5-ACETYL-2-METHOXYPYRIDINE, 97%
- Product Name
- 5-ACETYL-2-METHOXYPYRIDINE, 97%
- CAS No.
- 213193-32-9
- Chemical Name
- 5-ACETYL-2-METHOXYPYRIDINE, 97%
- Synonyms
- CAS:213193-32-9;5-Acetyl-2-methoxypyridine;5-Acetyl-2-methoxypyridine>1-(6-Methoxy-3-pyridinyl)ethanone;[5-ACETYL-2-METHOXYPYRIDINE, 97%];1-(6-Methoxy-pyridin-3-yl)-ethanone;1-(6-Methoxypyridin-3-yl)ethan-1-one;Ethanone, 1-(6-methoxy-3-pyridinyl)-;Ethanone, 1-(6-methoxy-3-pyridinyl)- (9CI);5-ACETYL-2-METHOXYPYRIDINE, 97% ISO 9001:2015 REACH
- CBNumber
- CB3973064
- Molecular Formula
- C8H9NO2
- Formula Weight
- 151.16
- MOL File
- 213193-32-9.mol
5-ACETYL-2-METHOXYPYRIDINE, 97% Property
- Melting point:
- 53-57 °C (lit.)
- Boiling point:
- 269.5±20.0 °C(Predicted)
- Density
- 1.093±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 1.60±0.10(Predicted)
- form
- Powder or Crystalline Powder
- color
- White to yellow
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 597767
- Product name
- 5-Acetyl-2-methoxypyridine
- Purity
- 97%
- Packaging
- 5g
- Price
- $84.48
- Updated
- 2025/07/31
- Product number
- 597767
- Product name
- 5-Acetyl-2-methoxypyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $38
- Updated
- 2023/06/20
- Product number
- A2797
- Product name
- 5-Acetyl-2-methoxypyridine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $38
- Updated
- 2025/07/31
- Product number
- A189020
- Product name
- 5-Acetyl-2-methoxypyridine
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- A189020
- Product name
- 5-Acetyl-2-methoxypyridine
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
5-ACETYL-2-METHOXYPYRIDINE, 97% Chemical Properties,Usage,Production
Uses
5-Acetyl-2-methoxypyridine is a useful synthesis intermediate.
Synthesis
858600-08-5
75-16-1
213193-32-9
Step 2: Amide (10.4 g, 53 mmol) was dissolved in tetrahydrofuran (THF, 100 mL) and the solution was cooled to 0°C. Methylmagnesium bromide (3M ether solution, 26.5 mL) was added slowly and dropwise at 0 °C. After the dropwise addition was completed, the reaction mixture was kept at 0°C and continued to be stirred for 1 hour. Subsequently, the reaction was quenched slowly with 1 M hydrochloric acid (aqueous solution). The mixture was extracted with ethyl acetate (EtOAc) and the organic layers were combined. The organic layer was washed with saturated brine and dried with anhydrous magnesium sulfate (MgSO4). After filtration to remove the drying agent, the filtrate was concentrated under reduced pressure to give 7.8 g of 5-acetyl-2-methoxypyridine in the form of a colorless solid in 97% yield.
References
[1] Patent: WO2009/5646, 2009, A2. Location in patent: Page/Page column 167
[2] Patent: WO2015/48507, 2015, A1. Location in patent: Paragraph 0169
[3] Tetrahedron, 2014, vol. 70, # 40, p. 7207 - 7220
5-ACETYL-2-METHOXYPYRIDINE, 97% Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-ACETYL-2-METHOXYPYRIDINE, 97% manufacturers
- Product
- 5-ACETYL-2-METHOXYPYRIDINE, 97% 213193-32-9
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2018-12-14