2-Methyl-2-nitropropan-1-ol

Product Name: 2-Methyl-2-nitropropan-1-ol
CAS No.: 76-39-1
Chemical Name: 2-Methyl-2-nitropropan-1-ol
Synonyms: 1-Propanol, 2-methyl-2-nitro-;2-Methyl-2-nitropropanol;2-methyl-2-nitro-1-propano;2-NITRO-2-METHYL-1-PROPANOL;2-METHYL-2-NITRO-1-PROPANOL;2-NITROISOBUTANOL;Methylnitropropanol;methyl-2nitro-2propanol;2-Nitro-2-methylpropanol;2-methyl-2-nitropropan-1-ol
CBNumber: CB3474945
Molecular Formula: C4H9NO3
Formula Weight: 119.12
MOL File: 76-39-1.mol

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2-Methyl-2-nitropropan-1-ol Property

Melting point:: 86-89 °C(lit.)
Boiling point:: 94-95 °C10 mm Hg(lit.)
Density: 1.0765 (estimate)
refractive index: 1.4413 (estimate)
pka: 13.79±0.10(Predicted)
InChI: InChI=1S/C4H9NO3/c1-4(2,3-6)5(7)8/h6H,3H2,1-2H3
InChIKey: MVGJRISPEUZYAQ-UHFFFAOYSA-N
SMILES: C(O)C(C)([N+]([O-])=O)C
NIST Chemistry Reference: 1-Propanol, 2-methyl-2-nitro-(76-39-1)
EPA Substance Registry System: 1-Propanol, 2-methyl-2-nitro- (76-39-1)

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Safety

WGK Germany: 3
RTECS: UB8575000
Hazardous Substances Data: 76-39-1(Hazardous Substances Data)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P330Rinse mouth.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

AK Scientific

Product number: 0231BA
Product name: 2-Methyl-2-nitro-1-propanol
Packaging: 250mg
Price: $181
Updated: 2021/12/16

Matrix Scientific

Product number: 159675
Product name: 2-Methyl-2-nitropropan-1-ol
Packaging: 0.500g
Price: $240
Updated: 2021/12/16

Matrix Scientific

Product number: 159675
Product name: 2-Methyl-2-nitropropan-1-ol
Packaging: 1g
Price: $300
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0009071
Product name: 2-METHYL-2-NITRO-1-PROPANOL
Purity: 95.00%
Packaging: 5MG
Price: $499.28
Updated: 2021/12/16

Matrix Scientific

Product number: 159675
Product name: 2-Methyl-2-nitropropan-1-ol
Packaging: 5g
Price: $1000
Updated: 2021/12/16

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2-Methyl-2-nitropropan-1-ol Chemical Properties,Usage,Production

Uses

The direct hydrogenation of 2-Methyl-2-nitropropan-1-ol obtains product 2-amino-2-methyl-1-propanol (AMP-95). AMP-95 is a kind of multifunction additive being widely known by the people, be widely used in coating and printing ink, metal working fluid, in the industries such as personal nursing and medicine intermediate.

Synthesis

By catalyst 10g (Ti-V-ZSM-5), acetone 58.08g, ammonium hydroxide 20g are added in 400ml methanol, are warming up to 70 DEG C, hydrogen peroxide (35%) 226.7g is slowly added dropwise, temperature is maintained to react 1h at 65-75 DEG C, obtain 2- nitros third after being added dropwise Alkane reaction solution；Filtering adds in 5g sodium hydroxides to reaction solution, is warming up to 35 DEG C, formaldehyde (40% aqueous solution) is added dropwise, drip with the reaction was continued afterwards 3h, obtains 2-Methyl-2-nitropropan-1-ol.

Purification Methods

Distil it under vacuum and/or crystallise it from pet ether or MeOH. [Astle & Abbott J Org Chem 21 1229 1956, Kambe & Yasuda Bull Soc Chem Jpn 41 1444 1968, Beilstein 1 H 378, 1 III 1546, 1 IV 1604.]

2-Methyl-2-nitropropan-1-ol Preparation Products And Raw materials

Raw materials

Preparation Products

2-Amino-2-methyl-1-propanol 1,2-DIAMINO-2-METHYLPROPANE

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2-Methyl-2-nitropropan-1-ol Suppliers

Belgium 1 China 41 Europe 1 France 1 Germany 3 India 2 Japan 1 Switzerland 1 United Kingdom 3 United States 20 Global 74

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