ChemicalBook > CAS DataBase List > 2-Methyl-4-phenyl-1H-imidazole

2-Methyl-4-phenyl-1H-imidazole

Product Name: 2-Methyl-4-phenyl-1H-imidazole
CAS No.: 13739-48-5
Chemical Name: 2-Methyl-4-phenyl-1H-imidazole
Synonyms: 2-Methyl-4-phenylimidazole;2-Methyl-5-phenyliMidazole;4-(2-Methyl Phenyl)IMidazole;2-METHYL-4-PHENYL-1H-IMIDAZOLE;2-methyl-4-phenyl-3H-imidazole;2-methyl-5-phenyl-1H-imidazole;1H-Imidazole, 2-methyl-5-phenyl-;1H-imidazole, 2-methyl-4-phenyl-;2-methyl-4-phenyl-1H-imidazole(SALTDATA: FREE)
CBNumber: CB3755312
Molecular Formula: C10H10N2
Formula Weight: 158.2
MOL File: 13739-48-5.mol

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2-Methyl-4-phenyl-1H-imidazole Property

Melting point:: 159-160.5 °C
Boiling point:: 396.2±11.0 °C(Predicted)
Density: 1.109±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.13±0.10(Predicted)
Appearance: White to light yellow Solid

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Safety

Risk Statements: 36
Safety Statements: 26
HazardClass: IRRITANT
HS Code: 2933299090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B399925
Product name: 2-Methyl-4-phenyl-1H-imidazole
Packaging: 100mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B399925
Product name: 2-Methyl-4-phenyl-1H-imidazole
Packaging: 500mg
Price: $220
Updated: 2021/12/16

Apolloscientific

Product number: OR942345
Product name: 2-Methyl-4-phenyl-1H-imidazole
Purity: 95%
Packaging: 1g
Price: $235
Updated: 2021/12/16

Matrix Scientific

Product number: 061241
Product name: 2-Methyl-4-phenyl-1H-imidazole
Packaging: 500mg
Price: $315
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-1-JA
Product name: 2-Methyl-4-phenyl-1H-imidazole
Purity: 95%
Packaging: 1g
Price: $376
Updated: 2021/12/16

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2-Methyl-4-phenyl-1H-imidazole Chemical Properties,Usage,Production

Synthesis

451-50-3

13739-48-5

Using stilbene (150 mL) as solvent, benzoylacetamide (10.15 mmol), ammonium acetate (64.86 mmol) and acetic acid (166.6 mmol) were added and the mixture was heated to reflux and azeotropized to remove the water, and the reaction lasted for 6 hours. Upon completion of the reaction, the reaction mixture was cooled to room temperature and washed with 25 mL of water followed by distillation to remove the solvent to give the crude product. The crude product was purified by column chromatography using silica gel (60-120 mesh) as stationary phase and a solvent mixture of dichloromethane and methanol (100:5, v/v) as mobile phase to give the final target compound 2-methyl-4-phenyl-1H-imidazole.

References

[1] Patent: WO2009/137081, 2009, A2. Location in patent: Page/Page column 49-51

2-Methyl-4-phenyl-1H-imidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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