PENTAERYTHRITOL TRICHLOROHYDRIN
- Product Name
- PENTAERYTHRITOL TRICHLOROHYDRIN
- CAS No.
- 813-99-0
- Chemical Name
- PENTAERYTHRITOL TRICHLOROHYDRIN
- Synonyms
- Pentaerythrityl trichlorohydrin;PENTAERYTHRITOL TRICHLOROHYDRIN;2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL;3-CHLORO-2,2-DICHLOROMETHYLPROPANOL;3-Chloro-2,2-bis(chloromethyl)propan-1-ol;2,2-bis(chloromethyl)-3-chloro-1-propanol;3- CHLORO-2,2-BIS(CHLOROMETHYL)-1-PROPANOL;1-Propanol,3-chloro-2,2-bis(chloromethyl)-;3-Chloro-2,2-bis(chloromethyl) propan-1-ol (Pentaerythrityl trichlorohydrin)
- CBNumber
- CB3767117
- Molecular Formula
- C5H9Cl3O
- Formula Weight
- 191.48
- MOL File
- 813-99-0.mol
PENTAERYTHRITOL TRICHLOROHYDRIN Property
- Melting point:
- 80 °C
- Boiling point:
- 274.39°C (rough estimate)
- Density
- 1.4096 (rough estimate)
- refractive index
- 1.5300 (estimate)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 13.83±0.10(Predicted)
- InChI
- InChI=1S/C5H9Cl3O/c6-1-5(2-7,3-8)4-9/h9H,1-4H2
- InChIKey
- VRWHPVMGJTYPLS-UHFFFAOYSA-N
- SMILES
- C(O)C(CCl)(CCl)CCl
Safety
- HS Code
- 2905599890
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H318Causes serious eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- S551198
- Product name
- 2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $185
- Updated
- 2025/07/31
- Product number
- S551198
- Product name
- 2,2,2-TRIS-(CHLOROMETHYL)-ETHANOL
- Purity
- AldrichCPR
- Packaging
- 250MG
- Price
- $179
- Updated
- 2024/03/01
- Product number
- C609745
- Product name
- 3-Chloro-2,2-bis(chloromethyl)propan-1-ol
- Packaging
- 2.5g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 2101-5-02
- Product name
- 3-Chloro-2,2-bis(chloromethyl)propan-1-ol
- Packaging
- 5G
- Price
- $100
- Updated
- 2021/12/16
- Product number
- 0075AF
- Product name
- 3-Chloro-2,2-bis(chloromethyl)propan-1-ol
- Packaging
- 5g
- Price
- $131
- Updated
- 2021/12/16
PENTAERYTHRITOL TRICHLOROHYDRIN Chemical Properties,Usage,Production
Synthesis
115-77-5
813-99-0
The general procedure for the synthesis of 3-chloro-2,2-dichloromethylpropan-1-ol from pentaerythritol was as follows: pentaerythritol (15 g, 0.11 mol) was dissolved in pyridine (27 ml) and heated to 65 °C. Thionyl chloride (24.7 ml, 0.33 mol) was added slowly and dropwise over a period of 4 h. The temperature of the reaction was controlled to be between 65°C and 95°C. After completion of the reaction, the reaction mixture was continued to be stirred at 50 °C for 18 hours. Subsequently, the reaction solution was heated to 120 °C-130 °C for concentration and then cooled to room temperature. The concentrated reaction solution was slowly poured into ice water (75 ml) and stirred for 30 minutes. The resulting solid product was collected by filtration, washed well with water and dried to give 3-chloro-2,2-bis(chloromethyl)propan-1-ol (15.4 g, 73% yield).
References
[1] Patent: KR101592370, 2016, B1. Location in patent: Paragraph 0204; 0205; 0206; 0207
[2] Australian Journal of Chemistry, 1988, vol. 41, # 12, p. 1953 - 1962
[3] Patent: US2835709, 1955,
[4] Mededelingen van de Koninklijke Vlaamse Academie voor Wetenschappen, Letteren en Schone Kunsten van Belgie, Klasse der Wetenschappen, 1940, vol. 2, # 5, p. 3,16
[5] Patent: US2835709, 1955,
PENTAERYTHRITOL TRICHLOROHYDRIN Preparation Products And Raw materials
Raw materials
Preparation Products
PENTAERYTHRITOL TRICHLOROHYDRIN Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from PENTAERYTHRITOL TRICHLOROHYDRIN manufacturers
- Product
- pentaerythritol trichlorohydrin 813-99-0
- Price
- US $2.00-6.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-08-08