ChemicalBook > CAS DataBase List > 9-IODOPHENANTHRENE

9-IODOPHENANTHRENE

Product Name: 9-IODOPHENANTHRENE
CAS No.: 17024-12-3
Chemical Name: 9-IODOPHENANTHRENE
Synonyms: 9-IODOPHENANTHRENE;9-Phenanthryl iodide;Phenanthrene, 9-iodo-;9-Iodophenanthrene 97%;2,5-bis(4-ethoxyanilino)-3,6-dimethoxycyclohexa-2,5-diene-1,4-dione
CBNumber: CB3760198
Molecular Formula: C14H9I
Formula Weight: 304.13
MOL File: 17024-12-3.mol

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9-IODOPHENANTHRENE Property

Melting point:: 91-93 °C (lit.)
Boiling point:: 411.0±14.0 °C(Predicted)
Density: 1.692±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
Appearance: Light yellow to yellow Solid
Stability:: Stable, but light sensitive - store in the dark. Incompatible with strong oxidizing agents.
InChI: InChI=1S/C14H9I/c15-14-9-10-5-1-2-6-11(10)12-7-3-4-8-13(12)14/h1-9H
InChIKey: CBFIPOTVFMLMFQ-UHFFFAOYSA-N
SMILES: C1=C2C(C3C(C(I)=C2)=CC=CC=3)=CC=C1

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 389358
Product name: 9-Iodophenanthrene
Purity: 97%
Packaging: 1g
Price: $74.7
Updated: 2025/07/31

Usbiological

Product number: 280756
Product name: 9-Iodophenanthrene
Packaging: 5g
Price: $2088
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0067235
Product name: 9-IODOPHENANTHRENE
Purity: 95.00%
Packaging: 50G
Price: $2679.6
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0067235
Product name: 9-IODOPHENANTHRENE
Purity: 95.00%
Packaging: 100G
Price: $2899.05
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0067235
Product name: 9-IODOPHENANTHRENE
Purity: 95.00%
Packaging: 25G
Price: $1270.5
Updated: 2021/12/16

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9-IODOPHENANTHRENE Chemical Properties,Usage,Production

Chemical Properties

solid

Synthesis

573-17-1

17024-12-3

General procedure for the synthesis of 9-iodophenanthrene from 9-bromophenanthrene: General method: aryl bromide (10 mmol) was dissolved in anhydrous THF (30 mL) and cooled to -78 °C at room temperature. Slowly add n-butyllithium (1.6 M, dissolved in hexane; 7.5 mL; 12 mmol) dropwise. After 15 min of reaction, a solution of anhydrous THF (10 mL) with iodine (I2, 3.81 g; 15 mmol) was added, followed by gradual warming of the reaction mixture to room temperature and stirring overnight. After completion of the reaction, the mixture was concentrated under vacuum. Water (H2O) was added to the residue and extracted with dichloromethane (DCM, 3 times). The organic phases were combined and washed sequentially with saturated sodium thiosulfate (Na2S2O5) solution and water. The organic phase was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure, and the resulting crude product was purified by column chromatography.

References

[1] Synlett, 2013, vol. 24, # 20, p. 2730 - 2734
[2] Synthesis, 1986, # 1, p. 121 - 122
[3] Journal of Organic Chemistry, 2009, vol. 74, # 12, p. 4650 - 4653
[4] Tetrahedron Letters, 1999, vol. 40, # 36, p. 6671 - 6672
[5] Beilstein Journal of Organic Chemistry, 2011, vol. 7, p. 1499 - 1503

9-IODOPHENANTHRENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 9-IODOPHENANTHRENE manufacturers

Henan Fengda Chemical Co., Ltd

Product: Phenanthrene, 9-iodo- 17024-12-3
Price: US $5.00-0.50/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-13

17024-12-3, 9-IODOPHENANTHRENERelated Search:

4-(3,5-dimethylphenyl)-3-iodophenanthrene 2-iodophenanthrene-9,10-dione 2,7-Diiodophenanthrenequinone 1-Iodonaphthalene 9-IODO-10-PHENYLPHENANTHRENE 2-IODONAPHTHALENE 9-IODOPHENANTHRENE

9-IODOPHENANTHRENE

9-Iodophenanthrene 97%

9-Phenanthryl iodide

2,5-bis(4-ethoxyanilino)-3,6-dimethoxycyclohexa-2,5-diene-1,4-dione

Phenanthrene, 9-iodo-

17024-12-3

C14H9I

Organic Building Blocks

Halogenated Hydrocarbons

C13 to C37+

Aryl

Building Blocks

Aryl

C13 to C37+

Halogenated Hydrocarbons