6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE

Product Name: 6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE
CAS No.: 54325-28-9
Chemical Name: 6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE
Synonyms: 6-O-Trityl-α-D-glucopyranose;6-O-TRITYL-ALPHA-D-GLUCOPYRANOSE;6-O-(Triphenylmethyl)-α-D-glucopyranose;6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE;α-D-Glucopyranose, 6-O-(triphenylmethyl)-;(2S,3R,4S,5S,6R)-6-((Trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol
CBNumber: CB42451905
Molecular Formula: C25H26O6
Formula Weight: 422.47
MOL File: 54325-28-9.mol

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6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE Property

Boiling point:: 595.6±50.0 °C(Predicted)
Density: 1.332±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 12.09±0.70(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CRB0005076
Product name: 6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE
Purity: 95.00%
Packaging: 5MG
Price: $503.93
Updated: 2021/12/16

Ambeed

Product number: A476635
Product name: (2S,3R,4S,5S,6R)-6-((Trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol
Purity: 95+%
Packaging: 100mg
Price: $62
Updated: 2021/12/16

Ambeed

Product number: A476635
Product name: (2S,3R,4S,5S,6R)-6-((Trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol
Purity: 95+%
Packaging: 250mg
Price: $93
Updated: 2021/12/16

Ambeed

Product number: A476635
Product name: (2S,3R,4S,5S,6R)-6-((Trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol
Purity: 95+%
Packaging: 1g
Price: $229
Updated: 2021/12/16

Crysdot

Product number: CD70000961
Product name: (2S,3R,4S,5S,6R)-6-((Trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol
Purity: 95+%
Packaging: 250mg
Price: $230
Updated: 2021/12/16

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6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE Chemical Properties,Usage,Production

Synthesis

50-99-7

76-83-5

54325-28-9

The general procedure for the synthesis of (2S,3R,4S,5S,6R)-6-((triphenylmethoxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol from D-anhydrous glucose and triphenylmethyl chloride was as follows: D-anhydrous glucose (5 g; 0.0277 mol) was suspended in pyridine (50 mL), followed by addition of triphenylmethyl chloride. The reaction mixture was stirred at 80 °C for about 4 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) using dichloromethane: methanol (85:15) as the unfolding agent. Upon completion of the reaction, the reaction was quenched with water (100 mL) and extracted with dichloromethane (150 mL x 2). The organic layers were combined, washed with saturated aqueous sodium bicarbonate and dried over anhydrous sodium sulfate. The solvent was subsequently removed using a rotary evaporator. The target product (2S,3R,4S,5S,6R)-6-((triphenylmethoxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol (10.3 g; 88% yield) was finally obtained by milling the crude product with a hexane:ether mixture (100 mL) to remove residual triphthaloyl chloride and pyridine. The structure of the product was confirmed by LC-MS and the molecular ion peak (M+) was observed to be 446 amu.

References

[1] Patent: WO2007/54977, 2007, A2. Location in patent: Page/Page column 21
[2] Patent: KR101595939, 2016, B1. Location in patent: Paragraph 0102-0103

6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE Suppliers

China 20 India 1 United States 1 Global 22

Shanghai Changyan Chem & Tech Co., Ltd.

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Energy Chemical

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Shanghai Sunway Pharmaceutical Technology Co.,Ltd.

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Beijing Qinling Pharmaceutical Co., Ltd.

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54325-28-9, 6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSERelated Search:

Methyl-6-O-trityl-2,3,4-tri-O-benzoyl-α-D-glucopyranoside Methyl-6-O-trityl-2,3,4-tri-O-benzyl-α-D-glucopyranoside 4-Nitrophenyl6-O-trityl-a-D-glucopyranoside 6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE BENZYL 2,3,4-TRI-O-BENZYL-6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSIDE 1,6,6'-TRI-O-TRITYLSUCROSE PENTAACETATE 4-NITROPHENYL 2,3,4-TRI-O-ACETYL-6-O-TRITYL-ALPHA-D-GLUCOPYRANOSIDE 1',6,6'-Tri-O-tritylsucrose METHYL-6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSIDE alpha-d-Glucopyranoside, methyl 6-O-(triphenylmethyl)-, triacetate 1,2,3,4-TETRA-O-ACETYL-6-O-(TRIPHENYLMETHYL)-BETA-D-GLUCOPYRANOSE

6-O-TRIPHENYLMETHYL-ALPHA-D-GLUCOPYRANOSE

6-O-TRITYL-ALPHA-D-GLUCOPYRANOSE

(2S,3R,4S,5S,6R)-6-((Trityloxy)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol

α-D-Glucopyranose, 6-O-(triphenylmethyl)-

6-O-Trityl-α-D-glucopyranose

6-O-(Triphenylmethyl)-α-D-glucopyranose

54325-28-9