2'-BROMOACETANILIDE

Product Name: 2'-BROMOACETANILIDE
CAS No.: 614-76-6
Chemical Name: 2'-BROMOACETANILIDE
Synonyms: N-(2-BROMOPHENYL)ACETAMIDE;2-BROMOACETANILIDE;NISTC614766;o-Bromoacetanilide;2'-Bromoacetanilide;Acetanilide, 2'-bromo-;2'-Bromoacetanilide >N-Acetyl-2-bromoaniline;2-Bromo-N-acetylaniline;2'-Bromoacetanilide, 98+%
CBNumber: CB8742191
Molecular Formula: C8H8BrNO
Formula Weight: 214.06
MOL File: 614-76-6.mol

More

Less

2'-BROMOACETANILIDE Property

Melting point:: 96.5-100.5 °C(lit.)
Boiling point:: 346.8±25.0 °C(Predicted)
Density: 1.543±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
pka: 14.19±0.70(Predicted)
form: Crystalline Powder
color: White
BRN: 2086970
CAS DataBase Reference: 614-76-6(CAS DataBase Reference)

More

Less

Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
Hazard Note: Irritant
HS Code: 29242990

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TCI Chemical

Product number: B3139
Product name: 2'-Bromoacetanilide
Purity: >98.0%(GC)
Packaging: 5g
Price: $90
Updated: 2025/07/31

TCI Chemical

Product number: B3139
Product name: 2'-Bromoacetanilide
Purity: >98.0%(GC)
Packaging: 25g
Price: $285
Updated: 2023/06/20

TRC

Product number: B679010
Product name: 2''-Bromoacetanilide
Packaging: 50g
Price: $250
Updated: 2021/12/16

TRC

Product number: B679010
Product name: 2''-Bromoacetanilide
Packaging: 25g
Price: $165
Updated: 2021/12/16

Apolloscientific

Product number: OR4339
Product name: 2'-Bromoacetanilide
Packaging: 25g
Price: $66
Updated: 2021/12/16

More

Less

2'-BROMOACETANILIDE Chemical Properties,Usage,Production

Uses

2''-Bromoacetanilide is used as a reagent in the preparation of furan-2-ylmethylene thiazolidinediones as novel, potent, and selective inhibitors of phosphoinositide 3-kinase γ.

Synthesis

108-24-7

615-36-1

614-76-6

General procedure for the synthesis of 2'-bromoacetanilide from ethanoic anhydride and o-bromoaniline: o-bromoaniline (22.0 g, 128 mmol), acetic anhydride (13.06 g, 128 mmol) and a catalytic amount of 4-dimethylaminopyridine (DMAP) were dissolved in dichloromethane (100 mL), and stirred at 0 °C. The reaction mixture was slowly warmed to room temperature and stirring was continued overnight. Upon completion of the reaction, the reaction mixture was washed with saturated aqueous sodium bicarbonate solution and subsequently concentrated. The concentrated residue was ground with a solvent mixture of hexane/dichloromethane, the solid product was collected by filtration and rinsed with hexane to give 2'-bromoacetanilide (25.4 g, 92.8% yield). The high performance liquid chromatography (HPLC) retention time (Rt) was 1.523 min.

References

[1] Journal of Medicinal Chemistry, 2003, vol. 46, # 11, p. 2187 - 2196
[2] Organic Letters, 2004, vol. 6, # 19, p. 3293 - 3296
[3] Organic Letters, 2016, vol. 18, # 22, p. 5896 - 5899
[4] Dyes and Pigments, 2018, vol. 159, p. 419 - 428
[5] Patent: US2005/192310, 2005, A1. Location in patent: Page/Page column 20

2'-BROMOACETANILIDE Preparation Products And Raw materials

Raw materials

Hexane Acetic anhydride 2-Bromoaniline Sodium bicarbonate Dichloromethane 4-Dimethylaminopyridine

Preparation Products

More

Less

2'-BROMOACETANILIDE Suppliers

Americas 1 China 107 Europe 1 Germany 3 India 5 Japan 1 Switzerland 1 The Netherlands 2 Ukraine 1 United Kingdom 5 United States 21 Global 148

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
Advantage: 62

Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
ProdList: 30123
Advantage: 84

TCI (Shanghai) Development Co., Ltd.

