5-Bromoquinoline

Product Name: 5-Bromoquinoline
CAS No.: 4964-71-0
Chemical Name: 5-Bromoquinoline
Synonyms: 5-BromoquinoL;5-BROMOQUINOLINE;5-bronoquinoline;5-bromooquinoline;RARECHEM AK ML 0010;Quinoline, 5-bromo-;5-Bromoquinoline >5-Bromoquinoline,97%;5-Bromoquinoline 97%;5-Bromoquinoline,>98%
CBNumber: CB4149284
Molecular Formula: C9H6BrN
Formula Weight: 208.05
MOL File: 4964-71-0.mol

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5-Bromoquinoline Property

Melting point:: 43-48 °C
Boiling point:: 105-107°C 1mm
Density: 1.5617 (rough estimate)
refractive index: 1.6641 (estimate)
Flash point:: 105-107°C/1mm
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: powder to crystal
pka: 3.88±0.12(Predicted)
color: White to Light yellow to Green
BRN: 115148
InChI: InChI=1S/C9H6BrN/c10-8-4-1-5-9-7(8)3-2-6-11-9/h1-6H
InChIKey: CHODTZCXWXCALP-UHFFFAOYSA-N
SMILES: N1C2C(=C(Br)C=CC=2)C=CC=1
CAS DataBase Reference: 4964-71-0(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 36/37/38-20/21/22-22
Safety Statements: 26-36
WGK Germany: 3
Hazard Note: Irritant
HS Code: 29334900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 714429
Product name: 5-Bromoquinoline
Purity: 97%
Packaging: 5g
Price: $178
Updated: 2025/07/31

TCI Chemical

Product number: B3078
Product name: 5-Bromoquinoline
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $50
Updated: 2025/07/31

TRC

Product number: B695903
Product name: 5-Bromoquinoline
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B695903
Product name: 5-Bromoquinoline
Packaging: 100mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB16134
Product name: 5-Bromoquinoline
Packaging: 5G
Price: $50
Updated: 2021/12/16

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5-Bromoquinoline Chemical Properties,Usage,Production

Chemical Properties

White solid

Uses

5-Bromoquinoline is a biochemical reagent that can be used as a biological material or organic compound for life science related research.

Preparation

5-Bromoquinoline can be prepared by the reaction of quinoline with dichloromethane and NBS.

Synthesis

611-34-7

4964-71-0

General procedure for the synthesis of 5-bromoquinoline from 5-aminoquinoline: 1. dissolve quinolin-5-amine (3.37 g, 23.38 mmol) in 9 mL of water and 11 mL of hydrogen bromide (48% aqueous solution), and the resulting solution is cooled to 0°C. 2. a solution of sodium nitrite (1.94 g, 28.12 mmol) dissolved in 9 mL of water was added slowly and dropwise. 3. the reaction mixture was stirred at room temperature for 5 minutes. 4. The above solution was added slowly dropwise to a pre-prepared solution of copper (I) bromide (4.02 g, 28.02 mmol dissolved in 23 mL of 48% aqueous hydrogen bromide). 5. The reaction mixture was stirred at 75°C for 2 hours. 6. Upon completion of the reaction, the reaction mixture was alkalized with sodium hydroxide solution. 7. The reaction mixture was extracted twice with ethyl acetate and the organic phases were combined. 8. The organic phase was washed sequentially with water and brine, and then dried over anhydrous sodium sulfate. 9. The desiccant was removed by filtration and the solvent was evaporated under reduced pressure to give 2.98 g (61% yield) of the target product 5-bromoquinoline. Product characterization data: 1H NMR (CDCl3) δ ppm: 7.44-7.63 (m, 2H), 7.84 (d, J = 7.42 Hz, 1H), 8.10 (d, J = 8.24 Hz, 1H), 8.56 (d, J = 8.51 Hz, 1H), 8.94 (br.s., 1H). HPLC/MS (9 min) retention time 5.68 min. Mass spectral data: m/z 208 (M), 210 (M+2).

References

[1] Bioorganic and medicinal chemistry, 2002, vol. 10, # 8, p. 2611 - 2623
[2] Patent: EP2394998, 2011, A1. Location in patent: Page/Page column 16
[3] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 5, p. 1472 - 1476
[4] Journal of Labelled Compounds and Radiopharmaceuticals, 1994, vol. 34, # 10, p. 905 - 913
[5] Patent: US2003/96826, 2003, A1

5-Bromoquinoline Preparation Products And Raw materials

Raw materials

Preparation Products

Quinoline-5-boronic acid

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5-Bromoquinoline Suppliers

Americas 1 Austria 1 Canada 1 China 231 Europe 2 Germany 8 India 34 Japan 5 Russia 1 Switzerland 3 The Netherlands 1 Ukraine 2 United Kingdom 18 United States 38 Global 346

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View Lastest Price from 5-Bromoquinoline manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 5-Bromoquinoline 4964-71-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 2000tons
Release date: 2025-04-09

Henan Aochuang Chemical Co.,Ltd.

Product: 5-Bromoquinoline 4964-71-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-09-29

R&D Scientific Inc.

Product: 5-Bromoquinoline 4964-71-0
Price: US $1990.00/Kg
Min. Order: 1Kg
Purity: 98
Supply Ability: 500 Kg
Release date: 2024-04-01

4964-71-0, 5-BromoquinolineRelated Search:

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5-Bromoquinoline ISO 9001：2015 REACH

4964-71-0

Halogenated

Organohalides

Haloquinolines

Quinolines

Boronic Acid

Heterocyclic Compounds

Quinoline Derivertives

Quinoline

Halides

Heterocycles