3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER

Product Name: 3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER
CAS No.: 121912-29-6
Chemical Name: 3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER
Synonyms: Ethyl 1-(4-pyridinyl)-4-piperidinecarboxylate;Ethyl 1-(4-pyridinyl)piperidine-4-carboxylate;Ethyl 1-(pyridin-4-yl)piperidine-4-carboxylate;1-pyridin-4-yl-4-piperidinecarboxylic acid ethyl ester;4-Piperidinecarboxylic acid, 1-(4-pyridinyl)-, ethyl ester;3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER
CBNumber: CB4164285
Molecular Formula: C13H18N2O2
Formula Weight: 234.29
MOL File: 121912-29-6.mol

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3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER Property

Boiling point:: 356.4±32.0 °C(Predicted)
Density: 1.120±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 10.88±0.10(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

AK Scientific

Product number: 6672AH
Product name: Ethyl1-(pyridin-4-yl)piperidine-4-carboxylate
Packaging: 1g
Price: $587
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0290429
Product name: ETHYL-3,4,5,6-TETRAHYDRO-2H-[1,4]BIPYRIDINYL-4-CARBOXYLATE
Purity: 98.00%
Packaging: 25G
Price: $2009.7
Updated: 2021/12/16

Ambeed

Product number: A257521
Product name: Ethyl1-(pyridin-4-yl)piperidine-4-carboxylate
Purity: 97%
Packaging: 100mg
Price: $22
Updated: 2021/12/16

J&W Pharmlab

Product number: 60R0142
Product name: 3,4,5,6-tetrahydro-2H-[1,4'']bipyridinyl-4-carboxylicacidethylester
Purity: 97%
Packaging: 100mg
Price: $68
Updated: 2021/12/16

J&W Pharmlab

Product number: 60R0142
Product name: 3,4,5,6-tetrahydro-2H-[1,4'']bipyridinyl-4-carboxylicacidethylester
Purity: 97%
Packaging: 250mg
Price: $78
Updated: 2021/12/16

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3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER Chemical Properties,Usage,Production

Synthesis

64-17-5

93913-86-1

121912-29-6

Example 2 Difluorotriacetate of [1-(pyridin-4-yl)piperidin-4-yl]methyl 2-[amino(imino)methyl]-1,2,3,4-tetrahydroisoquinoline-7-carboxylic acid; Step 1 Synthesis of ethyl 1-(pyridin-4-yl)piperidin-4- carboxylate; To a 1-(pyridin-4-yl)piperidin-4-carboxylic acid (20.0 g, 97.0 mmol) ethanol (480 mL) suspension of thionyl chloride (7.1 mL, 97.0 mmol) was added dropwise and the mixture was stirred at 50°C overnight. After completion of the reaction, the solvent was removed by evaporation under reduced pressure and the resulting residue was diluted with dichloromethane, washed sequentially with 1N aqueous sodium hydroxide and saturated aqueous ammonium chloride, the organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to afford ethyl 1-(pyridin-4-yl)piperidine-4-carboxylate, which did not require further purification. Yield: 21.0 g (89.7 mmol, 93%). MS (ESI, m/z): 235 [M + H]+. 1H-NMR (CDCl3) δ: 1.26 (t, 3H), 1.72-1.86 (m, 2H), 1.97-2.05 (m, 2H), 2.49-2.58 (m, 1H), 2.93-3.02 (m , 2H), 3.82-3.02 (m, 2H). , 2H), 3.82 (dt, 2H), 4.16 (q, 2H), 6.66 (dd, 2H), 8.25 (dd, 2H).

References

[1] Patent: EP2311810, 2011, A1. Location in patent: Page/Page column 21
[2] Tetrahedron, 1988, vol. 44, # 23, p. 7095 - 7108

3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER Suppliers

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121912-29-6, 3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTERRelated Search:

BUTTPARK 63\09-20 3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER BUTTPARK 92\04-55 BUTTPARK 63\09-91 4-AMINO-3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER BUTTPARK 91\18-76 BUTTPARK 93\04-25

3,4,5,6-TETRAHYDRO-2H-[1,4']BIPYRIDINYL-4-CARBOXYLIC ACID ETHYL ESTER

Ethyl 1-(4-pyridinyl)piperidine-4-carboxylate

4-Piperidinecarboxylic acid, 1-(4-pyridinyl)-, ethyl ester

Ethyl 1-(pyridin-4-yl)piperidine-4-carboxylate

1-pyridin-4-yl-4-piperidinecarboxylic acid ethyl ester

Ethyl 1-(4-pyridinyl)-4-piperidinecarboxylate

121912-29-6