ChemicalBook > CAS DataBase List > 3-Bromo-N-methyl-N-boc-propylamine

3-Bromo-N-methyl-N-boc-propylamine

Product Name
3-Bromo-N-methyl-N-boc-propylamine
CAS No.
828272-19-1
Chemical Name
3-Bromo-N-methyl-N-boc-propylamine
Synonyms
tert-Butyl (3-bromopropyl)(methyl)carbamate;-N-boc-propyL;3-Bromo-N-methyL;N-Boc-N-methyl-3-bromopropylamine;3-Bromo-N-methyl-N-boc-propylamine;tert-butyl N-(3-bromopropyl)-N-methylcarbamate;(3-Bromo-propyl)-methyl-carbamic acid tert-butyl ester;Carbamic acid, (3-bromopropyl)methyl-, 1,1-dimethylethyl ester;N-(3-BroMopropyl)-N-MethylcarbaMic Acid 1,1-DiMethylethyl Ester;Carbamic acid, N-(3-bromopropyl)-N-methyl-, 1,1-dimethylethyl ester
CBNumber
CB42486949
Molecular Formula
C9H18BrNO2
Formula Weight
252.15
MOL File
828272-19-1.mol
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3-Bromo-N-methyl-N-boc-propylamine Property

Boiling point:
268.4±19.0 °C(Predicted)
Density 
1.254±0.06 g/cm3(Predicted)
solubility 
Chloroform, Dichloromethane, Ethyl Acetate
pka
-1.39±0.70(Predicted)
InChI
InChI=1S/C9H18BrNO2/c1-9(2,3)13-8(12)11(4)7-5-6-10/h5-7H2,1-4H3
InChIKey
PIUWBRCCWDAPFG-UHFFFAOYSA-N
SMILES
C(OC(C)(C)C)(=O)N(CCCBr)C
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P322Specific measures (see …on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P363Wash contaminated clothing before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
B685315
Product name
3-Bromo-N-methyl-N-boc-propylamine
Packaging
200mg
Price
$1320
Updated
2021/12/16
Activate Scientific
Product number
AS106701
Product name
N-Boc-N-methyl-3-bromopropylamine
Purity
97%
Packaging
1g
Price
$400
Updated
2021/12/16
AK Scientific
Product number
7673DG
Product name
3-Bromo-N-methyl-N-boc-propylamine
Packaging
500mg
Price
$700
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0104275
Product name
3-BROMO-N-METHYL-N-BOC-PROPYLAMINE
Purity
95.00%
Packaging
1G
Price
$769.65
Updated
2021/12/16
AK Scientific
Product number
7673DG
Product name
3-Bromo-N-methyl-N-boc-propylamine
Packaging
1g
Price
$870
Updated
2021/12/16
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3-Bromo-N-methyl-N-boc-propylamine Chemical Properties,Usage,Production

Synthesis

Into a 100 mL round-bottom flask were placed tert-butyl (3- hydroxypropyl)(methyl)carbamate (2.00 g, 10.60 mmol, 1.00 equiv), DCM (20.00 mL) and PPh3 (3.67 g, 13.80 mmol, 1.30 equiv). This was followed by addition of CBr4 (5.20 g, 13.80 mmol, 1.30 equiv) at 0 °C. The resulting solution was stirred for 1.5 h at 0 °C. The reaction mixture was quenched with H2O (50.00 mL), extracted with DCM (100 mL*2). The combined organic phase was washed with Na2CO3 (aq), brine and dried over anhydrous sodium sulfate. After filtration, the filtrate was concentrated under reduced pressure. The residue was purified by silica gel column with petroleum ether/ethyl acetate (93%/7%). This resulted in 2.6 g of 3-Bromo-N-methyl-N-boc-propylamine as light yellow oil.

3-Bromo-N-methyl-N-boc-propylamine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromo-N-methyl-N-boc-propylamine Suppliers

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View Lastest Price from 3-Bromo-N-methyl-N-boc-propylamine manufacturers

Huida Pharmaceutical Technology (Shanghai) Co., Ltd.
Product
3-Bromo-N-methyl-N-boc-propylamine 828272-19-1
Price
US $0.00-0.00/kg
Min. Order
0.1kg
Purity
98%
Supply Ability
100kg
Release date
2023-03-09

828272-19-1, 3-Bromo-N-methyl-N-boc-propylamineRelated Search:


  • 3-Bromo-N-methyl-N-boc-propylamine
  • N-(3-BroMopropyl)-N-MethylcarbaMic Acid 1,1-DiMethylethyl Ester
  • tert-butyl N-(3-bromopropyl)-N-methylcarbamate
  • tert-Butyl (3-bromopropyl)(methyl)carbamate
  • N-Boc-N-methyl-3-bromopropylamine
  • Carbamic acid, N-(3-bromopropyl)-N-methyl-, 1,1-dimethylethyl ester
  • (3-Bromo-propyl)-methyl-carbamic acid tert-butyl ester
  • -N-boc-propyL
  • 3-Bromo-N-methyL
  • Carbamic acid, (3-bromopropyl)methyl-, 1,1-dimethylethyl ester
  • 828272-19-1
  • Aliphatics
  • Amines
  • Miscellaneous Reagents