5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE
- Product Name
- 5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE
- CAS No.
- 583-42-6
- Chemical Name
- 5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE
- Synonyms
- SALOR-INT L202959-1EA;5-fluoro-2-mercaptobenzimidazole;2-Mercapto-5-fluorobenzimidazole;5-Fluoro-1H-benzo[d]imidazole-2(3H);5-fluoro-1,3-dihydrobenzimidazole-2-thione;5-Fluoro-1H-benzo[d]imidazole-2(3H)-thione;5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE;5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOLE-2-THIONE;2H-Benzimidazole-2-thione, 5-fluoro-1,3-dihydro-;2H-Benzimidazole-2-thione,5-fluoro-1,3-dihydro-(9CI)
- CBNumber
- CB4194002
- Molecular Formula
- C7H5FN2S
- Formula Weight
- 168.19
- MOL File
- 583-42-6.mol
5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE Property
- Melting point:
- 280 °C(Solv: ethanol (64-17-5))
- Boiling point:
- 261.8±42.0 °C(Predicted)
- Density
- 1.49±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 9?+-.0.30(Predicted)
- Appearance
- White to light yellow Solid
Safety
- HS Code
- 2933299090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- F593488
- Product name
- 6-fluoro-1H-benzimidazole-2-thiol
- Packaging
- 10mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- F593488
- Product name
- 6-fluoro-1H-benzimidazole-2-thiol
- Packaging
- 50mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- 7H67-3-0A
- Product name
- 5-Fluoro-1H-benzo[d]imidazole-2(3H)-thione
- Purity
- 95.0%
- Packaging
- 1g
- Price
- $111
- Updated
- 2021/12/16
- Product number
- 8640AB
- Product name
- 5-Fluoro-1H-benzo[d]imidazole-2(3H)-thione
- Packaging
- 1g
- Price
- $157
- Updated
- 2021/12/16
- Product number
- 036062
- Product name
- 6-Fluoro-1H-benzimidazole-2-thiol
- Packaging
- 500mg
- Price
- $189
- Updated
- 2021/12/16
5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE Chemical Properties,Usage,Production
Synthesis
75-15-0
367-31-7
583-42-6
The reaction was carried out with 4-fluoro-1,2-benzenediamine (10 g, 79.3 mmol) and carbon disulfide (70 ml, 1164 mmol) in methanol (100 ml) with stirring at room temperature for 86 hours and 50 minutes. After completion of the reaction, the reaction mixture was concentrated and the residue was suspended with hexane. The resulting precipitate was collected by filtration and washed with hexane to afford 5-fluoro-1H-benzo[d]imidazole-2(3H)-thione (13.1 g, yield: 98.2%), the product was a brown solid.1H NMR (400 MHz, DMSO-d6) δ ppm: 6.90-6.99 (2H, m), 7.06-7.13 (1H, m). 12.58 (1H, s), 12.61 (1H, s).
References
[1] Patent: US2007/10542, 2007, A1. Location in patent: Page/Page column 76
5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-FLUORO-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-THIONE manufacturers
- Product
- 5-fluoro-1,3-dihydrobenzimidazole-2-thione 583-42-6
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 97.0%
- Supply Ability
- 100 tons
- Release date
- 2022-01-14