Preparation
ChemicalBook > CAS DataBase List > 3 5-DICHLOROPYRIDINE 1-OXIDE 98

3 5-DICHLOROPYRIDINE 1-OXIDE 98

Preparation
Product Name
3 5-DICHLOROPYRIDINE 1-OXIDE 98
CAS No.
15177-57-8
Chemical Name
3 5-DICHLOROPYRIDINE 1-OXIDE 98
Synonyms
TAK438 Impurity 96;Vonoprazan Impuirty101;Vonoprazan Impurity 96;3,5-Dichloropyridine N-oxide;3,5-dicholoropyridine N-oxide;Pyridine,3,5-dichloro-, 1-oxide;3 5-DICHLOROPYRIDINE 1-OXIDE 98;3,5-Dichloropyridine N-oxide 98%
CBNumber
CB3505243
Molecular Formula
C5H3Cl2NO
Formula Weight
163.99
MOL File
15177-57-8.mol
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3 5-DICHLOROPYRIDINE 1-OXIDE 98 Property

Melting point:
110-113 °C(lit.)
Boiling point:
344.2±22.0 °C(Predicted)
Density 
1.47±0.1 g/cm3 (20 ºC 760 Torr)
storage temp. 
Room temperature.
pka
-0.72±0.10(Predicted)
form 
solid
InChIKey
RODXBOIDZPQDBH-UHFFFAOYSA-N
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36-24/25
WGK Germany 
3
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
596515
Product name
3,5-Dichloropyridine N-oxide
Purity
98%
Packaging
5g
Price
$171
Updated
2023/06/20
TRC
Product number
D438350
Product name
3,5-Dichloropyridine1-oxide
Packaging
100mg
Price
$75
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049610
Product name
3,5-DICHLOROPYRIDINE 1-OXIDE
Purity
95.00%
Packaging
1G
Price
$634.39
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049610
Product name
3,5-DICHLOROPYRIDINE 1-OXIDE
Purity
95.00%
Packaging
5G
Price
$876.46
Updated
2021/12/16
Oakwood
Product number
301129
Product name
3,5-Dichloropyridine N-oxide
Purity
98%
Packaging
1g
Price
$15
Updated
2021/12/16
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3 5-DICHLOROPYRIDINE 1-OXIDE 98 Chemical Properties,Usage,Production

Preparation

3,5-difluoropyridine-N-oxide is prepared by the following steps:A solution of (5) (0.37 g, 3 mmol), peracetic acid ( 1.5 cm3 of 40% solution in  acetic acid) in acetic acid (5 cm3) and chloroform (10 cm3) was heated at 50 "C, with  stirring, for 24 h. The mixture was neutralised by the addition of dilute sodium hydroxide  to the chilled mixture, then remaining peroxides were destroyed by the addition of  sodium metabisulphite (2 g). Following extraction into DCM, the DCM solution was  dried (MgS04) and evaporated to dryness giving a solid which was recrystallised from  DCM- petrol (1: 1) to yield 3,5-difluoropyridine-N-oxide (0.3 g, 71 %), m.p. 136.5 "C  (Found: C, 45.5; H, 2.3; N, 10.1. C5H3F2NO requires C, 45.8; H, 2.3; N, 10.7%); IR  spectra no. 23; mass spectra no. 31; nmr spectrum no. 21.

3 5-DICHLOROPYRIDINE 1-OXIDE 98 Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3 5-DICHLOROPYRIDINE 1-OXIDE 98 manufacturers

Hebei Chuanghai Biotechnology Co,.LTD
Product
3 5-DICHLOROPYRIDINE 1-OXIDE 98 15177-57-8
Price
US $9.00/KG
Min. Order
1KG
Purity
99.8%
Supply Ability
100tons
Release date
2024-08-16
Honest Joy Holdings Limited
Product
3,5-Dichloropyridine 1-oxide 15177-57-8
Price
US $0.00/KG
Min. Order
1KG
Purity
99.3%
Supply Ability
100 tons
Release date
2022-02-08
Career Henan Chemical Co
Product
3 5-DICHLOROPYRIDINE 1-OXIDE 98 15177-57-8
Price
US $0.01/KG
Min. Order
1KG
Purity
98%;99%
Supply Ability
1kg; 5kg;10kg;25kg
Release date
2020-01-07