin Jinyuda Chemical Co., Ltd.
Tel
022-58013646 13011382049
Fax
022-23854368
Email
sales@jinyudachem.com
Country
China
ProdList
1930
Advantage
55
Thermo Fisher Scientific
Tel
800-810-5118
Fax
+86-10-84193589
Email
cnchemical@thermofisher.com
Country
China
ProdList
17770
Advantage
75
Beijing innoChem Science & Technology Co.,Ltd.
Tel
400-810-7969 010-59572699
Fax
010-59572688
Email
ningzi.li@inno-chem.com.cn
Country
China
ProdList
6134
Advantage
55
Shanghai Topbiochem Technology Co., Ltd
Tel
+86-21-60341587
Fax
+86-21-61294319
Email
sales@topbiochem.com
Country
China
ProdList
6175
Advantage
58
9ding chemical ( Shanghai) Limited
Tel
4009209199
Fax
86-021-52271987
Email
sales@9dingchem.com
Country
China
ProdList
22514
Advantage
55
Shanghai Aladdin Bio-Chem Technology Co.,LTD
Tel
400-6206333 13167063860
Fax
021-50323701
Email
anhua.mao@aladdin-e.com
Country
China
ProdList
25003
Advantage
65
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
Country
China
ProdList
9899
Advantage
55
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Chengdu HuaXia Chemical Reagent Co. Ltd
Tel
400-1166-196 13458535857
Fax
QQ：800101999
Email
cdhxsj@163.com
Country
China
ProdList
13350
Advantage
58
ShangHai KenEn Chemical Technology Co., Ltd.
Tel
13120367189
Fax
021-50315529
Email
mychess007@163.com
Country
China
ProdList
1994
Advantage
55
Credit-Chem Co., Ltd.
Tel
400-821-5857 021-64326257
Fax
021-64393586 QQ;2798200800
Email
credit-chem@foxmail.com
Country
China
ProdList
5219
Advantage
58
Shanghai Yongye Biotechnology Co., Ltd.
Tel
86-021-61559134 15921386130
Fax
021-55068248
Email
3423497944@qq.com
Country
China
ProdList
8144
Advantage
55
Shanghai Song Yuan Chemical Technology Co., Ltd.
Tel
010-1234567 18521000990
Fax
86-021-33275113
Email
sonyuanchemical@163.com
Country
China
ProdList
6479
Advantage
50
Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66028182 18626450290
Email
yftan@aikonchem.com
Country
China
ProdList
16679
Advantage
50
Sigma-Aldrich
Tel
021-61415566 800-8193336
Email
orderCN@merckgroup.com
Country
China
ProdList
51395
Advantage
80
Tianjin Jiahan Chemical Co., Ltd.
Tel
18920613223 86-22-58055669
Fax
022-23863911
Email
sales@jiahanchem.com
Country
China
ProdList
122
Advantage
55
Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd
Tel
18210788515
Fax
18210788515
Email
zhuzixin999@163.c0m
Country
China
ProdList
2999
Advantage
55
Wuhan Chemwish Technology Co.， Ltd
Tel
027-67849912
Fax
027-87531808
Email
sales@chemwish.com
Country
China
ProdList
9148
Advantage
60
Shanghai Brain Biotechnology Co., Ltd.
Tel
13564638271
Fax
021-68948280
Email
shhjiang1977@163.com
Country
China
ProdList
2987
Advantage
55
Nanjing Vital Chemical Co., Ltd.
Tel
025-87193546 18652950785
Fax
025-87193546
Email
chemweiao@163.com
Country
China
ProdList
9021
Advantage
60
ShangHai Siyan Biological Technology Co., Ltd.
Tel
021-50908862，442785678，326799392 18721037013
Fax
021-50908862
Email
siyansales@126.com
Country
China
ProdList
9627
Advantage
58
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
Shandong Xiya Chemical Co., Ltd.
Tel
4009903999 13395398332
Fax
0539-6365991
Email
sales@xiyashiji.com
Country
China
ProdList
20794
Advantage
60
Suzhou JingTong Pharmaceutical Co., Ltd.
Tel
13675155016
Fax
18912765016
Email
tongtf110@sina.com
Country
China
ProdList
963
Advantage
55
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Nanjing Klender Bio-Technology Co., Ltd.
Tel
025-52343882 18112933882
Fax
025-52343882
Email
sales@kldbio.com
Country
China
ProdList
2019
Advantage
55
Shanghai Kangman Biological Technology Co., Ltd.
Tel
18800375331
Fax
021-50908862
Email
kangmansales@163.com
Country
China
ProdList
7570
Advantage
55
Shanghai CR Corporation Limited
Tel
13062833949; 4006653949 4006653949
Fax
QQ: 2136646215
Email
fred.wen@crcorporation.cn
Country
China
ProdList
9756
Advantage
58
Guangzhou Jhd Chemical Reagent Co., Ltd.
Tel
020-84383047
Fax
020-84380294
Email
sales@jhd.com.cn
Country
China
ProdList
9186
Advantage
65
Shanghai Zhen Li Biological Technology Co., Ltd
Tel
021-16621358918; 18516310516
Fax
13045646768
Email
zhenlipharma888@163.com
Country
China
ProdList
19035
Advantage
58
Capot Chemical Co.,Ltd.
Tel
+86-（0）57185586718; +8613336195806
Fax
+86-571-85864795
Email
sales@capot.com
Country
China
ProdList
29735
Advantage
60
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 400821072
Fax
021-58955996
Email
malulu@leyan.com
Country
China
ProdList
25000
Advantage
58
3A Chemicals
Tel
400-668-9898
Fax
010-51582189
Email
service@3achem.com
Country
China
ProdList
20557
Advantage
58
JIANGYIN RUISHIPHARM CO.,LIMITED
Tel
0510-0510-66227179 18921203887
Fax
+86-0510-66227179 QQ:2200317867
Email
sales@ruishipharm.com
Country
China
ProdList
749
Advantage
58
Shanghai Jizhi Biochemical Technology Co. Ltd.
Tel
4009004166/18616739031 18616739031
Email
3007523370@qq.com
Country
China
ProdList
52687
Advantage
58
Cool Pharm, Ltd
Tel
021-58581007 18019463053
Fax
021-50966098
Email
sales@coolpharm.com
Country
China
ProdList
12878
Advantage
58
TCI Chemicals
Tel
021-67121386, 800-988-0390
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
5391
Advantage
58
Jinan Carbotang Biotech Co.,Ltd.
Tel
+8615866703830
Email
figo.gao@foxmail.com
Country
China
ProdList
8497
Advantage
58
More
Less

