ChemicalBook > CAS DataBase List > 2'-AMINOACETANILIDE

2'-AMINOACETANILIDE

Product Name: 2'-AMINOACETANILIDE
CAS No.: 34801-09-7
Chemical Name: 2'-AMINOACETANILIDE
Synonyms: 2-AMinoactanilide;O-AMINOACETANILIDE;2-AMINOACETANILIDE;2'-Acetamidoaniline;2'-Aminoacetanilide;Trametinib Impurity 27;2'-Aminoacetanilide 98%;2'-Aminoacetanilide >2'-Aminoacetanilide ,98%;N-(2-aminophenyl)ethanamide
CBNumber: CB3389151
Molecular Formula: C8H10N2O
Formula Weight: 150.18
MOL File: 34801-09-7.mol

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2'-AMINOACETANILIDE Property

Melting point:: 133-137 °C(lit.)
Boiling point:: 271.72°C (rough estimate)
Density: 1.1392 (rough estimate)
refractive index: 1.6180 (estimate)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: powder to crystalline
pka: 14.73±0.70(Predicted)
color: Light orange to Light red
Water Solubility: 107.5g/L(22 ºC)
CAS DataBase Reference: 34801-09-7(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 549606
Product name: 2′-Aminoacetanilide
Purity: 98%
Packaging: 5g
Price: $68.1
Updated: 2022/05/15

Sigma-Aldrich

Product number: 549606
Product name: 2′-Aminoacetanilide
Purity: 98%
Packaging: 25g
Price: $223
Updated: 2022/05/15

TCI Chemical

Product number: A2426
Product name: 2'-Aminoacetanilide
Purity: >98.0%(T)
Packaging: 5g
Price: $70
Updated: 2025/07/31

TCI Chemical

Product number: A2426
Product name: 2'-Aminoacetanilide
Purity: >98.0%(T)
Packaging: 25g
Price: $249
Updated: 2024/03/01

TRC

Product number: A580013
Product name: 2''-Aminoacetanilide
Packaging: 10mg
Price: $45
Updated: 2021/12/16

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2'-AMINOACETANILIDE Chemical Properties,Usage,Production

Chemical Properties

White Powder

Uses

2′-Aminoacetanilide may be used in the preparation of:

2-Methylbenzimidazole.
N-(2-(1,3-Dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)phenyl)-5-methylfuran-2-carboxamide, a potent cystic fibrosis transmembrane conductance regulator (CFTR) inhibitor.
Azobenzothiazole dyes, N-[2-(6-nitrobenzothiazol-2-ylazo)phenyl]acetamide and N-[2-(benzothiazol-2-ylazo)phenyl]acetamide.

General Description

2′-Aminoacetanilide (2-aminoacetanilide, o-aminoacetanilide) can be prepared by the catalytic hydrogenation of 2-nitroacetanilide using 10%Pd/C (palladium/carbon).

Synthesis

552-32-9

34801-09-7

The general procedure for the synthesis of 2'-aminoacetanilide from 2-nitroacetanilide was as follows: first, 2-nitroacetanilide (1.0 g, 5.6 mmol) was dissolved in ethanol (EtOH) and the solution was purged with nitrogen to remove oxygen. Subsequently, palladium hydroxide (Pd(OH)2, 20% by weight, carbon carrier, 200 mg) was added to the solution as a catalyst. The reaction mixture was shaken under hydrogen (H2, 20 psi) atmosphere for 2 hours. Upon completion of the reaction, it was filtered through a 0.22 μm cellulose acetate membrane (Corning) to remove the catalyst. The filtrate was concentrated under vacuum to afford the white crystalline solid product 2'-aminoacetanilide (800 mg, 96% yield). The structure of the product was confirmed by 1H NMR (300 MHz, d6-DMSO) and LRMS (ES pos.): 1H NMR δ: 9.12 (s, 1H), 7.14 (dd, J = 7.8,1.3 Hz, 1H), 6.88 (dt, J = 7.6,1.5 Hz, 1H), 6.70 (dd, J = 8.0,1.3 Hz, 1H), 6.52 (dt, J = 7.5,1.4 Hz, 1H), 4.85 (br s, 2H), 2.03 (s, 3H); LRMS (ES pos.) m/z = 151 (M + 1).

References

[1] Journal of Organic Chemistry, 2008, vol. 73, # 23, p. 9235 - 9244
[2] Patent: US6667300, 2003, B2. Location in patent: Page column 98
[3] Chemistry - A European Journal, 2015, vol. 21, # 26, p. 9493 - 9504
[4] Russian Journal of Organic Chemistry, 1997, vol. 33, # 11, p. 1676 - 1677
[5] Russian Journal of Organic Chemistry, 1997, vol. 33, # 11, p. 1676 - 1677

2'-AMINOACETANILIDE Preparation Products And Raw materials

Raw materials

Sodium dodecyl sulfate Acetic anhydride Sodium sulfate Ethyl acetate o-Phenylenediamine

Preparation Products

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View Lastest Price from 2'-AMINOACETANILIDE manufacturers

Career Henan Chemical Co

Product: 2'-AMINOACETANILIDE 34801-09-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

34801-09-7, 2'-AMINOACETANILIDERelated Search:

2'-NITROBENZANILIDE 2'-NITROACETANILIDE 4-Acetamido-3-nitrobenzoic acid ALPHA-CHLORO-2-NITROACETANILIDE N1-(4,5-DICHLORO-2-NITROPHENYL)ACETAMIDE 4'-BROMO-2'-NITROACETANILIDE 2,4-DINITROACETANILIDE 4-METHOXY-2-NITROACETANILIDE 3-(N,N-DIACETHOXYETHYL)AMINOACETANILIDE,3'-Bis(2-acetoxyethyl)aminoacetanilide 2-[(3-acetamidophenyl)(2-cyanoethyl)amino]ethyl acetate P-AMINOACETANILIDE-3-SULFONIC ACID,4-aminoacetanilide-3-sulfonic acid 2-METHOXY-4-AMINOACETANILIDE 3-Aminoacetanilide HCl,M-AMINOACETANILIDE,3-AMINOACETANILIDE,3'-AMINOACETANILIDE 4-AMINOACETANILIDE HYDROCHLORIDE 3-(N-Cyanoethyl)aminoacetanilide N,N-DIALLYL-3-AMINOACETANILIDE 3'-AMINOACETANILIDE HYDROCHLORIDE 4'-Aminoacetanilide

N-(2-Aminophenyl)acetamide, 2-(Acetamido)aniline, N-Acetylphenylene-1,2-diamine

N-Acetyl-1,2-phenylenediamine 2'-Acetamidoaniline

2-AMinoactanilide

2'-Aminoacetanilide 98%

Acetanilide, 2-amino- (8CI)

N-(2-aminophenyl)ethanamide

Acetamide, N-(2-aminophenyl)- (9CI)

N-(2-azanylphenyl)ethanamide

2'-Aminoacetanilide ,98%

2-AMINOACETANILIDE

O-AMINOACETANILIDE

Acetamide, N-(2-aminophenyl)-

2'-Aminoacetanilide &gt

2'-Acetamidoaniline

N-Acetyl-1,2-phenylenediamine

2'-AMINOACETANILIDE ISO 9001：2015 REACH

2'-Aminoacetanilide

Trametinib Impurity 27

2′-Aminoacetanilide, CAS 34801-09-7

34801-09-7

CH3CONHC6H4NH2

Building Blocks

Organic Building Blocks

Nitrogen Compounds

Protected Amines

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Nitrogen Compounds

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AMINEPRIMARY

Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts