ChemicalBook > CAS DataBase List > 2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE

2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE

Product Name
2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE
CAS No.
18206-06-9
Chemical Name
2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE
Synonyms
2,6-Dimethylisonicotinaldehyde;6-diMethylpyridine-4-carbaldehyde;2,6-Dimethylpyridin-4-carbaldehyde;2,6-DiMethylpyridine-4-carbaldehyde;2,6-diMethyl-4-Pyridinecarboxaldehyde;2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE;4-Pyridinecarboxaldehyde, 2,6-dimethyl-
CBNumber
CB4187954
Molecular Formula
C8H9NO
Formula Weight
135.16
MOL File
18206-06-9.mol
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2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Property

Melting point:
8℃
Boiling point:
218℃
Density 
1.065
refractive index 
1.5282
Flash point:
91℃
storage temp. 
2-8°C, stored under nitrogen
pka
4.69±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
D461803
Product name
2,6-Dimethylisonicotinaldehyde
Packaging
500mg
Price
$350
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
D13895
Product name
2,6-Dimethylpyridine-4-carbaldehyde
Purity
98%
Packaging
1g
Price
$190
Updated
2021/12/16
Apolloscientific
Product number
OR946275
Product name
2,6-Dimethylisonicotinaldehyde
Purity
95%
Packaging
250mg
Price
$200
Updated
2021/12/16
AK Scientific
Product number
9540AA
Product name
2,6-Dimethylisonicotinaldehyde
Packaging
1g
Price
$304
Updated
2021/12/16
Apolloscientific
Product number
OR946275
Product name
2,6-Dimethylisonicotinaldehyde
Purity
95%
Packaging
1g
Price
$420
Updated
2021/12/16
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2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Chemical Properties,Usage,Production

Synthesis

18088-01-2

18206-06-9

The general procedure for the synthesis of 2,6-dimethylpyridine-4-carbaldehyde from 2,6-dimethyl-4-hydroxymethylpyridine was as follows: 2,6-dimethyl-4-hydroxymethylpyridine (1.00 g, 7.30 mmol) was dissolved in acetonitrile (20 mL), and 1,2-benzoyl-3(1H)-keto-1-hydroxyl-1-oxo (IBX) (2.00 g, 7.30 mmol). The reaction mixture was heated to reflux for 6 hours. After completion of the reaction, the solid was removed by filtration and washed with acetonitrile. The filtrate was concentrated under reduced pressure to give 2,6-dimethylpyridine-4-carbaldehyde as a brown liquid. Yield: 0.81 g (82%).

References

[1] Patent: US9238640, 2016, B2. Location in patent: Page/Page column 134; 135
[2] Patent: US2013/281399, 2013, A1. Location in patent: Paragraph 0732; .0735; 0740; 0760; 0770; 0752
[3] Chemical Communications, 2015, vol. 51, # 61, p. 12258 - 12261

2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Suppliers

J & K SCIENTIFIC LTD.
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18210857532; 18210857532
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Suzhou Nuoouman Biological Technology Co., Ltd.
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View Lastest Price from 2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
2,6-Dimethylpyridine-4-carboxaldehyde 18206-06-9
Price
US $0.10/KG
Min. Order
1KG
Purity
99.0%
Supply Ability
1000 tons
Release date
2019-12-27