Ethyl thiazole-2-carboxylate
- Product Name
- Ethyl thiazole-2-carboxylate
- CAS No.
- 14527-42-5
- Chemical Name
- Ethyl thiazole-2-carboxylate
- Synonyms
- 2-(Ethoxycarbonyl)thiazole;Ethyl thiazole-2-carboxylate;2-Thiazolecarboxylic acid, ethyl ester
- CBNumber
- CB42130541
- Molecular Formula
- C6H7NO2S
- Formula Weight
- 157.19
- MOL File
- 14527-42-5.mol
Ethyl thiazole-2-carboxylate Property
- storage temp.
- 2-8°C
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2934100090
N-Bromosuccinimide Price
- Product number
- E938815
- Product name
- EthylThiazole-2-Carboxylate
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- P000126541
- Product name
- Ethyl thiazole-2-carboxylate
- Purity
- 97%
- Packaging
- 1g
- Price
- $53
- Updated
- 2021/12/16
- Product number
- P000126541
- Product name
- Ethyl thiazole-2-carboxylate
- Purity
- 97%
- Packaging
- 100mg
- Price
- $13
- Updated
- 2021/12/16
- Product number
- P000126541
- Product name
- Ethyl thiazole-2-carboxylate
- Purity
- 97%
- Packaging
- 250mg
- Price
- $20
- Updated
- 2021/12/16
- Product number
- OR964945
- Product name
- Ethylthiazole-2-carboxylate
- Purity
- 95%
- Packaging
- 250mg
- Price
- $110
- Updated
- 2021/12/16
Ethyl thiazole-2-carboxylate Chemical Properties,Usage,Production
Synthesis
79265-30-8
541-41-3
14527-42-5
General procedure for the preparation of ethyl 2-thiazolecarboxylate: a solution of 2-(trimethylsilyl)thiazole (135 g, 858.1 mmol) in toluene (1350 mL) was slowly added to a solution of ethyl chloroformate (98.4 mL, 1.03 mol) in toluene (1350 mL) over a period of 15 minutes. The reaction mixture was stirred continuously at 22°C for 2 hours. Subsequently, the reaction solution was poured into 25% (wt/wt) aqueous sodium carbonate solution (5 L) and stirring was continued for 30 min. The organic layer was separated and the aqueous layer was subjected to secondary extraction with dichloromethane (2 x 1 L). All organic layers were combined and the solvents were evaporated under reduced pressure to give ethyl 2-thiazolecarboxylate (134 g, 99% yield).ES/MS m/z 158 (M + 1)+.
References
[1] Patent: WO2008/36579, 2008, A1. Location in patent: Page/Page column 26
[2] Patent: US2009/176779, 2009, A1. Location in patent: Page/Page column 13
[3] Patent: US2003/229079, 2003, A1. Location in patent: Page 77
Ethyl thiazole-2-carboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Ethyl thiazole-2-carboxylate manufacturers
- Product
- Ethyl thiazole-2-carboxylate 14527-42-5
- Price
- US $0.00/kg
- Min. Order
- 25kg
- Purity
- 98%
- Supply Ability
- Inquiry
- Release date
- 2023-07-12
- Product
- Ethyl thiazole-2-carboxylate 14527-42-5
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 97.5%
- Supply Ability
- 100 tons
- Release date
- 2022-01-26