3,5-DIMETHYL-4-IODOPHENOL
- Product Name
- 3,5-DIMETHYL-4-IODOPHENOL
- CAS No.
- 80826-86-4
- Chemical Name
- 3,5-DIMETHYL-4-IODOPHENOL
- Synonyms
- 4-IODO-3,5-XYLENOL;3,5-Xylenol, 4-iodo-;3,5-DIMETHYL-4-IODOPHENOL;5-Hydroxy-2-iodo-m-xylene;4-IODO-3,5-DIMETHYL-PHENOL;Phenol, 4-iodo-3,5-dimethyl-;4-Iodo-3,5-dimethyl-phenol, CAS 80826-86-4;5-Hydroxy-2-iodo-m-xylene, 4-Iodo-3,5-xylenol
- CBNumber
- CB4201821
- Molecular Formula
- C8H9IO
- Formula Weight
- 248.06
- MOL File
- 80826-86-4.mol
3,5-DIMETHYL-4-IODOPHENOL Property
- Melting point:
- 129 °C
- Boiling point:
- 293.0±28.0 °C(Predicted)
- Density
- 1.740±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- crystalline needles
- pka
- 9.59±0.23(Predicted)
- color
- Faint brown
- Sensitive
- Light Sensitive
- CAS DataBase Reference
- 80826-86-4(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- D476898
- Product name
- 3,5-Dimethyl-4-iodophenol
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 2701-H-X1
- Product name
- 3,5-Dimethyl-4-iodophenol
- Packaging
- 5G
- Price
- $69
- Updated
- 2021/12/16
- Product number
- 2701-H-X1
- Product name
- 3,5-Dimethyl-4-iodophenol
- Packaging
- 250mg
- Price
- $16
- Updated
- 2021/12/16
- Product number
- 2701-H-X1
- Product name
- 3,5-Dimethyl-4-iodophenol
- Packaging
- 1g
- Price
- $23
- Updated
- 2021/12/16
- Product number
- X5963
- Product name
- 3,5-Dimethyl-4-Iodophenol
- Packaging
- 25g
- Price
- $318
- Updated
- 2021/12/16
3,5-DIMETHYL-4-IODOPHENOL Chemical Properties,Usage,Production
Chemical Properties
Light yellow crystalline
Synthesis
108-68-9
80826-86-4
The general procedure for the synthesis of 3,5-dimethyl-4-iodophenol from 3,5-dimethylphenol was as follows: 395 mL of 36% hydrochloric acid was slowly added to a 1 L methanol solution containing 59.1 g (484 mmol) of 3,5-dimethylphenol, which was cooled intermittently to maintain the reaction temperature between 20°C and 30°C. The reaction was then carried out over a period of 5 min by dropwise addition of 54.3 g (327 mmol) of potassium iodide and 33.5 g (157 mmol) of potassium iodate to 500 mL of water. Subsequently, a solution prepared from 54.3 g (327 mmol) of potassium iodide and 33.5 g (157 mmol) of potassium iodate dissolved in 500 mL of water was added dropwise to the reaction system over a period of 5 min. It was observed that the solution gradually turned red and became turbid, followed by the formation of a tan precipitate. The reaction mixture was stirred continuously for 20 h at room temperature before being cooled in an ice bath, the precipitate was collected by filtration and washed with a pre-cooled 2:1 (v:v) water/methanol mixture. The resulting brown solid was purified by several recrystallizations from hot methanol and water, resulting in 36.4 g (15% yield) of white acicular crystals with a melting point of 131-132°C, which were identified as 3,5-dimethyl-4-iodophenol. The structure of the compound was confirmed by 1H NMR (δ, CDCl3) 8.03 (br s, 1H), 6.52 (s, 2H), and 2.35 (s, 6H) as well as by mass spectra (m/e) 248 (M+, 100%), 121, 91, and 77.
References
[1] Catalysis Communications, 2017, vol. 93, p. 1 - 4
[2] Bioorganic and Medicinal Chemistry Letters, 2001, vol. 11, # 3, p. 323 - 325
[3] Synthesis, 2001, # 11, p. 1639 - 1644
[4] Journal of Chemical Research, 2004, # 4, p. 294 - 295
[5] Organic Letters, 2015, vol. 17, # 12, p. 2886 - 2889
3,5-DIMETHYL-4-IODOPHENOL Preparation Products And Raw materials
Raw materials
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View Lastest Price from 3,5-DIMETHYL-4-IODOPHENOL manufacturers
- Product
- 3,5-DIMETHYL-4-IODOPHENOL 80826-86-4
- Price
- US $5.00-2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10000kg
- Release date
- 2024-08-22
- Product
- 3,5-DIMETHYL-4-IODOPHENOL 80826-86-4
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- g/kg/T
- Release date
- 2019-12-18