ChemicalBook > CAS DataBase List > 1-Bromo-4-ethoxy-2,3-difluorobenzene

1-Bromo-4-ethoxy-2,3-difluorobenzene

Product Name
1-Bromo-4-ethoxy-2,3-difluorobenzene
CAS No.
156573-09-0
Chemical Name
1-Bromo-4-ethoxy-2,3-difluorobenzene
Synonyms
B90001;4-Bromo-2,3-difluorophenetole >1-BROMO-4-ETHOXY-2,3-DIFLUOROBENZENE;2,3-Difluoro-4-bromophenylethyl ether;1-Bromo-4-ethoxyl-2,3-difulorobenzene;4-BroMo-2,3-difluorophenyl ethyl ether;Benzene, 1-bromo-4-ethoxy-2,3-difluoro-;5-broMo-1,2-difluoro-3-(MethoxyMethyl)benzene
CBNumber
CB4265438
Molecular Formula
C8H7BrF2O
Formula Weight
237.04
MOL File
156573-09-0.mol
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1-Bromo-4-ethoxy-2,3-difluorobenzene Property

Melting point:
31 °C
Boiling point:
222.7±35.0 °C(Predicted)
Density 
1.533±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
solubility 
soluble in Methanol
form 
powder to lump
color 
White to Almost white
InChIKey
OJZVBJOHBGYINN-UHFFFAOYSA-N
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Safety

HS Code 
2909309090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B3884
Product name
4-Bromo-2,3-difluorophenetole
Purity
>98.0%(GC)
Packaging
5g
Price
$58
Updated
2025/07/31
TRC
Product number
B683160
Product name
1-Bromo-4-ethoxy-2,3-difluorobenzene
Packaging
100mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
J96869
Product name
2,3-Difluoro-4-ethoxybromobenzene
Packaging
1g
Price
$20
Updated
2021/12/16
AK Scientific
Product number
Y3181
Product name
2,3-Difluoro-4-ethoxybromobenzene
Packaging
1g
Price
$26
Updated
2021/12/16
AK Scientific
Product number
J96869
Product name
2,3-Difluoro-4-ethoxybromobenzene
Packaging
100g
Price
$362
Updated
2021/12/16
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1-Bromo-4-ethoxy-2,3-difluorobenzene Chemical Properties,Usage,Production

Chemical Properties

Off-white crystalline

Synthesis

74-96-4

144292-32-0

156573-09-0

To an aqueous sodium hydroxide solution (400 ml) of 4-bromo-2,3-difluorophenol (T-1) (195.0 g), ethidium bromide (196.2 g), and tetrabutylammonium bromide (TBAB) (24.2 g) was added sodium hydroxide (75.9 g), and the reaction was heated and stirred under nitrogen protection for 6 hr at 80 °C. After completion of the reaction, extraction was carried out with heptane and the organic layer was washed sequentially with water and saturated saline. Subsequently, the organic layer was dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give a black oily substance. The oily substance was purified by distillation to give 1-ethoxy-2,3-difluorobromobenzene (T-2) as a colorless oily liquid (230.0 g, yield: 97%).

References

[1] Patent: EP2484658, 2012, A1. Location in patent: Page/Page column 37
[2] Patent: JP5663957, 2015, B2. Location in patent: Paragraph 0137-0138; 0139

1-Bromo-4-ethoxy-2,3-difluorobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Bromo-4-ethoxy-2,3-difluorobenzene Suppliers

J & K SCIENTIFIC LTD.
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18210857532; 18210857532
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86-10-82849933
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jkinfo@jkchemical.com
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China
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Meryer (Shanghai) Chemical Technology Co., Ltd.
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4006356688 18621169109
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86-21-61259102
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China
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TCI (Shanghai) Development Co., Ltd.
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021-67121386
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021-67121385
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Sales-CN@TCIchemicals.com
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China
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Capot Chemical Co., Ltd
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+86 (0) 571 85 58 67 18
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JinYan Chemicals(ShangHai) Co.,Ltd.
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Tianjin heowns Biochemical Technology Co., Ltd.
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400 638 7771
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Xi'an Manareco New Materials Co., Ltd.
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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
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025-66113011 17798518460
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(1)02557626880
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View Lastest Price from 1-Bromo-4-ethoxy-2,3-difluorobenzene manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
1-Bromo-4-ethoxy-2,3-difluorobenzene 156573-09-0
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2024-10-24
Henan Aochuang Chemical Co.,Ltd.
Product
1-Bromo-4-ethoxy-2,3-difluorobenzene 156573-09-0
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-10-18
Shanghai Daken Advanced Materials Co.,Ltd
Product
1-bromo-4-ethoxy-2,3-difluorobenzene 156573-09-0
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
1000KG/month
Release date
2021-11-04

156573-09-0, 1-Bromo-4-ethoxy-2,3-difluorobenzeneRelated Search:


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