Tel: 021-67121386
Fax: 021-67121385
Email: Sales-CN@TCIchemicals.com
Country: China
ProdList: 24529
Advantage: 81

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

JinYan Chemicals(ShangHai) Co.,Ltd.

Tel: 13817811078
Fax: 86-021-50426522,50426273
Email: sales@jingyan-chemical.com
Country: China
ProdList: 9976
Advantage: 60

Shandong Xiya Chemical Co., Ltd

Tel: 4009903999 13355009207
Fax: 0539-6365991
Email: 3007715519@qq.com
Country: China
ProdList: 18729
Advantage: 57

Syntechem Co.,Ltd

Tel
Fax: E-Mail Inquiry
Email: info@syntechem.com
Country: China
ProdList: 12984
Advantage: 57

ShangHai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847 13636370518
Fax: 021-55068248
Email: shyysw007@163.com
Country: China
ProdList: 4999
Advantage: 60

Thermo Fisher Scientific

Tel: 800-810-5118
Fax: +86-10-84193589
Email: cnchemical@thermofisher.com
Country: China
ProdList: 17770
Advantage: 75

More

Less

View Lastest Price from 2'-BROMOACETANILIDE manufacturers

Honest Joy Holdings Limited

Product: 2-Bromoacetanilide 614-76-6
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.7%
Supply Ability: 100 tons
Release date: 2022-01-14

Career Henan Chemical Co

Product: 2'-BROMOACETANILIDE 614-76-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-08

614-76-6, 2'-BROMOACETANILIDERelated Search:

2'-Bromo-4'-fluoroacetanilide 2',4'-DIBROMOACETANILIDE 2'-BROMOACETANILIDE 4-Acetyl-2-bromoacetanilide 2-BROMO-4'-(TRIFLUOROMETHYL)ACETANILIDE 2'-BROMO-4'-METHYLACETANILIDE 4'-BROMOACETANILIDE,4-BROMOACETANILIDE,P-BROMOACETANILIDE,4'-Bromoacetanilide 250,Bromoacetanilide,P-BROMOACETANILIDE, 98% (SEE 1735),p-BROMOACETANILIDE pure 2-METHYL-4-BROMOACETANILIDE N-Methyl-2-bromoacetanilide 3'-BROMOACETANILIDE,m-bromoacetanilid 4-AMINO-2,6-DIBROMOACETANILIDE N-(2-BROMO-4-ISOPROPYL-PHENYL)-ACETAMIDE 2-CHLORO-N-(2,6-DIBROMO-4-METHYLPHENYL)ACETAMIDE 2'-BROMO-4'-CHLOROACETANILIDE N-(2-BROMO-4-NITRO-PHENYL)-2-CHLORO-ACETAMIDE N-(2-BROMOPHENYL)-3-PHENYLPROP-2-ENAMIDE 2'-BROMO-5'-FLUORO-4'-METHYLACETANILIDE N-(2-BROMOPHENYL)PHTHALIMIDE

2-Bromo-N-acetylaniline

Acetanilide, 2'-bromo-

o-Bromoacetanilide

2-BROMOACETANILIDE

N-(2-BROMOPHENYL)ACETAMIDE

2'-Bromoacetanilide, 98+%

N-(2-bromophenyl)ethanamide

AcetaMide, N-(2-broMophenyl)-

NISTC614766

N-Acetyl-2-bromoaniline

2'-Bromoacetanilide &gt

2'-BROMOACETANILIDE ISO 9001：2015 REACH

2'-Bromoacetanilide

2′-Bromoacetanilide, CAS 614-76-6

614-76-6

C8H8NOBr

Protected Amines

Nitrogen Compounds

Organic Building Blocks

Building Blocks

Anilines, Amides & Amines

Bromine Compounds

Nitrogen Compounds

Organic Building Blocks

Protected Amines