1-Bromo-4-ethoxy-2,3-difluorobenzene
- Product Name
- 1-Bromo-4-ethoxy-2,3-difluorobenzene
- CAS No.
- 156573-09-0
- Chemical Name
- 1-Bromo-4-ethoxy-2,3-difluorobenzene
- Synonyms
- B90001;4-Bromo-2,3-difluorophenetole >1-BROMO-4-ETHOXY-2,3-DIFLUOROBENZENE;2,3-Difluoro-4-bromophenylethyl ether;1-Bromo-4-ethoxyl-2,3-difulorobenzene;4-BroMo-2,3-difluorophenyl ethyl ether;Benzene, 1-bromo-4-ethoxy-2,3-difluoro-;5-broMo-1,2-difluoro-3-(MethoxyMethyl)benzene
- CBNumber
- CB4265438
- Molecular Formula
- C8H7BrF2O
- Formula Weight
- 237.04
- MOL File
- 156573-09-0.mol
1-Bromo-4-ethoxy-2,3-difluorobenzene Property
- Melting point:
- 31 °C
- Boiling point:
- 222.7±35.0 °C(Predicted)
- Density
- 1.533±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- solubility
- soluble in Methanol
- form
- powder to lump
- color
- White to Almost white
- InChIKey
- OJZVBJOHBGYINN-UHFFFAOYSA-N
Safety
- HS Code
- 2909309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B3884
- Product name
- 4-Bromo-2,3-difluorophenetole
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $58
- Updated
- 2025/07/31
- Product number
- B683160
- Product name
- 1-Bromo-4-ethoxy-2,3-difluorobenzene
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- J96869
- Product name
- 2,3-Difluoro-4-ethoxybromobenzene
- Packaging
- 1g
- Price
- $20
- Updated
- 2021/12/16
- Product number
- Y3181
- Product name
- 2,3-Difluoro-4-ethoxybromobenzene
- Packaging
- 1g
- Price
- $26
- Updated
- 2021/12/16
- Product number
- J96869
- Product name
- 2,3-Difluoro-4-ethoxybromobenzene
- Packaging
- 100g
- Price
- $362
- Updated
- 2021/12/16
1-Bromo-4-ethoxy-2,3-difluorobenzene Chemical Properties,Usage,Production
Chemical Properties
Off-white crystalline
Synthesis
74-96-4
144292-32-0
156573-09-0
To an aqueous sodium hydroxide solution (400 ml) of 4-bromo-2,3-difluorophenol (T-1) (195.0 g), ethidium bromide (196.2 g), and tetrabutylammonium bromide (TBAB) (24.2 g) was added sodium hydroxide (75.9 g), and the reaction was heated and stirred under nitrogen protection for 6 hr at 80 °C. After completion of the reaction, extraction was carried out with heptane and the organic layer was washed sequentially with water and saturated saline. Subsequently, the organic layer was dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give a black oily substance. The oily substance was purified by distillation to give 1-ethoxy-2,3-difluorobromobenzene (T-2) as a colorless oily liquid (230.0 g, yield: 97%).
References
[1] Patent: EP2484658, 2012, A1. Location in patent: Page/Page column 37
[2] Patent: JP5663957, 2015, B2. Location in patent: Paragraph 0137-0138; 0139
1-Bromo-4-ethoxy-2,3-difluorobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-Bromo-4-ethoxy-2,3-difluorobenzene manufacturers
- Product
- 1-Bromo-4-ethoxy-2,3-difluorobenzene 156573-09-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-10-24
- Product
- 1-Bromo-4-ethoxy-2,3-difluorobenzene 156573-09-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-18
- Product
- 1-bromo-4-ethoxy-2,3-difluorobenzene 156573-09-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 1000KG/month
- Release date
- 2021-11-04