2-METHOXY-6-METHYLBENZONITRILE

Product Name: 2-METHOXY-6-METHYLBENZONITRILE
CAS No.: 53005-44-0
Chemical Name: 2-METHOXY-6-METHYLBENZONITRILE
Synonyms: 2-methoxy-6-methylbenzenitrile;2-METHOXY-6-METHYLBENZONITRILE;2-Methoxy-6-methay benzonitrile;Benzonitrile, 2-methoxy-6-methyl-
CBNumber: CB42454951
Molecular Formula: C9H9NO
Formula Weight: 147.17
MOL File: 53005-44-0.mol

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2-METHOXY-6-METHYLBENZONITRILE Property

Boiling point:: 70-74℃ (0.4 Torr)
Density: 1.06±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: Light yellow to light brown Solid

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M329860
Product name: 2-Methoxy-6-methylbenzonitrile
Packaging: 1g
Price: $105
Updated: 2021/12/16

AK Scientific

Product number: W6749
Product name: 2-Methoxy-6-methaybenzonitrile
Packaging: 1g
Price: $117
Updated: 2021/12/16

Matrix Scientific

Product number: 074687
Product name: 2-Methoxy-6-methylbenzonitrile
Purity: 95+%
Packaging: 5g
Price: $899
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0167387
Product name: 2-METHOXY-6-METHAY BENZONITRILE
Purity: 95.00%
Packaging: 1G
Price: $958.65
Updated: 2021/12/16

Matrix Scientific

Product number: 074687
Product name: 2-Methoxy-6-methylbenzonitrile
Purity: 95+%
Packaging: 10g
Price: $1286
Updated: 2021/12/16

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2-METHOXY-6-METHYLBENZONITRILE Chemical Properties,Usage,Production

Synthesis

1030446-72-0

53005-44-0

The general procedure for the synthesis of 2-methoxy-6-methylbenzonitrile, using the compound (CAS: 1030446-72-0) as starting material, was as follows: to a solution of intermediate 144 (7.50 g, 45.41 mmol) in dichloromethane (55 mL) was added N,N'-dicarbonyldiimidazole (8.09 g, 49.95 mmol), and the reaction was stirred for 15 h at room temperature. The reaction was stirred for 15 hours at room temperature. After completion of the reaction, the reaction mixture was quenched with water, the organic phase was extracted with dichloromethane, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 2-methoxy-6-methylbenzonitrile as a brown solid (5.0 g, 75% yield). The product was characterized by nuclear magnetic resonance hydrogen spectroscopy (1H NMR, 400 MHz, CDCl3) with the following chemical shifts (δ ppm): 7.41 (t, J = 8.1 Hz, 1H), 6.87 (d, J = 7.7 Hz, 1H), 6.78 (d, J = 8.5 Hz, 1H), 3.91 (s, 3H), 2.50 (s, 3H).

References

[1] Patent: WO2012/151525, 2012, A1. Location in patent: Page/Page column 132
[2] Patent: US2012/289496, 2012, A1. Location in patent: Page/Page column 115

2-METHOXY-6-METHYLBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-METHOXY-6-METHYLBENZONITRILE Suppliers

China 47 India 2 Switzerland 1 United States 7 Global 57

Beijing Ouhe Technology Co., Ltd

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Xinyanhe Pharmatech Co.,Ltd

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View Lastest Price from 2-METHOXY-6-METHYLBENZONITRILE manufacturers

Career Henan Chemica Co

Product: 2-METHOXY-6-METHYLBENZONITRILE 53005-44-0
Price: US $3.07/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1000KG
Release date: 2020-10-27

53005-44-0, 2-METHOXY-6-METHYLBENZONITRILERelated Search:

3,4,5-TRIMETHOXY-2'-CYANO-DI-HYDROCINNAMALDEHYDE DIMETHYLACETAL 1,4-DIACETOXY-2,3-DICYANOBENZENE 1,2-DICYANO-3-(4-NITRILEPHENYL)BENZENE 1,4-DIBUTOXY-2,3-DICHLORO-5,6-DICYANOBENZENE BAY 59-3074 2-BENZYLOXY-6-NITROMETHYLCYANOBENZENE 1 4-DIBUTOXY-2 3-NAPHTHALENEDI- 3-(2-METHOXYCARBONYL PHENOXY)-PHTHALONITRILE 2-METHOXY-6-(TRIFLUOROMETHYL)BENZONITRILE 3-(4-METHYLPHENOXY)-1,2-BENZENEDICARBONITRILE 2,4-DIMETHOXY-6-METHYLBENZONITRILE 3,4,5-TRIMETHOXY-D9-2'-CYANO-DI-HYDROCINNAMALDEHYDE DIMETHYLACETAL 3 6-DIBUTOXY-1 2-BENZENEDICARBONITRILE 2-FORMYL-6-METHOXYBENZONITRILE 3-PHENOXYPHTHALONITRILE 98 2-METHOXY-6-METHYLBENZONITRILE

2-METHOXY-6-METHYLBENZONITRILE

2-Methoxy-6-methay benzonitrile

Benzonitrile, 2-methoxy-6-methyl-

2-methoxy-6-methylbenzenitrile

53005-44-0