3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
- Product Name
- 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
- CAS No.
- 24422-15-9
- Chemical Name
- 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
- Synonyms
- Rivaroxaban Impurity 166;trichlorothiophene-2-carbonyl chloride;3,4,5-trichloro-2-thiophenecarbonyl chloride;3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE;2-Thiophenecarbonyl chloride, 3,4,5-trichloro-;3,4,5-Trichlorothien-2-carboxylic acid chloride
- CBNumber
- CB3482535
- Molecular Formula
- C5Cl4OS
- Formula Weight
- 249.93
- MOL File
- 24422-15-9.mol
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Property
- Melting point:
- 38-40°C
- Boiling point:
- 124-125°C 10mm
- Flash point:
- 124-125°C/10mm
- Sensitive
- Moisture Sensitive
- BRN
- 1427060
Safety
- Risk Statements
- 34
- Safety Statements
- 26-36/37/39-45
- RIDADR
- 3261
- HazardClass
- 8
- PackingGroup
- II
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H314Causes severe skin burns and eye damage
H318Causes serious eye damage
- Precautionary statements
-
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- L17704
- Product name
- 3,4,5-Trichlorothiophene-2-carbonyl chloride, 97%
- Packaging
- 1g
- Price
- $38.9
- Updated
- 2021/12/16
- Product number
- L17704
- Product name
- 3,4,5-Trichlorothiophene-2-carbonyl chloride, 97%
- Packaging
- 5g
- Price
- $118
- Updated
- 2021/12/16
- Product number
- MT-36791
- Product name
- 3,4,5-Trichlorothiophene-2-carbonylchloride
- Purity
- 97%
- Packaging
- 25g
- Price
- $300
- Updated
- 2021/12/16
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Chemical Properties,Usage,Production
Preparation
3,4,5-Trichlorothiophene-2-carbonyl chloride synthesis: A mixture of 3,4,5-trichloro-2-thiophenecarboxylic acid (20.4 g, 0.088 mol), SOCl2 (7.3 mL, 0.1 mol), and DMF (0.2 mL) in 80 mL of 1,2-dichloroethane was heated at reflux temperature for 3 h. The reaction mixture became homogeneous after 1 h of heating. The solution was cooled to 25℃, concentrated and placed under high vacuum to remove residual solvent, giving 22.0 g (98% wt.) of 3,4,5-trichloro-2-thiophenecarbonyl chloride as an oil which solidified on standing to an off-white powder; m.p. 37-41℃, having a GC area % purity > 99%.
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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