ChemicalBook > CAS DataBase List > 5-ACETYL-2-METHOXYPYRIDINE, 97%

5-ACETYL-2-METHOXYPYRIDINE, 97%

Product Name
5-ACETYL-2-METHOXYPYRIDINE, 97%
CAS No.
213193-32-9
Chemical Name
5-ACETYL-2-METHOXYPYRIDINE, 97%
Synonyms
CAS:213193-32-9;5-Acetyl-2-methoxypyridine;5-Acetyl-2-methoxypyridine>1-(6-Methoxy-3-pyridinyl)ethanone;[5-ACETYL-2-METHOXYPYRIDINE, 97%];1-(6-Methoxy-pyridin-3-yl)-ethanone;1-(6-Methoxypyridin-3-yl)ethan-1-one;Ethanone, 1-(6-methoxy-3-pyridinyl)-;Ethanone, 1-(6-methoxy-3-pyridinyl)- (9CI);5-ACETYL-2-METHOXYPYRIDINE, 97% ISO 9001:2015 REACH
CBNumber
CB3973064
Molecular Formula
C8H9NO2
Formula Weight
151.16
MOL File
213193-32-9.mol
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5-ACETYL-2-METHOXYPYRIDINE, 97% Property

Melting point:
53-57 °C (lit.)
Boiling point:
269.5±20.0 °C(Predicted)
Density 
1.093±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
1.60±0.10(Predicted)
form 
Powder or Crystalline Powder
color 
White to yellow
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
597767
Product name
5-Acetyl-2-methoxypyridine
Purity
97%
Packaging
5g
Price
$84.48
Updated
2025/07/31
Sigma-Aldrich
Product number
597767
Product name
5-Acetyl-2-methoxypyridine
Purity
97%
Packaging
1g
Price
$38
Updated
2023/06/20
TCI Chemical
Product number
A2797
Product name
5-Acetyl-2-methoxypyridine
Purity
>98.0%(GC)
Packaging
1g
Price
$38
Updated
2025/07/31
TRC
Product number
A189020
Product name
5-Acetyl-2-methoxypyridine
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
A189020
Product name
5-Acetyl-2-methoxypyridine
Packaging
50mg
Price
$60
Updated
2021/12/16
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5-ACETYL-2-METHOXYPYRIDINE, 97% Chemical Properties,Usage,Production

Uses

5-Acetyl-2-methoxypyridine is a useful synthesis intermediate.

Synthesis

858600-08-5

75-16-1

213193-32-9

Step 2: Amide (10.4 g, 53 mmol) was dissolved in tetrahydrofuran (THF, 100 mL) and the solution was cooled to 0°C. Methylmagnesium bromide (3M ether solution, 26.5 mL) was added slowly and dropwise at 0 °C. After the dropwise addition was completed, the reaction mixture was kept at 0°C and continued to be stirred for 1 hour. Subsequently, the reaction was quenched slowly with 1 M hydrochloric acid (aqueous solution). The mixture was extracted with ethyl acetate (EtOAc) and the organic layers were combined. The organic layer was washed with saturated brine and dried with anhydrous magnesium sulfate (MgSO4). After filtration to remove the drying agent, the filtrate was concentrated under reduced pressure to give 7.8 g of 5-acetyl-2-methoxypyridine in the form of a colorless solid in 97% yield.

References

[1] Patent: WO2009/5646, 2009, A2. Location in patent: Page/Page column 167
[2] Patent: WO2015/48507, 2015, A1. Location in patent: Paragraph 0169
[3] Tetrahedron, 2014, vol. 70, # 40, p. 7207 - 7220

5-ACETYL-2-METHOXYPYRIDINE, 97% Preparation Products And Raw materials

Raw materials

Preparation Products

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5-ACETYL-2-METHOXYPYRIDINE, 97% Suppliers

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View Lastest Price from 5-ACETYL-2-METHOXYPYRIDINE, 97% manufacturers

Career Henan Chemical Co
Product
5-ACETYL-2-METHOXYPYRIDINE, 97% 213193-32-9
Price
US $1.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
Customized
Release date
2018-12-14

213193-32-9, 5-ACETYL-2-METHOXYPYRIDINE, 97%Related Search:


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  • 1-(6-Methoxypyridin-3-yl)ethan-1-one
  • 1-(6-Methoxy-pyridin-3-yl)-ethanone
  • [5-ACETYL-2-METHOXYPYRIDINE, 97%]
  • 1-(6-Methoxy-3-pyridinyl)ethanone
  • Ethanone, 1-(6-methoxy-3-pyridinyl)- (9CI)
  • 5-Acetyl-2-methoxypyridine&gt
  • Ethanone, 1-(6-methoxy-3-pyridinyl)-
  • 5-ACETYL-2-METHOXYPYRIDINE, 97% ISO 9001:2015 REACH
  • CAS:213193-32-9
  • 213193-32-9
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