5-Bromo-2-(dimethylamino)pyridine

Product Name: 5-Bromo-2-(dimethylamino)pyridine
CAS No.: 26163-07-5
Chemical Name: 5-Bromo-2-(dimethylamino)pyridine
Synonyms: 3-Bromo-6-dimethylaminopyridine;5-Bromo-N,N-dimethylpyridin-2-amine;5-Bromo-N,N-dimethyl-2-pyridinamine;(5-bromo-pyridin-2-yl)-dimethylamine;5-bromo-2-(N,N-dimethyl-1-yl)pyridine;2-PyridinaMine, 5-broMo-N,N-diMethyl-;5-Bromo-N,N-dimethylpyridin-2-ylamine;5-Bromo-2-(dimethylamino)pyridine ISO 9001：2015 REACH
CBNumber: CB3957798
Molecular Formula: C7H9BrN2
Formula Weight: 201.06
MOL File: 26163-07-5.mol

More

Less

5-Bromo-2-(dimethylamino)pyridine Property

Melting point:: 69-71 °C
Boiling point:: 253.5±20.0 °C(Predicted)
Density: 1.469±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: solid
pka: 5.31±0.10(Predicted)
Appearance: Off-white to light yellow Solid
InChI: InChI=1S/C7H9BrN2/c1-10(2)7-4-3-6(8)5-9-7/h3-5H,1-2H3
InChIKey: XIMCGXXYEMOWQP-UHFFFAOYSA-N
SMILES: C1(N(C)C)=NC=C(Br)C=C1

More

Less

Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
Hazard Note: Irritant
HS Code: 2933399990

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

Sigma-Aldrich

Product number: SYX00280
Product name: 5-Bromo-2-dimethylaminopyridine
Packaging: 1g
Price: $87.5
Updated: 2025/07/31

TRC

Product number: B691533
Product name: 5-Bromo-2-(dimethylamino)pyridine
Packaging: 1g
Price: $75
Updated: 2021/12/16

TRC

Product number: B691533
Product name: 5-Bromo-2-(dimethylamino)pyridine
Packaging: 250mg
Price: $55
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-9-Y9
Product name: 5-Bromo-2-(dimethylamino)pyridine
Packaging: 5G
Price: $66
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: B1391
Product name: 5-Bromo-2-(dimethylamino)pyridine
Purity: 97%
Packaging: 25g
Price: $70
Updated: 2021/12/16

More

Less

5-Bromo-2-(dimethylamino)pyridine Chemical Properties,Usage,Production

Synthesis

1072-97-5

74-88-4

26163-07-5

Step 64a: Synthesis of 5-bromo-N,N-dimethylpyridin-2-amine (Compound 0601-114) To a solution of 5-bromopyridin-2-amine (1.0 g, 5.8 mmol) in tetrahydrofuran (THF, 25 mL) was added sodium hydride (NaH, 60% dispersed in mineral oil, 0.92 g, 23.1 mmol) at 0°C and the reaction mixture was stirred for 10 minutes. Subsequently, iodomethane (CH3I, 1 mL, 16 mmol) was added and the reaction continued to be stirred for 2 hours. Upon completion of the reaction, the reaction was quenched by the addition of water (30 mL) and extracted with ethyl acetate (3 x 30 mL). The organic layers were combined, washed with saturated brine, dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate, 10% v/v) to give the title compound (1.1 g, 94% yield) as a white solid. LCMS: 203 [M+2]+. 1H NMR (400 MHz, DMSO-d6) δ 2.99 (s, 6H), 6.61 (d, J = 9.6 Hz, 1H), 7.62 (dd, J = 9.2, 2.8 Hz, 1H), 8.12 (d, J = 2.4 Hz, 1H).

