ChemicalBook > CAS DataBase List > 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE

1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE

Product Name: 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE
CAS No.: 63057-72-7
Chemical Name: 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE
Synonyms: 2-(Benzyloxy)-5-bromoanisole;4-Bromo-2-methoxy-1-phenylmethoxybenzene;Benzene, 4-bromo-2-methoxy-1-(phenylmethoxy)-
CBNumber: CB42456692
Molecular Formula: C14H13BrO2
Formula Weight: 293.16
MOL File: 63057-72-7.mol

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1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE Property

storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Solid
color: White to Off-White

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S813834
Product name: 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $30.7
Updated: 2025/07/31

Sigma-Aldrich

Product number: S813834
Product name: 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE
Purity: Aldrich
Packaging: 5mg
Price: $29.8
Updated: 2024/03/01

TRC

Product number: B291493
Product name: 1-(Benzyloxy)-4-bromo-2-methoxybenzene
Packaging: 100mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: V6997
Product name: 1-(Benzyloxy)-4-bromo-2-methoxybenzene
Packaging: 1g
Price: $103
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0109876
Product name: 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE
Purity: 95.00%
Packaging: 5MG
Price: $503.25
Updated: 2021/12/16

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1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE Chemical Properties,Usage,Production

Synthesis

7368-78-7

100-39-0

63057-72-7

Step 1: Synthesis of 1-(benzyloxy)-4-bromo-2-methoxybenzene (2). Potassium carbonate (K2CO3, 30.5 g, 221 mmol) and benzyl bromide (18.9 g, 171 mmol) were added to a solution of N,N-dimethylformamide (DMF, 150 mL) containing 4-bromo-2-methoxyphenol (15 g, 73.8 mmol). The reaction mixture was stirred at 100 °C for 2 hours. Upon completion of the reaction, the reaction was quenched by the addition of water and the organic layer was extracted with ethyl acetate (EtOAc). The organic phases were combined and concentrated. The crude product was purified by column chromatography to afford the target compound 2 (17.6 g, 86% yield).

References

[1] Patent: US2005/43300, 2005, A1. Location in patent: Page/Page column 39
[2] Bioorganic and Medicinal Chemistry Letters, 2015, vol. 25, # 14, p. 2793 - 2799
[3] Journal of Organic Chemistry, 2002, vol. 67, # 10, p. 3425 - 3436
[4] Patent: WO2018/64557, 2018, A1. Location in patent: Paragraph 0444; 0445; 0446; 0447
[5] Patent: US2006/264473, 2006, A1. Location in patent: Page/Page column 5

1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE Suppliers

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63057-72-7, 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENERelated Search:

2-Bromo-4-methoxy-5-(benzyloxy)benzaldehyde (5-BENZYLOXY-2-BROMO-4-METHOXY)PHENYLACETONE 1-(BENZYLOXY)-4-BROMO-2,5-DIMETHOXYBENZENE RARECHEM AN KB 2339 BENZENE, 1,2-DIBROMO-4,5-BIS(PHENYLMETHOXY)- 5-BENZYLOXY-2-BROMO-4-METHOXYBENZYL ALCOHOL RARECHEM AN KC 2330 RARECHEM AN KD 2349 5-BENZYLOXY-2-BROMO-4-METHOXYCINNAMIC ACID 1-(BENZYLOXY)-4-BROMO-2-METHOXYBENZENE RARECHEM AN KA 2334 5-BENZYLOXY-2-BROMO-4-METHOXYBENZALDEHYDE OXIME 5-BENZYLOXY-2-BROMO-4-METHOXYPHENYLACETONE OXIME 2-Bromo-4-methoxy-5-benzyloxybenzoic acid 5-(BENZYLOXY)-2-BROMO-4-METHOXYPHENOL

Benzene, 4-bromo-2-methoxy-1-(phenylmethoxy)-

4-Bromo-2-methoxy-1-phenylmethoxybenzene

2-(Benzyloxy)-5-bromoanisole

63057-72-7