ChemicalBook > CAS DataBase List > 3-(3,5-Dimethylphenoxy)propane-1,2-diol

3-(3,5-Dimethylphenoxy)propane-1,2-diol

Product Name
3-(3,5-Dimethylphenoxy)propane-1,2-diol
CAS No.
59365-66-1
Chemical Name
3-(3,5-Dimethylphenoxy)propane-1,2-diol
Synonyms
Nsc25239;Metaxalone Impurity 3;Metaxalone Impurity A;3-(3,5-Dimethylphenoxy)-1,2-propanediol;3-(3,5-dimethylphenoxy)propane-1,2-diol;1,2-Propanediol, 3-(3,5-dimethylphenoxy)-;Metaxalone Impurity A (3-(3,5-Dimethylphenoxy)propane-1,2-diol);Metaxalone IMpurity A (3-(3, 5-DiMethylphenoxyl)-Propane-1, 2-Diol);Metaxalone Impurity AQ: What is Metaxalone Impurity A Q: What is the CAS Number of Metaxalone Impurity A Q: What is the storage condition of Metaxalone Impurity A Q: What are the applications of Metaxalone Impurity A
CBNumber
CB3855124
Molecular Formula
C11H16O3
Formula Weight
196.24
MOL File
59365-66-1.mol
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3-(3,5-Dimethylphenoxy)propane-1,2-diol Property

Melting point:
66-67 °C
Boiling point:
165-170 °C(Press: 2 Torr)
Density 
1.125±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
DMSO, Methanol
form 
Solid
pka
13.56±0.20(Predicted)
color 
White to Off-White Waxy
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Safety

HS Code 
2905599890
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
D469575
Product name
3-(3,5-Dimethylphenoxy)propane-1,2-diol
Packaging
10g
Price
$250
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD151190
Product name
3-(3,5-Dimethylphenoxy)-1,2-propanediol
Packaging
1g
Price
$280
Updated
2021/12/16
AK Scientific
Product number
J10648
Product name
MetaxaloneImpurityA
Packaging
25mg
Price
$29
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD151190
Product name
3-(3,5-Dimethylphenoxy)-1,2-propanediol
Packaging
250mg
Price
$125
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD151190
Product name
3-(3,5-Dimethylphenoxy)-1,2-propanediol
Packaging
500mg
Price
$200
Updated
2021/12/16
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3-(3,5-Dimethylphenoxy)propane-1,2-diol Chemical Properties,Usage,Production

Uses

3-(3,5-Dimethylphenoxy)propane-1,2-diol is an impurity in the synthesis of Metaxalone (M225850), a muscle relaxant used to relax muscles and relieve pain.

Synthesis

556-52-5

108-68-9

59365-66-1

A mixture of 3,5-dimethylphenol (5.00 g, 40.93 mmol), (±)-glycidol (2.72 mL, 41.01 mmol), triethylamine (0.29 mL, 2.08 mmol), and ethanol (25 mL) was heated and refluxed for about 7 hours. Upon completion of the reaction, ethanol was removed by distillation under reduced pressure. The residue was purified by silica gel column chromatography (eluent: petroleum ether solution of 25% ethyl acetate) to afford the target product 3-(3,5-dimethylphenoxy)-1,2-propanediol as a white solid (6.00 g, 75% yield). The melting point of the product was 47-49°C. 1H NMR (400 MHz, CDCl3) δ 2.28 (s, 6H), 3.68-3.87 (m, 2H), 3.94-4.04 (m, 2H), 4.04-4.12 (m, 1H), 6.55 (s, 2H), 6.62 (s, 1H); IR (film) υ3383,2923,. 2875,1600,1462,1324 cm-1; MS 197 (M + 1).

References

[1] Patent: US2009/270469, 2009, A1. Location in patent: Page/Page column 27-28

3-(3,5-Dimethylphenoxy)propane-1,2-diol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(3,5-Dimethylphenoxy)propane-1,2-diol manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
3-(3,5-Dimethylphenoxy)propane-1,2-diol 59365-66-1
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-10-13
Career Henan Chemical Co
Product
3-(3,5-Dimethylphenoxy)propane-1,2-diol 59365-66-1
Price
US $1.00/KG
Min. Order
1KG
Purity
98%-99.9%HPLC
Supply Ability
100KG
Release date
2020-02-04

59365-66-1, 3-(3,5-Dimethylphenoxy)propane-1,2-diolRelated Search:

Diethoxydimethylsilane (Trifluoromethoxy)benzene 1-Phenoxy-2-propanol (R)-(-)-1,2-Propanediol Propylene glycol 2,2-Dimethyl-1,3-propanediol BIS-Tris Propane Benzaldehyde propylene glycol acetal Anisole Oxydipropyl dibenzoate Dimethyldimethoxysilane Propane CLEMASTANIN A Carlinoside 4-Hydroxy Propofol 4-O-b-D-Glucuronide 3-(3,5-Dimethylphenoxy)propane-1,2-diol AURORA 4790

  • 3-(3,5-dimethylphenoxy)propane-1,2-diol
  • 3-(3,5-Dimethylphenoxy)-1,2-propanediol
  • Nsc25239
  • Metaxalone IMpurity A (3-(3, 5-DiMethylphenoxyl)-Propane-1, 2-Diol)
  • Metaxalone Impurity A
  • Metaxalone Impurity A (3-(3,5-Dimethylphenoxy)propane-1,2-diol)
  • 1,2-Propanediol, 3-(3,5-dimethylphenoxy)-
  • Metaxalone Impurity 3
  • Metaxalone Impurity AQ: What is Metaxalone Impurity A Q: What is the CAS Number of Metaxalone Impurity A Q: What is the storage condition of Metaxalone Impurity A Q: What are the applications of Metaxalone Impurity A
  • 59365-66-1