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(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL

Product Name
(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL
CAS No.
57012-20-1
Chemical Name
(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL
Synonyms
AKOS PAO-0016;BUTTPARK 93\11-63;RARECHEM AL BD 1315;(2,5-Dimethylpyrazol-3-yl)methanol;(2,5-dimethyl-3-pyrazolyl)methanol;3-diMethyl-1H-pyrazol-5-yl)Methanol;1,3-Dimethyl-1H-pyrazole-5-methanol;1H-Pyrazole-5-methanol, 1,3-dimethyl-;1,3-DIMETHYL-5-(HYDROXYMETHYL)PYRAZOLE;(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL
CBNumber
CB3770797
Molecular Formula
C6H10N2O
Formula Weight
126.16
MOL File
57012-20-1.mol
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(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL Property

Boiling point:
117-118°C 0,8mm
Density 
1.13±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
14.37±0.10(Predicted)
Appearance
Light yellow to yellow Solid
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-22
Safety Statements 
26-36/37/39
Hazard Note 
Irritant
HS Code 
29339900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR23188
Product name
1,3-Dimethyl-5-(hydroxymethyl)-1H-pyrazole
Packaging
250mg
Price
$73
Updated
2021/12/16
SynQuest Laboratories
Product number
4H01-1-W3
Product name
1,3-Dimethyl-5-(hydroxymethyl)-1H-pyrazole
Packaging
250mg
Price
$80
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD135259
Product name
(1,3-Dimethyl-1H-pyrazol-5-yl)methanol
Packaging
250mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD135259
Product name
(1,3-Dimethyl-1H-pyrazol-5-yl)methanol
Packaging
500mg
Price
$150
Updated
2021/12/16
Matrix Scientific
Product number
100968
Product name
(1,3-Dimethyl-1H-pyrazol-5-yl)methanol
Packaging
1g
Price
$208
Updated
2021/12/16
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(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL Chemical Properties,Usage,Production

Chemical Properties

Light yellow solid

Synthesis

891273-63-5

57012-20-1

Step 1: Preparation of (2,5-dimethyl-2H-pyrazol-3-yl) methanol (14): to a solution of compound 13 (4.5 g, 24.7 mmol) in THF (60 mL) was added lithium aluminum hydride (LiAlH4) (1.22 g, 32.1 mmol) in batches at 0°C under nitrogen atmosphere. The reaction mixture was stirred at the same temperature for 2-3 h. The excess LiAlH4 was subsequently quenched by addition of saturated sodium sulfate solution.The reaction mixture was filtered and the residue was washed with ethyl acetate. The filtrates were combined and concentrated under reduced pressure to afford the target product (2,5-dimethyl-2H-pyrazol-3-yl) methanol (14) 3 g as a brown solid. Yield: 86%; 1H NMR (200 MHz, CDCl3): δ 6.0 (s, 1H), 4.57 (d, J = 5.9 Hz, 2H), 3.8 (s, 3H), 3.16 (s, 1H), 2.24 (s, 3H); Mass Spectrometry (CI method, isobutane): 127 (M+1, 100%); IR (KBr, cm-1 ): ν max 3281.

References

[1] Patent: US2006/128729, 2006, A1. Location in patent: Page/Page column 98

(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL Preparation Products And Raw materials

Raw materials

Ethyl 1,3-dimethylpyrazole-5-carboxylate Chloroform Tetrahydrofuran Lithium Aluminum Hydride Methanol

Preparation Products

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(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL Suppliers

Belgium 1 China 73 Germany 4 India 1 Switzerland 1 United Kingdom 4 United States 12 Global 96
J & K SCIENTIFIC LTD.
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18210857532; 18210857532
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86-10-82849933
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jkinfo@jkchemical.com
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China
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025-85760892 13376080562
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Changsha Luxing Bio-Chem Technology Co., Ltd.
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0731-88827538 15873153880
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China
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View Lastest Price from (1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL manufacturers

Career Henan Chemical Co
Product
(1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL 57012-20-1
Price
US $1.00/g
Min. Order
100g
Purity
99%
Supply Ability
KG/T
Release date
2019-12-18

57012-20-1, (1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOLRelated Search:

1-(TERT-BUTYL)-3-METHYL-1H-PYRAZOLE-5-CARBOXYLIC ACID 1-ETHYL-3-METHYL-1H-PYRAZOLE-5-CARBOXYLIC ACID ETHYL ESTER 3-(TERT-BUTYL)-1-METHYL-1H-PYRAZOLE-5-CARBOXYLIC ACID Ethyl 1,3-dimethylpyrazole-5-carboxylate 1,3-Dimethylpyrazole-5-carboxylic acid 4-BROMO-1-ETHYL-3-METHYL-1H-PYRAZOLE-5-CARBOXYLIC ACID 1-ETHYL-3-METHYL-1H-PYRAZOLE-5-CARBOXYLIC ACID (1,5-DIMETHYL-1H-PYRAZOL-3-YL)METHANOL (3,5-DIMETHYL-1H-PYRAZOL-1-YL)METHANOL ETHYL 3-(TERT-BUTYL)-1-METHYL-1H-PYRAZOLE-5-CARBOXYLATE METHYL 1-ETHYL-3-METHYL-1H-PYRAZOLE-5-CARBOXYLATE ETHYL 1-BENZYL-3-(TERT-BUTYL)-1H-PYRAZOLE-5-CARBOXYLATE 1-ETHYL-3-METHYL-4-NITRO-1H-PYRAZOLE-5-CARBOXYLIC ACID ETHYL 3-METHYL-1-PHENYLPYRAZOLE-5-CARBOXYLATE 2,5-DIPHENYL-2H-PYRAZOLE-3-CARBOXYLIC ACID 1-(TERT-BUTYL)-3-METHYL-1H-PYRAZOLE-5-CARBOXYLIC ACID ETHYL ESTER METHYL 4-BROMO-1-ETHYL-3-METHYL-1H-PYRAZOLE-5-CARBOXYLATE (1-ETHYL-3,5-DIMETHYL-1H-PYRAZOL-4-YL)-METHANOL

  • BUTTPARK 93\11-63
  • (1,3-DIMETHYL-1H-PYRAZOL-5-YL)METHANOL
  • 1,3-DIMETHYL-5-(HYDROXYMETHYL)PYRAZOLE
  • 5-(Hydroxymethyl)-1,3-dimethyl-1H-pyrazole
  • 1,3-Dimethyl-5-(hydroxymethyl)-1H-pyrazole
  • (1,3-Dimethyl-1H-pyrazol-5-yl)methanol ,97%
  • 3-diMethyl-1H-pyrazol-5-yl)Methanol
  • (1,3-diMethyl-1h-pyrazole-5-yl)Methanol
  • (2,5-Dimethyl-2H-pyrazol-3-yl)methanol
  • 1,3-Dimethyl-1H-pyrazole-5-methanol
  • (2,5-Dimethylpyrazol-3-yl)methanol
  • AKOS PAO-0016
  • RARECHEM AL BD 1315
  • (2,5-dimethyl-3-pyrazolyl)methanol
  • 5-(Hydroxymethyl)-1,3-dimethylpyrazole
  • 1H-Pyrazole-5-methanol, 1,3-dimethyl-
  • 57012-20-1