ChemicalBook > CAS DataBase List > 2,3-DIMETHYL-4-METHOXYBENZOIC ACID

2,3-DIMETHYL-4-METHOXYBENZOIC ACID

Product Name
2,3-DIMETHYL-4-METHOXYBENZOIC ACID
CAS No.
5628-61-5
Chemical Name
2,3-DIMETHYL-4-METHOXYBENZOIC ACID
Synonyms
RARECHEM AL BE 0657;2,3-DIMETHYL-4-METHOXYBENZOIC ACID;4-Methoxy-2,3-diMethylbenzoic acid;Benzoic acid, 4-Methoxy-2,3-diMethyl-
CBNumber
CB4147972
Molecular Formula
C10H12O3
Formula Weight
180.2
MOL File
Mol file
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2,3-DIMETHYL-4-METHOXYBENZOIC ACID Property

storage temp. 
Sealed in dry,Room Temperature
Appearance
Off-white to light yellow Solid
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Safety

HazardClass 
IRRITANT
HS Code 
2918290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

SynQuest Laboratories
Product number
2721-1-15
Product name
2,3-Dimethyl-4-methoxybenzoic acid
Purity
98%
Packaging
1g
Price
$66
Updated
2021/12/16
Apolloscientific
Product number
OR47850
Product name
2,3-Dimethyl-4-methoxybenzoicacid
Packaging
1g
Price
$73
Updated
2021/12/16
ChemScene
Product number
CS-M2517
Product name
Benzoicacid,4-methoxy-2,3-dimethyl-
Packaging
100mg
Price
$85
Updated
2021/12/16
ChemScene
Product number
CS-M2517
Product name
Benzoicacid,4-methoxy-2,3-dimethyl-
Packaging
250mg
Price
$142
Updated
2021/12/16
Matrix Scientific
Product number
056852
Product name
2,3-Dimethyl-4-methoxybenzoic acid
Purity
98%
Packaging
1g
Price
$210
Updated
2021/12/16
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2,3-DIMETHYL-4-METHOXYBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

38998-17-3

5628-61-5

General procedure for the synthesis of 4-methoxy-2,3-dimethylbenzoic acid from 4-methoxy-2,3-dimethylbenzaldehyde: 60.0 g of 4-methoxy-2,3-dimethylbenzaldehyde was dissolved in 1.20 L of dimethyl sulfoxide. Subsequently, a solution prepared by dissolving 131.5 g of sodium dihydrogen phosphate and 132.2 g of sodium chlorite in 480 mL of water was added dropwise, during which the reaction temperature was controlled not to exceed 40 °C. After addition, the reaction mixture was continued to be stirred at room temperature for 2 hours. Upon completion of the reaction, the suspension was diluted with 2.0 L of water, the precipitate was collected by filtration, washed with water and dried under vacuum at 100 °C to afford 65.0 g of the target product 4-methoxy-2,3-dimethylbenzoic acid as a colorless solid with a melting point of 214 °C (MS: 181.2 [MH+]).

References

[1] Patent: US2011/60050, 2011, A1. Location in patent: Page/Page column 4
[2] Patent: US2011/224302, 2011, A1. Location in patent: Page/Page column 10; 15
[3] Bioorganic Chemistry, 1996, vol. 24, # 4, p. 386 - 400
[4] Patent: EP1666473, 2006, A1. Location in patent: Page/Page column 41

2,3-DIMETHYL-4-METHOXYBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2,3-DIMETHYL-4-METHOXYBENZOIC ACID Suppliers

China 19 France 1 Germany 1 India 1 United States 4 Global 26
Synthonix Inc
Tel
--
Fax
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Email
info@synthonix.com
Country
United States
ProdList
6872
Advantage
58
SynQuest Laboratories, Inc.
Tel
--
Fax
--
Email
info@synquestlabs.com
Country
United States
ProdList
6871
Advantage
62
Matrix Scientific
Tel
--
Fax
--
Email
sales@matrixscientific.com
Country
United States
ProdList
6632
Advantage
80
Trans World Chemicals, Inc.
Tel
--
Fax
--
Email
transworldchems@aol.com
Country
United States
ProdList
1591
Advantage
59

5628-61-5, 2,3-DIMETHYL-4-METHOXYBENZOIC ACIDRelated Search:

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  • 2,3-DIMETHYL-4-METHOXYBENZOIC ACID
  • RARECHEM AL BE 0657
  • 4-Methoxy-2,3-diMethylbenzoic acid
  • Benzoic acid, 4-Methoxy-2,3-diMethyl-
  • 5628-61-5