2-CHLORO-6-HYDRAZINOPYRIDINE
- Product Name
- 2-CHLORO-6-HYDRAZINOPYRIDINE
- CAS No.
- 5193-03-3
- Chemical Name
- 2-CHLORO-6-HYDRAZINOPYRIDINE
- Synonyms
- 2-CHLOROPYRIDINEHYDRAZINE;2-Chloro-6hydrazine pyridine;2-CHLORO-6-HYDRAZINOPYRIDINE;2-Chloro-6-hydrazinylpyridine;6-CHLOROPYRIDIN-2-YLHYDRAZINE;6-Chloropyridine-2-ylhydrazine;Pyridine, 2-chloro-6-hydrazinyl-;2-Chloro-6-hydrazinopyridine >(6-Chloro-2-pyridyl)hydrazine, 95%;1-(6-Chloropyridin-2-yl)hydrazine, 96%
- CBNumber
- CB3370564
- Molecular Formula
- C5H6ClN3
- Formula Weight
- 143.57
- MOL File
- 5193-03-3.mol
2-CHLORO-6-HYDRAZINOPYRIDINE Property
- Melting point:
- 118°C
- Boiling point:
- 118°C
- Density
- 1.43±0.1 g/cm3(Predicted)
- Flash point:
- 117-120°C
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- form
- powder to crystal
- pka
- 9.08±0.70(Predicted)
- color
- Light yellow to Brown
- InChI
- InChI=1S/C5H6ClN3/c6-4-2-1-3-5(8-4)9-7/h1-3H,7H2,(H,8,9)
- InChIKey
- HFTSPKIAXHZROA-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NC(NN)=CC=C1
- CAS DataBase Reference
- 5193-03-3(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,T
- Risk Statements
- 20/21/22-36/37/38-41-25
- Safety Statements
- 26-36/37/39-39-45-36
- HazardClass
- IRRITANT
- PackingGroup
- III
- HS Code
- 29333990
N-Bromosuccinimide Price
- Product number
- SYX00272
- Product name
- 2-Chloro-6-hydrazinopyridine
- Packaging
- 1G
- Price
- $42.8
- Updated
- 2025/07/31
- Product number
- C2463
- Product name
- 2-Chloro-6-hydrazinopyridine
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $37
- Updated
- 2025/07/31
- Product number
- C349440
- Product name
- 2-Chloro-6-hydrazinylpyridine
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- C349440
- Product name
- 2-Chloro-6-hydrazinylpyridine
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 3H39-5-Y2
- Product name
- 2-Chloro-6-hydrazinopyridine
- Packaging
- 25g
- Price
- $50
- Updated
- 2021/12/16
2-CHLORO-6-HYDRAZINOPYRIDINE Chemical Properties,Usage,Production
Uses
2-Chloro-6-hydrazinopyridine is used as a useful research chemical.
Synthesis
2402-78-0
5193-03-3
General procedure for the synthesis of 2-chloro-6-hydrazinopyridine from 2,6-dichloropyridine: 2,6-dichloropyridine (50.0 g, 0.34 mol) was dissolved in a solvent mixture of 80% hydrazine monohydrate solution (120 mL, 1.92 mol) and ethanol (200 mL), and heated and refluxed for 4 hours at 100 °C. The progress of the reaction was monitored by thin layer chromatography (TLC) to confirm complete consumption of 2,6-dichloropyridine. Upon completion of the reaction, the reaction solution was cooled to room temperature and subsequently concentrated to dryness in a rotary evaporator. The resulting crude product was purified by recrystallization from petroleum ether to afford 2-chloro-6-hydrazinopyridine (31.0 g, 64%) as a white solid. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 7.42 (dd, J = 7.2 Hz, 0.4 Hz, 1H), 6.65 (t, J = 7.2 Hz, 2H), 6.14 (s, 1H), 3.63 (s, 2H).
References
[1] Organic and Biomolecular Chemistry, 2004, vol. 2, # 2, p. 246 - 256
[2] Patent: US2003/187014, 2003, A1
[3] Patent: WO2014/201127, 2014, A2. Location in patent: Paragraph 00582
[4] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2006, vol. 65, # 1, p. 206 - 214
[5] Patent: US4997835, 1991, A
2-CHLORO-6-HYDRAZINOPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
2-CHLORO-6-HYDRAZINOPYRIDINE Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
- ProdList
- 23653
- Advantage
- 75
View Lastest Price from 2-CHLORO-6-HYDRAZINOPYRIDINE manufacturers
- Product
- 2-CHLORO-6-HYDRAZINOPYRIDINE 5193-03-3
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-26
- Product
- 2-CHLORO-6-HYDRAZINOPYRIDINE 5193-03-3
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200KG
- Release date
- 2020-01-12