View Lastest Price from 3-BROMOBENZENESULFONAMIDE manufacturers

Dideu Industries Group Limited
Product
3-BROMOBENZENESULFONAMIDE 89599-01-9
Price
US $1.10/g
Min. Order
1g
Purity
99.9%
Supply Ability
100 Tons Min
Release date
2021-07-12
Career Henan Chemical Co
Product
3-BROMOBENZENESULFONAMIDE 89599-01-9
Price
US $1.00/KG
Min. Order
1KG
Purity
95-99%
Supply Ability
1ton
Release date
2020-01-02

89599-01-9, 3-BROMOBENZENESULFONAMIDERelated Search:

5-BROMO-N,N-DIETHYL-2-METHOXYBENZENESULFONAMIDE 4-(5-BROMO-2-METHOXYBENZENESULPHONYL)MORPHOLINE N-BENZYL 5-BROMO-2-METHOXYBENZENESULFONAMIDE 3-BROMOBENZENESULFONAMIDE 1-(5-BROMO-2-METHOXYBENZENESULPHONYL)PIPERIDINE 3,5-DIBROMOSULFANILAMIDE N-(4-Fluorobenzyl) 2-bromobenzenesulfonamide N-t-Butyl 2-bromobenzenesulfonamide N-(4-Methoxybenzyl) 4-bromobenzenesulfonamide N-Methyl 2-bromobenzenesulfonamide 2-BROMOBENZENESULFONAMIDE N,N-Dimethyl 2-bromobenzenesulfonamide 4-BROMOBENZENESULFONAMIDE, 98 % 3-Boronophenyl 3-bromobenzenesulfonamide N-Phenethyl 2-bromobenzenesulfonamide N-Benzyl-2-bromobenzenesulfonamide Benzenesulfonamide 2-AMINO-3,5-DIBROMOBENZENESULFONAMIDE

  • 3-BROMOBENZENESULPHONAMIDE
  • 3-BROMOBENZENESULFONAMIDE
  • 3-BROMO-BENZENESULFONIC ACID AMIDE
  • 3-BROMOBENZENE-1-SULFONAMIDE
  • 3-Bromobenzenesulfonamide,97%
  • BUTTPARK 95\57-08
  • m-bromobenzenesulfonamide
  • 3-Bromobenzene-1-Sulphonamide
  • 3-BROMOBENZENESULFON
  • 3-BroMobenzenesulfonaMide, 97% 1GR
  • Benzenesulfonamide, 3-bromo-
  • 3-BROMOBENZENESULFONAMIDE USP/EP/BP
  • TCMDC-123819
  • 89599-01-9
  • C6H4BrSO2NH2
  • C6H6BrN2O2S
  • Building Blocks
  • ARYL HALIDE
  • Organic Building Blocks
  • Sulfonamides/Sulfinamides
  • Sulfur Compounds
  • Aryl
  • Organohalides
  • Organic Building Blocks
  • Sulfonamides/Sulfinamides
  • Sulfur Compounds
  • blocks
  • Bromides
  • Sulfonamides