3-Bromo-N-methyl-N-boc-propylamine

Product Name: 3-Bromo-N-methyl-N-boc-propylamine
CAS No.: 828272-19-1
Chemical Name: 3-Bromo-N-methyl-N-boc-propylamine
Synonyms: tert-Butyl (3-bromopropyl)(methyl)carbamate;-N-boc-propyL;3-Bromo-N-methyL;N-Boc-N-methyl-3-bromopropylamine;3-Bromo-N-methyl-N-boc-propylamine;tert-butyl N-(3-bromopropyl)-N-methylcarbamate;(3-Bromo-propyl)-methyl-carbamic acid tert-butyl ester;Carbamic acid, (3-bromopropyl)methyl-, 1,1-dimethylethyl ester;N-(3-BroMopropyl)-N-MethylcarbaMic Acid 1,1-DiMethylethyl Ester;Carbamic acid, N-(3-bromopropyl)-N-methyl-, 1,1-dimethylethyl ester
CBNumber: CB42486949
Molecular Formula: C9H18BrNO2
Formula Weight: 252.15
MOL File: 828272-19-1.mol

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3-Bromo-N-methyl-N-boc-propylamine Property

Boiling point:: 268.4±19.0 °C(Predicted)
Density: 1.254±0.06 g/cm3(Predicted)
solubility: Chloroform, Dichloromethane, Ethyl Acetate
pka: -1.39±0.70(Predicted)
InChI: InChI=1S/C9H18BrNO2/c1-9(2,3)13-8(12)11(4)7-5-6-10/h5-7H2,1-4H3
InChIKey: PIUWBRCCWDAPFG-UHFFFAOYSA-N
SMILES: C(OC(C)(C)C)(=O)N(CCCBr)C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P322Specific measures (see …on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P363Wash contaminated clothing before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B685315
Product name: 3-Bromo-N-methyl-N-boc-propylamine
Packaging: 200mg
Price: $1320
Updated: 2021/12/16

Activate Scientific

Product number: AS106701
Product name: N-Boc-N-methyl-3-bromopropylamine
Purity: 97%
Packaging: 1g
Price: $400
Updated: 2021/12/16

AK Scientific

Product number: 7673DG
Product name: 3-Bromo-N-methyl-N-boc-propylamine
Packaging: 500mg
Price: $700
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0104275
Product name: 3-BROMO-N-METHYL-N-BOC-PROPYLAMINE
Purity: 95.00%
Packaging: 1G
Price: $769.65
Updated: 2021/12/16

AK Scientific

Product number: 7673DG
Product name: 3-Bromo-N-methyl-N-boc-propylamine
Packaging: 1g
Price: $870
Updated: 2021/12/16

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3-Bromo-N-methyl-N-boc-propylamine Chemical Properties,Usage,Production

Synthesis

Into a 100 mL round-bottom flask were placed tert-butyl (3- hydroxypropyl)(methyl)carbamate (2.00 g, 10.60 mmol, 1.00 equiv), DCM (20.00 mL) and PPh3 (3.67 g, 13.80 mmol, 1.30 equiv). This was followed by addition of CBr4 (5.20 g, 13.80 mmol, 1.30 equiv) at 0 °C. The resulting solution was stirred for 1.5 h at 0 °C. The reaction mixture was quenched with H2O (50.00 mL), extracted with DCM (100 mL*2). The combined organic phase was washed with Na2CO3 (aq), brine and dried over anhydrous sodium sulfate. After filtration, the filtrate was concentrated under reduced pressure. The residue was purified by silica gel column with petroleum ether/ethyl acetate (93%/7%). This resulted in 2.6 g of 3-Bromo-N-methyl-N-boc-propylamine as light yellow oil.

3-Bromo-N-methyl-N-boc-propylamine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromo-N-methyl-N-boc-propylamine Suppliers

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View Lastest Price from 3-Bromo-N-methyl-N-boc-propylamine manufacturers

Huida Pharmaceutical Technology (Shanghai) Co., Ltd.

Product: 3-Bromo-N-methyl-N-boc-propylamine 828272-19-1
Price: US $0.00-0.00/kg
Min. Order: 0.1kg
Purity: 98%
Supply Ability: 100kg
Release date: 2023-03-09

828272-19-1, 3-Bromo-N-methyl-N-boc-propylamineRelated Search:

3-Bromo-N-methyl-N-boc-propylamine

N-(3-BroMopropyl)-N-MethylcarbaMic Acid 1,1-DiMethylethyl Ester

tert-butyl N-(3-bromopropyl)-N-methylcarbamate

tert-Butyl (3-bromopropyl)(methyl)carbamate

N-Boc-N-methyl-3-bromopropylamine

Carbamic acid, N-(3-bromopropyl)-N-methyl-, 1,1-dimethylethyl ester

(3-Bromo-propyl)-methyl-carbamic acid tert-butyl ester

-N-boc-propyL

3-Bromo-N-methyL

Carbamic acid, (3-bromopropyl)methyl-, 1,1-dimethylethyl ester

828272-19-1

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