3'-BROMOACETANILIDE
Application- Product Name
- 3'-BROMOACETANILIDE
- CAS No.
- 621-38-5
- Chemical Name
- 3'-BROMOACETANILIDE
- Synonyms
- m-bromoacetanilide;3’-bromo-acetanilid;CHEMBRDG-BB 5475603;3'-BROMOACETANILIDE;3’-Bromoacetanilide;3'-Bromoacetoanilide;Acetanilide, 3'-bromo-;n-(3-bromophenyl)-acetamid;N-(3-bromophenyl)ethanamide;Acetamide, N-(3-bromophenyl)-
- CBNumber
- CB3457571
- Molecular Formula
- C8H8BrNO
- Formula Weight
- 214.06
- MOL File
- 621-38-5.mol
3'-BROMOACETANILIDE Property
- Melting point:
- 87-89 °C
- Boiling point:
- 349.2±25.0 °C(Predicted)
- Density
- 1.5097 (rough estimate)
- refractive index
- 1.6120 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 14.45±0.70(Predicted)
- Appearance
- Yellow to brown Solid
Safety
- HazardClass
- IRRITANT
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B680218
- Product name
- N-(3-Bromophenyl)acetamide
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- FB121739
- Product name
- N-(3-Bromophenyl)acetamide
- Packaging
- 100mg
- Price
- $58
- Updated
- 2021/12/16
- Product number
- 062493
- Product name
- N-(3-Bromophenyl)acetamide
- Packaging
- 1g
- Price
- $79
- Updated
- 2021/12/16
- Product number
- FB121739
- Product name
- N-(3-Bromophenyl)acetamide
- Packaging
- 250mg
- Price
- $115
- Updated
- 2021/12/16
- Product number
- 062493
- Product name
- N-(3-Bromophenyl)acetamide
- Packaging
- 5g
- Price
- $195
- Updated
- 2021/12/16
3'-BROMOACETANILIDE Chemical Properties,Usage,Production
Application
3-Bromoacetanilide can be used as a pharmaceutical synthesis intermediate and an organic synthesis intermediate, mainly in laboratory research and development processes and chemical and pharmaceutical synthesis processes.
Synthesis
Preparation of 3-bromoacetanilide: a 50 mL reaction vial was taken and 3-bromoacetophenone oxime (0.21 g, 1 mmol) dissolved in 2 mL of acetonitrile was transferred into the reaction vial and under stirring conditions, bismuth trifluoromethanesulfonate (0.10 g, 0.15 mmol) dissolved in 1 mL of acetonitrile was added and finally 2-3 mL of acetonitrile was added, and the reaction was carried out with stirring under an oil bath at 80 ??C. 3-bromoacetophenone oxime and bismuth trifluoromethanesulfonate were mixed and stirred, the solution immediately showed a slightly white suspension, and the reaction was monitored by TLC (DCM: 100%) until the reaction was complete, which was carried out for about 4 hours. The heating was stopped and the solvent was spun dry using a rotary evaporator, after which water and DCM were added to extract, the organic phases were combined and dried over anhydrous Na2SO4. Filtered, concentrated, separated by column chromatography (DCM: 100%), spun dry, evacuated, weighed the dried product 3-bromoacetanilide and calculated the yield to be 60%. mp86-88 ??C.
3'-BROMOACETANILIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3'-BROMOACETANILIDE manufacturers
- Product
- N-(3-bromophenyl)acetamide 621-38-5
- Price
- US $0.00/kg
- Min. Order
- 20kg
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2025-04-08