ChemicalBook > CAS DataBase List > 2-BROMOBENZAMIDE

2-BROMOBENZAMIDE

Product Name
2-BROMOBENZAMIDE
CAS No.
4001-73-4
Chemical Name
2-BROMOBENZAMIDE
Synonyms
2-BROMOBENZAMIDE;O-BROMOBENZAMIDE;Benzamide, o-bromo-;Benzamide, 2-bromo-;2-Bromobenzamide >2-BROMOBENZAMIDE 98%;2-Bromobenzamide,98%;2-Bromobenzamide, 97+%;2-Bromobenzenecarboxamide
CBNumber
CB3692905
Molecular Formula
C7H6BrNO
Formula Weight
200.03
MOL File
4001-73-4.mol
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2-BROMOBENZAMIDE Property

Melting point:
160-162 °C (lit.)
Boiling point:
158-161 °C(Press: 12 Torr)
Density 
1.5488 (rough estimate)
refractive index 
1.5500 (estimate)
storage temp. 
Sealed in dry,Room Temperature
form 
Powder
pka
15.36±0.50(Predicted)
color 
Beige
Water Solubility 
Slightly soluble in water.
CAS DataBase Reference
4001-73-4(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39
WGK Germany 
3
HS Code 
29242990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
190594
Product name
2-Bromobenzamide
Purity
98%
Packaging
10g
Price
$129.2
Updated
2025/07/31
TCI Chemical
Product number
B2050
Product name
2-Bromobenzamide
Purity
>98.0%(HPLC)(N)
Packaging
5g
Price
$161
Updated
2025/07/31
TRC
Product number
B680328
Product name
2-Bromobenzamide
Packaging
2.5g
Price
$65
Updated
2021/12/16
SynQuest Laboratories
Product number
4648-9-02
Product name
2-Bromobenzamide
Purity
98%
Packaging
5G
Price
$20
Updated
2021/12/16
SynQuest Laboratories
Product number
4648-9-02
Product name
2-Bromobenzamide
Purity
98%
Packaging
25g
Price
$55
Updated
2021/12/16
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2-BROMOBENZAMIDE Chemical Properties,Usage,Production

Chemical Properties

Beige powder

Uses

2-Bromobenzamide has been used in microwave assisted one-pot synthesis of substituted 3-(phenylmethylene)isoindolin-1-ones, palladium-catalyzed synthesis of phenanthridinones and in the synthesis of new water-soluble iminophosphorane ligand.

Uses

2-Bromobenzamide has been used in:

  • microwave assisted one-pot synthesis of substituted 3-(phenylmethylene)isoindolin-1-ones
  • palladium-catalyzed synthesis of phenanthridinones
  • synthesis of new water-soluble iminophosphorane ligand

Synthesis

34158-72-0

4001-73-4

General procedure for the synthesis of 2-bromobenzamide from 2-bromobenzaldehyde oxime: In a 25 mL Schlenk reaction flask, 2-bromobenzaldehyde oxime (100 mg, 0.5 mmol) and water (1 mL) were added sequentially. Subsequently, [Cp*Ir(H2O)3][OTf] catalyst was added. The reaction mixture was stirred at 110 °C for 12 h and then cooled to room temperature. Water was removed by rotary evaporation and the product was purified by column chromatography. Yield: 80%. Product characterization data: 1H NMR (500 MHz, DMSO-d6) δ 7.88 (br s, 1H, NH2), 7.64-7.58 (m, 2H, ArH), 7.41-7.34 (m, 2H, ArH); 13C NMR (125 MHz, DMSO-d6) δ 169.0, 139.3, 132.7, 130.6, 128.5, 127.5, 118.6.

References

[1] RSC Advances, 2016, vol. 6, # 43, p. 37093 - 37098
[2] Advanced Synthesis and Catalysis, 2009, vol. 351, # 11-12, p. 1807 - 1812
[3] Catalysis Science and Technology, 2014, vol. 4, # 4, p. 988 - 996
[4] Patent: CN104418682, 2016, B. Location in patent: Paragraph 0070-0074
[5] Catalysis Communications, 2015, vol. 60, p. 120 - 123

2-BROMOBENZAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMOBENZAMIDE Suppliers

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View Lastest Price from 2-BROMOBENZAMIDE manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
2-BROMOBENZAMIDE 4001-73-4
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10000KGS
Release date
2025-04-29
Shaanxi Dideu Medichem Co. Ltd
Product
2-BROMOBENZAMIDE 4001-73-4
Price
US $1.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100000KG
Release date
2024-07-26
Career Henan Chemical Co
Product
2-BROMOBENZAMIDE 4001-73-4
Price
US $3.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2020-02-01

4001-73-4, 2-BROMOBENZAMIDERelated Search:

2-BROMO-N-METHYLBENZAMIDE 2-BROMO-5-METHOXYBENZENE-1-CARBOHYDRAZIDE 2-BROMOBENZAMIDE 2-BROMOBENZHYDRAZIDE N-BENZYL 2-BROMOBENZAMIDE 2-Bromo-N-o-tolylbenzamide 3,5-DIBROMOBENZAMIDE 2-AMINO-5-BROMOBENZAMIDE 4-Bromo-N-isopropylbenzamide 3-Bromo-N-butylbenzamide 4-Bromo-N-cyclopentylbenzamide 4-Bromo-N-phenylbenzamide N-Benzyl-4-bromobenzamide Propargyl 4-bromobenzamide 2-Bromo-N-(3,4-dimethylphenyl)benzamide 2-BROMO-N-(2,4-DIFLUOROPHENYL)BENZAMIDE 4-BROMOBENZAMIDE {[(4-Bromobenzoyl)amino]methyl}furan

  • Benzamide, 2-bromo-
  • Benzamide, o-bromo-
  • 2-Bromobenzamide,98%
  • 2-BROMOBENZAMIDE 98%
  • 2-Bromobenzenecarboxamide
  • 2-Bromobenzamide, 97+%
  • O-BROMOBENZAMIDE
  • 2-BROMOBENZAMIDE
  • 2-Bromobenzamide &gt
  • 4001-73-4
  • C7H6BrNO
  • AMINE
  • Building Blocks
  • Amides
  • Carbonyl Compounds
  • Organic Building Blocks
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
  • Anilines, Amides & Amines
  • Bromine Compounds
  • Amides
  • Carbonyl Compounds
  • Organic Building Blocks