References

[1] Patent: WO2011/130628, 2011, A1. Location in patent: Page/Page column 206
[2] Patent: US2013/102595, 2013, A1. Location in patent: Paragraph 0485; 0486
[3] Patent: JP2015/187145, 2015, A. Location in patent: Paragraph 0418

5-Bromo-2-(dimethylamino)pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

5-Bromo-2-(dimethylamino)pyridine Suppliers

China 93 Germany 1 India 1 United Kingdom 4 United States 8 Global 107

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

ChemFuture PharmaTech (Jiangsu) Ltd

Tel: 5108538618
Fax: 86 510 85386988-8017
Email: suger.wang@chemfuture.com
Country: China
ProdList: 832
Advantage: 65

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Wuhan Chemwish Technology Co., Ltd

Tel: 86-027-67849912
Fax: 86-027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 35896
Advantage: 56

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
Advantage: 66

Tetranov Biopharm

Tel: 13526569071
Email: sales@leadmedpharm.com
Country: China
ProdList: 7892
Advantage: 64

Nanjing Chemlin Chemical Co., Ltd

Tel: 025-83697070
Fax: +86-25-83453306
Email: info@chemlin.com.cn
Country: China
ProdList: 16075
Advantage: 64

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Chiba Pharmaceutical Science and technology Co, Ltd.

Tel: 0531-81313138 13066006660
Fax: QQ: 3366077777
Email: chibapharm@foxmail.com
Country: China
ProdList: 3991
Advantage: 55

NovoChemy Ltd.

Tel: 021-31261262/ 49 (0)17662837245
Fax: (0)21-33250524
Email: sales@novochemy.com
Country: Germany
ProdList: 6328
Advantage: 58

More

Less

View Lastest Price from 5-Bromo-2-(dimethylamino)pyridine manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 5-Bromo-2-(dimethylamino)pyridine 26163-07-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-12

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-Bromo-2-(dimethylamino)pyridine 26163-07-5
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-Bromo-2-(dimethylamino)pyridine 26163-07-5
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

26163-07-5, 5-Bromo-2-(dimethylamino)pyridineRelated Search:

5-Bromo-2-(dimethylamino)pyridine 4-(5-BROMOPYRIDIN-2-YL)MORPHOLINE 2-Dimethylaminopyridine 5-Bromo-2-(piperidin-1-yl)pyridine 4-(5-BROMO-3-NITRO-PYRIDIN-2-YL)-MORPHOLINE 1-(5-bromopyridin-2-yl)-2,5-dihydro-1H-pyrrole-2,5-dione SALOR-INT L331910-1EA 2-amino-1-(5-bromo-2-pyridinyl)-4-(2,4-dichlorophenyl)-7,7-dimethyl-5-oxo-1,4,5,6,7,8-hexahydro-3-quinolinecarbonitrile 2-amino-4-(4-bromophenyl)-1-(5-bromo-2-pyridinyl)-5-oxo-1,4,5,6,7,8-hexahydro-3-quinolinecarbonitrile 4-ACETYL-1-(5-BROMOPYRIDIN-2-YL)-3-HYDROXY-5-(4-HYDROXY-3-METHOXYPHENYL)-1,5-DIHYDRO-2H-PYRROL-2-ONE SALOR-INT L148709-1EA SALOR-INT L357340-1EA 3-(5-BROMOPYRIDIN-2-YL)-2-(2,4-DICHLOROPHENYL)QUINAZOLIN-4(3H)-ONE 3-(5-BROMOPYRIDIN-2-YL)-2-(2-FURYL)QUINAZOLIN-4(3H)-ONE SALOR-INT L220426-1EA SALOR-INT L331899-1EA SALOR-INT L221848-1EA SALOR-INT L357367-1EA

2-PyridinaMine, 5-broMo-N,N-diMethyl-

5-Bromo-N,N-dimethyl-2-pyridinamine

5-Bromo-N,N-dimethylpyridin-2-amine

5-bromo-2-(N,N-dimethyl-1-yl)pyridine

(5-bromo-pyridin-2-yl)-dimethylamine

3-Bromo-6-dimethylaminopyridine

5-Bromo-2-(dimethylamino)pyridine ISO 9001：2015 REACH

5-Bromo-N,N-dimethylpyridin-2-ylamine

26163-07-5

alkyl bromide

Pyridine

Amino

Organohalides