ChemicalBook > CAS DataBase List > 5-AMINO-2-FLUOROBENZONITRILE

5-AMINO-2-FLUOROBENZONITRILE

Product Name: 5-AMINO-2-FLUOROBENZONITRILE
CAS No.: 77123-60-5
Chemical Name: 5-AMINO-2-FLUOROBENZONITRILE
Synonyms: 3-ETHYNYL-4-FLUOROANILINE;2-FLUORO-5-AMINOBENZONITRILE;3-Ethynyl-4-fluorobenzenamine;Benzenamine, 3-ethynyl-4-fluoro-;5-AMINO-2-FLUOROBENZONITRILE 95%min;3-Ethynyl-4-fluoroaniline - [E47969];Benzenamine, 3-ethynyl-4-fluoro- (9CI);5-AMINO-2-FLUOROBENZONITRILE ISO 9001：2015 REACH
CBNumber: CB4217806
Molecular Formula: C8H6FN
Formula Weight: 135.14
MOL File: 77123-60-5.mol

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5-AMINO-2-FLUOROBENZONITRILE Property

Melting point:: 92-96 °C(lit.)
Boiling point:: 247℃
Density: 1.16
Flash point:: 114℃
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 3.73±0.10(Predicted)
Appearance: Light yellow to yellow Liquid

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Safety

Hazard Codes: Xi
Risk Statements: 38-41
Safety Statements: 26-39
WGK Germany: 3
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: E932653
Product name: 3-Ethynyl-4-fluoroaniline
Packaging: 250mg
Price: $165
Updated: 2021/12/16

Matrix Scientific

Product number: 075879
Product name: 3-Ethynyl-4-fluoroaniline
Purity: 95+%
Packaging: 500mg
Price: $175
Updated: 2021/12/16

Activate Scientific

Product number: AS34493
Product name: 3-Ethynyl-4-fluoroaniline
Purity: 97+%
Packaging: 1g
Price: $191
Updated: 2021/12/16

Matrix Scientific

Product number: 075879
Product name: 3-Ethynyl-4-fluoroaniline
Purity: 95+%
Packaging: 250mg
Price: $339
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0352017
Product name: 3-ETHYNYL-4-FLUOROANILINE
Purity: 95.00%
Packaging: 5MG
Price: $498.56
Updated: 2021/12/16

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5-AMINO-2-FLUOROBENZONITRILE Chemical Properties,Usage,Production

Synthesis

77123-63-8

77123-60-5

Step 3d. Synthesis of 3-ethynyl-4-fluoroaniline (Compound 0605): Compound 0604 (1.49 g) obtained above was dissolved in 20 mL of methanol, 100 mg of potassium hydroxide was added and the reaction was stirred at room temperature overnight. Upon completion of the reaction, the reaction solution was concentrated, diluted to neutral with water and subsequently extracted with ether. The organic phases were combined, dried with anhydrous magnesium sulfate, filtered and concentrated to give 3-alkynyl-4-fluoroaniline 0605 (1.49 g, 85% yield) as a brown oil. The molecular weight of the product was 136 [M + 1]+ by LCMS. The obtained product can be directly used in the subsequent reaction without further purification.

References

[1] Patent: US2009/111772, 2009, A1. Location in patent: Page/Page column 77
[2] Patent: WO2008/33747, 2008, A2. Location in patent: Page/Page column 139
[3] Patent: US2009/76022, 2009, A1. Location in patent: Page/Page column 78
[4] Journal of Organic Chemistry, 1981, vol. 46, # 11, p. 2280 - 2286
[5] Patent: JP5680638, 2015, B2. Location in patent: Paragraph 0347-0348

5-AMINO-2-FLUOROBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-AMINO-2-FLUOROBENZONITRILE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-Ethynyl-4-fluoroaniline 77123-60-5
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-17

Career Henan Chemical Co

Product: 5-AMINO-2-FLUOROBENZONITRILE 77123-60-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-08

77123-60-5, 5-AMINO-2-FLUOROBENZONITRILERelated Search:

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Benzenamine, 3-ethynyl-4-fluoro- (9CI)

3-ETHYNYL-4-FLUOROANILINE

3-Ethynyl-4-fluorobenzenamine

Benzenamine, 3-ethynyl-4-fluoro-

5-AMINO-2-FLUOROBENZONITRILE ISO 9001：2015 REACH

5-AMINO-2-FLUOROBENZONITRILE 95%min

3-Ethynyl-4-fluoroaniline - [E47969]

77123-60-5