ChemicalBook > CAS DataBase List > Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI)

Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI)

Product Name: Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI)
CAS No.: 87674-21-3
Chemical Name: Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI)
Synonyms: 4-Acetyl-3-fluoropyridine;3-Fluoro-4-acetylpyridine;1-(3-Fluoro-4-pyridinyl)ethanone;1-(3-fluoropyridin-4-yl)ethan-1-one;Ethanone, 1-(3-fluoro-4-pyridinyl)-;Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI);Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) ISO 9001：2015 REACH
CBNumber: CB41052860
Molecular Formula: C7H6FNO
Formula Weight: 139.13
MOL File: 87674-21-3.mol

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Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) Property

Boiling point:: 199℃
Density: 1.175
Flash point:: 74℃
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 1.10±0.18(Predicted)
Appearance: Colorless to light yellow Liquid
InChI: InChI=1S/C7H6FNO/c1-5(10)6-2-3-9-4-7(6)8/h2-4H,1H3
InChIKey: PPULDLJGJZUOBS-UHFFFAOYSA-N
SMILES: C(=O)(C1C=CN=CC=1F)C

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F596315
Product name: 1-(3-Fluoropyridin-4-yl)ethanone
Packaging: 25mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: PC201340
Product name: 1-(3-Fluoropyridin-4-yl)ethanone
Purity: 98%
Packaging: 250mg
Price: $111
Updated: 2021/12/16

AK Scientific

Product number: W9003
Product name: 1-(3-Fluoropyridin-4-yl)ethanone
Packaging: 250mg
Price: $157
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0353949
Product name: 1-(3-FLUOROPYRIDIN-4-YL)ETHANONE
Purity: 95.00%
Packaging: 250MG
Price: $257.25
Updated: 2021/12/16

Apolloscientific

Product number: PC201340
Product name: 1-(3-Fluoropyridin-4-yl)ethanone
Purity: 98%
Packaging: 1g
Price: $275
Updated: 2021/12/16

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Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

1187669-49-3

75-16-1

87674-21-3

Step 2: Synthesis of 1-(3-fluoropyridin-4-yl)ethanone To a stirred solution of 3-fluoro-N-methoxy-N-methylpyridine-4-carboxamide (1.2 g, 6.5 mmol) in tetrahydrofuran (THF) (15 mL) was slowly added methylmagnesium bromide (2M solution in THF, 16 mL, 32 mmol) at 0 °C. After addition, the reaction mixture was brought to room temperature and stirring was continued for 2 hours. Upon completion of the reaction, the reaction was quenched with saturated ammonium chloride (NH4Cl) solution and subsequently extracted with ethyl acetate (EtOAc). The organic layers were combined, washed sequentially with water and saturated saline, dried over anhydrous sodium sulfate (Na2SO4), and concentrated under reduced pressure to afford 0.650 g (92% yield) of the target product 1-(3-fluoropyridin-4-yl)ethanone as a colorless oil. Mass spectrum (MS): 140.1 [M+H]+.

References

[1] Patent: US2017/291894, 2017, A1. Location in patent: Paragraph 0486-0488
[2] Journal of Medicinal Chemistry, 2010, vol. 53, # 2, p. 787 - 797
[3] Patent: WO2009/114552, 2009, A1. Location in patent: Page/Page column 167

Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) Preparation Products And Raw materials

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Preparation Products

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View Lastest Price from Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) 87674-21-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-26

87674-21-3, Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI)Related Search:

Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI)

1-(3-Fluoro-4-pyridinyl)ethanone

3-Fluoro-4-acetylpyridine

4-Acetyl-3-fluoropyridine

Ethanone, 1-(3-fluoro-4-pyridinyl)-

1-(3-fluoropyridin-4-yl)ethan-1-one

Ethanone, 1-(3-fluoro-4-pyridinyl)- (9CI) ISO 9001：2015 REACH

87674-21-3

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