N1-(3-Aminophenyl)acetamide

Product Name: N1-(3-Aminophenyl)acetamide
CAS No.: 102-28-3
Chemical Name: N1-(3-Aminophenyl)acetamide
Synonyms: META AMINO ACETANILIDE;N-(3-AMINOPHENYL)ACETAMIDE;3-AMINOACETANILIDE;FR-2203;AKOS BB-8162;WLN: ZR CMV1;3-AcetamidoaniL;ASISCHEM B52481;3-aminoacetanilid;m-acetaminoaniline
CBNumber: CB3404737
Molecular Formula: C8H10N2O
Formula Weight: 150.18
MOL File: 102-28-3.mol

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N1-(3-Aminophenyl)acetamide Property

Melting point:: 86-88 °C(lit.)
Boiling point:: 271.72°C (rough estimate)
Density: 1.1392 (rough estimate)
refractive index: 1.6180 (estimate)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: powder to crystal
pka: 14.82±0.70(Predicted)
color: White to Gray to Brown
Water Solubility: 1-5 g/100 mL at 24 ºC
InChI: InChI=1S/C8H10N2O/c1-6(11)10-8-4-2-3-7(9)5-8/h2-5H,9H2,1H3,(H,10,11)
InChIKey: PEMGGJDINLGTON-UHFFFAOYSA-N
SMILES: C(NC1=CC=CC(N)=C1)(=O)C
CAS DataBase Reference: 102-28-3(CAS DataBase Reference)
EPA Substance Registry System: 3'-Aminoacetanilide (102-28-3)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36-37/39
WGK Germany: 3
RTECS: AD8050000
TSCA: Yes
HazardClass: IRRITANT
HS Code: 29214200
Toxicity: mouse,LD50,intravenous,320mg/kg (320mg/kg),U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#02899,

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 485055
Product name: 3′-Aminoacetanilide
Purity: 97%
Packaging: 250g
Price: $163
Updated: 2023/06/20

TCI Chemical

Product number: A1533
Product name: 3'-Aminoacetanilide
Purity: >98.0%(HPLC)(T)
Packaging: 25g
Price: $27
Updated: 2025/07/31

TRC

Product number: A638140
Product name: N-(3-Aminophenyl)acetamide
Packaging: 25g
Price: $75
Updated: 2021/12/16

TRC

Product number: A638140
Product name: N-(3-Aminophenyl)acetamide
Packaging: 2.5g
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA137386
Product name: 3'-Aminoacetanilide
Packaging: 100g
Price: $50
Updated: 2021/12/16

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N1-(3-Aminophenyl)acetamide Chemical Properties,Usage,Production

Chemical Properties

light brown crystalline powder

Uses

3'-Aminoacetanilide is mainly used as reaction intermediates dyes and disperse dyes.

General Description

Gray solid.

Air & Water Reactions

Soluble in water.

Reactivity Profile

Amines are chemical bases. They neutralize acids to form salts plus water. These acid-base reactions are exothermic. The amount of heat that is evolved per mole of amine in a neutralization is largely independent of the strength of the amine as a base. Amines may be incompatible with isocyanates, halogenated organics, peroxides, phenols (acidic), epoxides, anhydrides, and acid halides. Flammable gaseous hydrogen is generated by amines in combination with strong reducing agents, such as hydrides.

Health Hazard

ACUTE/CHRONIC HAZARDS: When heated to decomposition N1-(3-Aminophenyl)acetamide emits toxic fumes.

Fire Hazard

Flash point data concerning N1-(3-Aminophenyl)acetamide are not available, however, N1-(3-Aminophenyl)acetamide is probably combustible.

Synthesis

122-28-1

102-28-3

m-Nitroacetanilide (1 g, 5.66 mmol) was dissolved in 100 mL of methanol and a catalytic amount of 10% palladium/activated charcoal (~0.015 g) was added. The reaction mixture was cooled via an ice bath and sodium borohydride (1 g, 26.43 mmol) was added in batches. Subsequently, the mixture was stirred vigorously for 1 hour. The reaction process was monitored by thin layer chromatography (TLC) using toluene-acetone (5:2, v/v) as unfolding agent. Upon completion of the reaction, the product was purified by silica gel column chromatography with toluene-acetone (5:2, v/v) as eluent. A white solid product was obtained in 75% yield with a melting point of 86-88 °C. Elemental analysis (C8H10N2O, Mr=150.18) Calculated values: C 63.98%, H 6.71%, N 18.65%; measured values: C 63.76%, H 6.50%, N 18.53%.1H NMR (400 MHz, DMSO-d6) δ: 9.58 (s, 1H, NH), 6.92 (t, 1H, H-2, J = 2.00 Hz), 6.88 (t, 1H, H-4, J = 8.00 Hz), 6.64 (dd, 1H, H-6, J1 = 0.80 Hz, J2 = 8.00 Hz), 6.23 (dd, 1H, H-5, J1 = 1.60 Hz, J2 = 8.00 Hz), 5.00 (bs, 2H, NH2), 1.99 (s, 3H , CH3-CO).13C NMR (100 MHz, DMSO-d6) δ: 167.85 (C=O), 148.85 (C1), 139.85 (C3), 128.75 (C4), 109.04 (C5), 106.93 (C6), 104.67 (C2), 23.98 (CH3-CO).

References

[1] Green Chemistry, 2018, vol. 20, # 1, p. 130 - 135
[2] Supramolecular Chemistry, 2010, vol. 22, # 10, p. 586 - 597
[3] Bioorganic Chemistry, 2014, vol. 57, p. 13 - 29
[4] Chemical & Pharmaceutical Bulletin, 1989, vol. 37, # 3, p. 615 - 617
[5] Journal of Chemical Research, 2006, # 4, p. 223 - 224

N1-(3-Aminophenyl)acetamide Preparation Products And Raw materials

Raw materials

CALCIUM SULFIDE m-Phenylenediamine Acetic acid 3-Nitroaniline

Preparation Products

Acid Blue BGL Reactive Golden Yellow KM-G trisodium 7-[[2-[(aminocarbonyl)amino]-4-[(4-amino-6-chloro-1,3,5-triazin-2-yl)amino]phenyl]azo]naphthalene-1,3,5-trisulphonate Reactive Yellow 3 Reactive Yellow KE-RN

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N1-(3-Aminophenyl)acetamide Suppliers

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View Lastest Price from N1-(3-Aminophenyl)acetamide manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: N1-(3-Aminophenyl)acetamide 102-28-3
Price: US $0.00-0.00/KG
Min. Order: 50KG
Purity: 99%
Supply Ability: 500000kg
Release date: 2024-10-25

Hebei Yanxi Chemical Co., Ltd.

Product: N1-(3-Aminophenyl)acetamide 102-28-3
Price: US $0.00/kg
Min. Order: 1kg
Purity: 0.99
Supply Ability: 20tons
Release date: 2023-11-08

Hebei Chuanghai Biotechnology Co,.LTD

Product: 3-Acetamidoaniline 102-28-3
Price: US $5.00-2.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10000kg
Release date: 2024-08-19

102-28-3, N1-(3-Aminophenyl)acetamideRelated Search:

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