3-AMINO-4-BROMO-1H-INDAZOLE
- Product Name
- 3-AMINO-4-BROMO-1H-INDAZOLE
- CAS No.
- 914311-50-5
- Chemical Name
- 3-AMINO-4-BROMO-1H-INDAZOLE
- Synonyms
- 4-Bromo-1H-indazol-3-amine;4-Bromo-1H-indazol-4-amine;4-bromo-2H-indazol-3-amine;3-AMINO-4-BROMO-1H-INDAZOLE;4-BroMo-1H-indazol-3-ylaMine;1H-Indazol-3-aMine, 4-broMo-
- CBNumber
- CB41558706
- Molecular Formula
- C7H6BrN3
- Formula Weight
- 212.05
- MOL File
- 914311-50-5.mol
3-AMINO-4-BROMO-1H-INDAZOLE Property
- Melting point:
- 142-144℃
- Boiling point:
- 431.3±25.0 °C(Predicted)
- Density
- 1.867±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- Slightly soluble.
- form
- Crystalline Powder
- pka
- 13.68±0.40(Predicted)
- color
- Off-white to brown to gray
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- FB139563
- Product name
- 4-Bromo-1H-indazol-3-amine
- Packaging
- 500mg
- Price
- $95
- Updated
- 2021/12/16
- Product number
- 054370
- Product name
- 4-Bromo-1H-indazol-3-amine
- Purity
- >95%
- Packaging
- 500mg
- Price
- $244
- Updated
- 2021/12/16
- Product number
- FB139563
- Product name
- 4-Bromo-1H-indazol-3-amine
- Packaging
- 5G
- Price
- $569
- Updated
- 2021/12/16
- Product number
- 4H30-9-03
- Product name
- 3-Amino-4-bromo-1H-indazole
- Packaging
- 1g
- Price
- $80
- Updated
- 2021/12/16
- Product number
- HCH0005441
- Product name
- 4-BROMO-1H-INDAZOL-3-AMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $832.18
- Updated
- 2021/12/16
3-AMINO-4-BROMO-1H-INDAZOLE Chemical Properties,Usage,Production
Uses
Microwave heating of 2-halobenzaldehydes or 2-haloacetophenones with phenylhydrazines at 160°C for 10 min quantitatively yielded the arylhydrazones, which were further cyclized to give 1-aryl-1H-indazoles via CuI/diamine-catalyzed N-arylation under microwave heating (160°C, 10 min). Good to excellent yields were observed for 2-iodo, 2-bromo, and 2-chloro benzaldehydes or acetophenones.
Synthesis
A solution of 2-fluoro-6-bromobenzonitrile (22.0 mmol) and 98% hydrazine hydrate (90.0 mmol) in n-butanol (15 ml) was stirred at reflux for 7 hours. The mixture was cooled to room temperature. The resulting mixture was concentrated under reduced pressure to a volume of 5 ml. water was added to the resulting mixture. The solid product was precipitated. The precipitate was filtered. Wash the precipitate with water. Dry the precipitate. The precipitate was purified by crystallization from methanol to give 4-bromo-1H-indazol-3-amine.
3-AMINO-4-BROMO-1H-INDAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
3-AMINO-4-BROMO-1H-INDAZOLE Suppliers
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View Lastest Price from 3-AMINO-4-BROMO-1H-INDAZOLE manufacturers
- Product
- 3-AMINO-4-BROMO-1H-INDAZOLE 914311-50-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 20 tons
- Release date
- 2019-09-10