METHYL 4-FLUOROPHENYLACETATE
- Product Name
- METHYL 4-FLUOROPHENYLACETATE
- CAS No.
- 34837-84-8
- Chemical Name
- METHYL 4-FLUOROPHENYLACETATE
- Synonyms
- Methyl 2-(4-fluorophenyl);METHYL 4-FLUOROPHENYLACETATE;Methyl4-fluorophenylacetate,98%;METHYL 4-FLUOROPHENYLACETATE, 99;Methyl 4-fluorophenylacetate 98%;Methyl 2-(4-fluorophenyl)acetate;Benzeneacetic acid, 4-fluoro-, methyl ester
- CBNumber
- CB3502055
- Molecular Formula
- C9H9FO2
- Formula Weight
- 168.16
- MOL File
- 34837-84-8.mol
METHYL 4-FLUOROPHENYLACETATE Property
- Boiling point:
- 210°C (rough estimate)
- Density
- 1.1410 (estimate)
- refractive index
- 1.4870
- storage temp.
- Sealed in dry,Room Temperature
- form
- Liquid
- color
- Clear colorless to yellow
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 36/37/39-26
- HS Code
- 29153900
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M305558
- Product name
- Methyl2-(4-fluorophenyl)acetate
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 119944
- Product name
- Methyl 2-(4-fluorophenyl)acetate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $82
- Updated
- 2021/12/16
- Product number
- 2623-3-X0
- Product name
- Methyl 4-fluorophenylacetate
- Purity
- 98%
- Packaging
- 1g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- JK623400
- Product name
- Methyl4-fluorophenylacetate
- Purity
- 99%
- Packaging
- 5g
- Price
- $67
- Updated
- 2021/12/16
- Product number
- J96330
- Product name
- Methyl2-(4-fluorophenyl)acetate
- Packaging
- 100g
- Price
- $135
- Updated
- 2021/12/16
METHYL 4-FLUOROPHENYLACETATE Chemical Properties,Usage,Production
Chemical Properties
clear colorless to yellow liquid
Synthesis
67-56-1
405-50-5
34837-84-8
Step 1: 4-Fluorophenylacetic acid (700 mg, 4.34 mmol) was dissolved in methanol at room temperature and concentrated sulfuric acid (0.42 mL, 4.34 mmol, 0.1 equiv) was added slowly. The reaction mixture was refluxed under nitrogen protection at 70 °C for 3 h. The progress of the reaction was monitored by thin layer chromatography (TLC) to confirm complete consumption of the feedstock. After completion of the reaction, the mixture was cooled to room temperature. The solvent was evaporated under reduced pressure and the residue was extracted with ethyl acetate. The organic phase was washed sequentially with saturated brine and dried over anhydrous magnesium sulfate. The organic phase was concentrated under reduced pressure to give the crude product. Finally, the crude product was purified by column chromatography to afford methyl 2-(4-fluorophenyl)acetate (660 mg, 84% yield).
References
[1] Bioorganic and Medicinal Chemistry, 2003, vol. 11, # 13, p. 2843 - 2866
[2] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 15, p. 4694 - 4703
[3] Bioorganic and Medicinal Chemistry Letters, 2008, vol. 18, # 3, p. 1151 - 1156
[4] Patent: WO2005/14539, 2005, A2. Location in patent: Page/Page column 57-59; 68-69
[5] Tetrahedron, 2002, vol. 58, # 51, p. 10113 - 10126
METHYL 4-FLUOROPHENYLACETATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from METHYL 4-FLUOROPHENYLACETATE manufacturers
- Product
- METHYL 4-FLUOROPHENYLACETATE 34837-84-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-07-31
- Product
- METHYL 4-FLUOROPHENYLACETATE, 99 34837-84-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99.99%
- Supply Ability
- 200KG
- Release date
- 2019-09-03