ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate

Product Name: ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate
CAS No.: 577711-94-5
Chemical Name: ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate
Synonyms: methyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate;ethyl 6-broMo-1H-pyrrolo[2;ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate;6-Bromo-1H-pyrrolo [2,3-b]pyridine-2-carboxylic acid ethyl ester;1H-Pyrrolo[2,3-b]pyridine-2-carboxylic acid, 6-broMo-, ethyl ester
CBNumber: CB41856198
Molecular Formula: C10H9BrN2O2
Formula Weight: 269.09
MOL File: 577711-94-5.mol

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ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate Property

Density: 1.624±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 10.96±0.40(Predicted)
Appearance: white solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: E900810
Product name: Ethyl6-bromo-1h-pyrrolo[2,3-b]pyridine-2-carboxylate
Packaging: 25mg
Price: $150
Updated: 2021/12/16

AK Scientific

Product number: W7109
Product name: Ethyl6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate
Packaging: 1g
Price: $1400
Updated: 2021/12/16

Matrix Scientific

Product number: 070398
Product name: Ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate
Purity: 96%
Packaging: 500mg
Price: $719
Updated: 2021/12/16

Matrix Scientific

Product number: 070398
Product name: Ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate
Purity: 96%
Packaging: 1g
Price: $1000
Updated: 2021/12/16

Matrix Scientific

Product number: 070398
Product name: Ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate
Purity: 96%
Packaging: 5g
Price: $3327
Updated: 2021/12/16

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ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate Chemical Properties,Usage,Production

Synthesis

577711-92-3

577711-94-5

General procedure for the synthesis of ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate from ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate: 18.4 g (0.05 mol) of ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate 1-tert-butyl ester 2-ethyl ester was dissolved in 165 mL of dichloromethane and cooled to 0°C. 38.0 mL of trifluoroacetic acid was added slowly over 5 minutes. The cooling bath was removed and the reaction mixture was stirred at room temperature for 2 hours. Subsequently, the reaction mixture was poured into 500 mL of saturated aqueous sodium bicarbonate solution. The aqueous phase was extracted three times with 150 mL of dichloromethane and the organic phase was combined. The organic phase was washed with 200 mL of brine, dried over anhydrous magnesium sulfate and filtered. The solvent was evaporated and the residue was dried under high vacuum to give 12.0 g (95.5%) of the target product, ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate, as a colorless solid.ISP-MS: m/e = 269.2 ([M+H]+).

References

[1] Patent: WO2005/849, 2005, A1. Location in patent: Page/Page column 62
[2] Patent: US2003/207888, 2003, A1

ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate Suppliers

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View Lastest Price from ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate manufacturers

Career Henan Chemical Co

Product: ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate 577711-94-5
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-12

577711-94-5, ethyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylateRelated Search:

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1H-Pyrrolo[2,3-b]pyridine-2-carboxylic acid, 6-broMo-, ethyl ester

methyl 6-bromo-1H-pyrrolo[2,3-b]pyridine-2-carboxylate

6-Bromo-1H-pyrrolo [2,3-b]pyridine-2-carboxylic acid ethyl ester

577711-94-5

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