2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE
- Product Name
- 2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE
- CAS No.
- 18206-06-9
- Chemical Name
- 2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE
- Synonyms
- 2,6-Dimethylisonicotinaldehyde;6-diMethylpyridine-4-carbaldehyde;2,6-Dimethylpyridin-4-carbaldehyde;2,6-DiMethylpyridine-4-carbaldehyde;2,6-diMethyl-4-Pyridinecarboxaldehyde;2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE;4-Pyridinecarboxaldehyde, 2,6-dimethyl-
- CBNumber
- CB4187954
- Molecular Formula
- C8H9NO
- Formula Weight
- 135.16
- MOL File
- 18206-06-9.mol
2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Property
- Melting point:
- 8℃
- Boiling point:
- 218℃
- Density
- 1.065
- refractive index
- 1.5282
- Flash point:
- 91℃
- storage temp.
- 2-8°C, stored under nitrogen
- pka
- 4.69±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D461803
- Product name
- 2,6-Dimethylisonicotinaldehyde
- Packaging
- 500mg
- Price
- $350
- Updated
- 2021/12/16
- Product number
- D13895
- Product name
- 2,6-Dimethylpyridine-4-carbaldehyde
- Purity
- 98%
- Packaging
- 1g
- Price
- $190
- Updated
- 2021/12/16
- Product number
- OR946275
- Product name
- 2,6-Dimethylisonicotinaldehyde
- Purity
- 95%
- Packaging
- 250mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 9540AA
- Product name
- 2,6-Dimethylisonicotinaldehyde
- Packaging
- 1g
- Price
- $304
- Updated
- 2021/12/16
- Product number
- OR946275
- Product name
- 2,6-Dimethylisonicotinaldehyde
- Purity
- 95%
- Packaging
- 1g
- Price
- $420
- Updated
- 2021/12/16
2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Chemical Properties,Usage,Production
Synthesis
18088-01-2
18206-06-9
The general procedure for the synthesis of 2,6-dimethylpyridine-4-carbaldehyde from 2,6-dimethyl-4-hydroxymethylpyridine was as follows: 2,6-dimethyl-4-hydroxymethylpyridine (1.00 g, 7.30 mmol) was dissolved in acetonitrile (20 mL), and 1,2-benzoyl-3(1H)-keto-1-hydroxyl-1-oxo (IBX) (2.00 g, 7.30 mmol). The reaction mixture was heated to reflux for 6 hours. After completion of the reaction, the solid was removed by filtration and washed with acetonitrile. The filtrate was concentrated under reduced pressure to give 2,6-dimethylpyridine-4-carbaldehyde as a brown liquid. Yield: 0.81 g (82%).
References
[1] Patent: US9238640, 2016, B2. Location in patent: Page/Page column 134; 135
[2] Patent: US2013/281399, 2013, A1. Location in patent: Paragraph 0732; .0735; 0740; 0760; 0770; 0752
[3] Chemical Communications, 2015, vol. 51, # 61, p. 12258 - 12261
2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,6-DIMETHYLPYRIDINE-4-CARBOXALDEHYDE manufacturers
- Product
- 2,6-Dimethylpyridine-4-carboxaldehyde 18206-06-9
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2019-12-27