2,6-Dichlorobenzyl acetonitrile
- Product Name
- 2,6-Dichlorobenzyl acetonitrile
- CAS No.
- 3215-64-3
- Chemical Name
- 2,6-Dichlorobenzyl acetonitrile
- Synonyms
- Guanfacine Impurity 13;2,6-DICHLOROBENZYL CYANIDE;6-Dichlorophenylacetontrile;2,6-DichlorobenzylCyanide>2,6-DICHLOROPHENYLACETONTRILE;2,6-DICHLOROPHENYLACETONITRILE;2,6-Dichlorobenzeneacetonitrile;2,6-dichlorobenzyl acetonitrile;2,6-Dichloropenzyl Acetonitrile;2,6-Dichlorophenylacetonitrile,97%
- CBNumber
- CB3784389
- Molecular Formula
- C8H5Cl2N
- Formula Weight
- 186.04
- MOL File
- 3215-64-3.mol
2,6-Dichlorobenzyl acetonitrile Property
- Melting point:
- 73-75 °C (lit.)
- Boiling point:
- 306.06°C (rough estimate)
- Density
- 1.4274 (rough estimate)
- refractive index
- 1.5690 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Methanol
- form
- Crystalline Powder
- color
- White to light yellow
- BRN
- 1910482
- Exposure limits
- NIOSH: IDLH 25 mg/m3
- CAS DataBase Reference
- 3215-64-3(CAS DataBase Reference)
- NIST Chemistry Reference
- 2,6-Dichlorophenylacetic acid nitrile(3215-64-3)
Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-36/37/38
- Safety Statements
- 26-37/39-36/37/39
- RIDADR
- 3439
- WGK Germany
- 3
- HazardClass
- 6.1
- PackingGroup
- III
- HS Code
- 29269095
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 126012
- Product name
- 2,6-Dichlorophenylacetonitrile
- Purity
- 97%
- Packaging
- 25g
- Price
- $185
- Updated
- 2023/01/07
- Product number
- D1793
- Product name
- 2,6-Dichlorobenzyl Cyanide
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $73
- Updated
- 2025/07/31
- Product number
- D474038
- Product name
- 2,6-Dichlorophenylacetonitrile
- Packaging
- 500mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D474038
- Product name
- 2,6-Dichlorophenylacetonitrile
- Packaging
- 2.5g
- Price
- $65
- Updated
- 2021/12/16
- Product number
- C146
- Product name
- 2,6-Dichlorophenylacetonitrile
- Packaging
- 5g
- Price
- $10
- Updated
- 2021/12/16
2,6-Dichlorobenzyl acetonitrile Chemical Properties,Usage,Production
Chemical Properties
White to light yellow crystalline powder
General Description
2,6-Dichlorophenylacetonitrile was found to degrade rapidly in non-sterile soils but not in azide treated soils.
Synthesis
151-50-8
2014-83-7
3215-64-3
Example 13-(2,6-dichloro-phenyl)-6-(2,4-difluoro-phenylamino)-1-diethyl-pyrazolo[1,5-a]pyrimidin-2-one was synthesized as follows: Step 1 (Synthesis of 2,6-dichlorophenylacetonitrile): a solution of potassium cyanide (26 g, 400.00 mmol) and 18-crown-6 (0.05 g) in water (60 mL) was added to a 500 mL round bottom flask. Subsequently, an ethanol (300 mL) solution of 2,6-dichlorobenzyl chloride (40 g, 206.24 mmol) was added to this solution. The reaction mixture was stirred under reflux conditions for 1 to 3 hours and the progress of the reaction was monitored by thin layer chromatography (TLC, unfolding agent ratio ethyl acetate: petroleum ether = 1:4). After completion of the reaction, the mixture was concentrated to dryness using a rotary evaporator. The concentrated residue was transferred to a dispensing funnel and washed with water (5 x 100 mL) to afford 35.4 g (95% yield) of 2-(2,6-dichlorophenyl)acetonitrile as a white solid. The product can be used directly in the next reaction without further purification.
References
[1] Patent: WO2007/15866, 2007, A2. Location in patent: Page/Page column 29; 31
2,6-Dichlorobenzyl acetonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,6-Dichlorobenzyl acetonitrile manufacturers
- Product
- 2,6-Dichlorobenzyl acetonitrile 3215-64-3
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-08
- Product
- 2,6-Dichlorobenzyl acetonitrile 3215-64-3
- Price
- US $10.00-7.00/kg
- Min. Order
- 1kg
- Purity
- 99.99%
- Supply Ability
- 10 tons
- Release date
- 2024-06-14
- Product
- 2,6-Dichlorobenzyl acetonitrile 3215-64-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 20T
- Release date
- 2024-07-10