ChemicalBook > CAS DataBase List > 5-BROMOISOQUINOLIN-1-AMINE

5-BROMOISOQUINOLIN-1-AMINE

Product Name: 5-BROMOISOQUINOLIN-1-AMINE
CAS No.: 852570-80-0
Chemical Name: 5-BROMOISOQUINOLIN-1-AMINE
Synonyms: 5-Bromo-1-isoquinolinamine;5-BROMOISOQUINOLIN-1-AMINE;1-Amino-5-bromoisoquinoline;1-Isoquinolinamine, 5-bromo-;5-bromoisoquinolin-1-ylamine;1-Amino-5-bromoisoquinoline 95%;5-BROMOISOQUINOLIN-1-AMINE ISO 9001：2015 REACH;5-Bromoisoquinolin-1-amine, 1-Amino-5-bromo-2-azanaphthalene
CBNumber: CB42459370
Molecular Formula: C9H7BrN2
Formula Weight: 223.07
MOL File: 852570-80-0.mol

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5-BROMOISOQUINOLIN-1-AMINE Property

Boiling point:: 380.7±27.0 °C(Predicted)
Density: 1.649
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 6.50±0.43(Predicted)
form: solid
color: White to faint orange

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Safety

Risk Statements: 41
Safety Statements: 26-39
HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B292410
Product name: 5-Bromoisoquinolin-1-amine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR17656
Product name: 1-Amino-5-bromoisoquinoline
Purity: 95%
Packaging: 50mg
Price: $58
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-9-V5
Product name: 1-Amino-5-bromoisoquinoline
Purity: 95%
Packaging: 50mg
Price: $64
Updated: 2021/12/16

Apolloscientific

Product number: OR17656
Product name: 1-Amino-5-bromoisoquinoline
Purity: 95%
Packaging: 250mg
Price: $116
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-9-V5
Product name: 1-Amino-5-bromoisoquinoline
Purity: 95%
Packaging: 250mg
Price: $128
Updated: 2021/12/16

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5-BROMOISOQUINOLIN-1-AMINE Chemical Properties,Usage,Production

Synthesis

34551-41-2

852570-80-0

Step 3: To a 500 mL round bottom flask purged with nitrogen and maintained in an inert atmosphere under nitrogen protection was added a mixture of 5-bromo-1-chloroisoquinoline (17.5 g, 72.16 mmol, 1.00 eq.), AcNH2 (85.8 g, 1.45 mol, 20.15 eq.) and potassium carbonate (49.0 g, 354.53 mmol, 4.91 equivalent) in a mixture. The reaction mixture was stirred at 180 °C for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature and slowly poured into 2000 mL of water with stirring. The precipitated solid was collected by filtration to give 12.0 g (75% yield) of 5-bromoisoquinolin-1-amine as a brown solid.

References

[1] Patent: WO2005/49576, 2005, A1. Location in patent: Page/Page column 29
[2] Patent: WO2005/49577, 2005, A1. Location in patent: Page/Page column 32-33
[3] Patent: WO2016/201052, 2016, A1. Location in patent: Page/Page column 272
[4] Patent: WO2008/86014, 2008, A2. Location in patent: Page/Page column 60

5-BROMOISOQUINOLIN-1-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-BROMOISOQUINOLIN-1-AMINE manufacturers

Career Henan Chemica Co

Product: 5-BROMOISOQUINOLIN-1-AMINE 852570-80-0
Price: US $1.80/KG
Min. Order: 1g
Purity: 96%-99%
Supply Ability: 1kg/10kg/100kg
Release date: 2020-11-07

852570-80-0, 5-BROMOISOQUINOLIN-1-AMINERelated Search:

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5-BROMOISOQUINOLIN-1-AMINE

1-Amino-5-bromoisoquinoline

1-Amino-5-bromoisoquinoline 95%

5-Bromo-1-isoquinolinamine

5-Bromoisoquinolin-1-amine, 1-Amino-5-bromo-2-azanaphthalene

5-bromoisoquinolin-1-ylamine

1-Isoquinolinamine, 5-bromo-

5-BROMOISOQUINOLIN-1-AMINE ISO 9001：2015 REACH

852570-80-0

Building Blocks

Isoquinoline