9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- Product Name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- CAS No.
- 618442-57-2
- Chemical Name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- Synonyms
- 3,6-Bis(4,4,5,5-tetramethyl-1,3,2;9-Phenyl-3,6-bis(4,4,5,5- tetraMethyl-1,3,2-dioxaborol;9-Phenyl-9H-carbazole-3,6-diboronic Acid Bis(pinacol) Ester;9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole;3,6-Bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9-phenylcarbazole;9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole;3,6-Bis(4,4,5,5-tetramethyl-1,3,2- dioxaborolan-2-yl)-9-phenyl-9H-carbazole;9-Phenyl-3,6-bis(4,4,5,5- tetraMethyl-1,3,2-dioxaborolan- 2-yl)-9H-carbazol;9H-Carbazole, 9-phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
- CBNumber
- CB42655325
- Molecular Formula
- C30H35B2NO4
- Formula Weight
- 495.23
- MOL File
- 618442-57-2.mol
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Property
- Melting point:
- 238.0 to 242.0 °C
- Boiling point:
- 587.8±43.0 °C(Predicted)
- Density
- 1.11±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder to crystal
- color
- White to Light yellow
Safety
- HS Code
- 2934.99.4400
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- P2350
- Product name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 200mg
- Price
- $50
- Updated
- 2025/07/31
- Product number
- P2350
- Product name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 1g
- Price
- $149
- Updated
- 2025/07/31
- Product number
- AK202330
- Product name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- Purity
- 97%
- Packaging
- 250mg
- Price
- $16
- Updated
- 2021/12/16
- Product number
- AK202330
- Product name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- Purity
- 97%
- Packaging
- 1g
- Price
- $39
- Updated
- 2021/12/16
- Product number
- 6971AL
- Product name
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
- Packaging
- 10g
- Price
- $319
- Updated
- 2021/12/16
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Chemical Properties,Usage,Production
Synthesis
73183-34-3
57103-20-5
618442-57-2
3,6-Dibromo-9-phenylcarbazole (0.075 mol) and pinacol ester of bisboronic acid (0.164 mol) were dissolved in 300 mL of dioxane and potassium acetate (0.375 mol) and tetrakis(triphenylphosphine)palladium (0.00075 mol) were added sequentially. The reaction mixture was heated to reflux for 5 hours. Upon completion of the reaction, the reaction was quenched with dichloromethane and water. The organic phase was separated and filtered through a silica gel funnel. Subsequently, the organic phase was concentrated under reduced pressure to remove the solvent. Finally, the resulting solid was purified by column chromatography to afford the target product 9-phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole (45% yield).
References
[1] Patent: CN106928237, 2017, A. Location in patent: Paragraph 0212; 0213; 0214
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole manufacturers
- Product
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole 618442-57-2
- Price
- US $2.20-8.80/kg
- Min. Order
- 1kg
- Purity
- 99%min
- Supply Ability
- 100kg
- Release date
- 2025-06-17
- Product
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole 618442-57-2
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-12
- Product
- 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole 618442-57-2
- Price
- US $15.00-250.00/g
- Min. Order
- 5g
- Purity
- 0.98
- Supply Ability
- 100kg
- Release date
- 2024-10-25