4-Chloro-N-Methoxy-N-MethylbutyraMide

Product Name: 4-Chloro-N-Methoxy-N-MethylbutyraMide
CAS No.: 64214-66-0
Chemical Name: 4-Chloro-N-Methoxy-N-MethylbutyraMide
Synonyms: 4- Chloro-N-methoxy-N-methyl butyl;N-Methyl-N-methoxy-4-chlorobutanamide;4-Chloro-N-methoxy-N-methylbutanamide;4-Chloro-N-Methoxy-N-MethylbutyraMide;N-methoxy-N-methyl-4-chloroprene amide;3-N-Methoxy-N-methyl-4-chlorobutyramide;Butanamide, 4-chloro-N-methoxy-N-methyl-;2- Chloro - N - Methoxy - N - Methylbutyramide
CBNumber: CB42657495
Molecular Formula: C6H12ClNO2
Formula Weight: 165.62
MOL File: 64214-66-0.mol

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4-Chloro-N-Methoxy-N-MethylbutyraMide Property

Boiling point:: 199.1±42.0 °C(Predicted)
Density: 1.106±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C381975
Product name: 4-Chloro-N-methoxy-N-methylbutanamide
Packaging: 500mg
Price: $155
Updated: 2021/12/16

ChemScene

Product number: CS-0046358
Product name: 4-Chloro-N-methoxy-N-methylbutanamide
Packaging: 250mg
Price: $51
Updated: 2021/12/16

ChemScene

Product number: CS-0046358
Product name: 4-Chloro-N-methoxy-N-methylbutanamide
Packaging: 1g
Price: $101
Updated: 2021/12/16

ChemScene

Product number: CS-0046358
Product name: 4-Chloro-N-methoxy-N-methylbutanamide
Packaging: 5g
Price: $302
Updated: 2021/12/16

AK Scientific

Product number: 2564AQ
Product name: 4-CHLORO-N-METHOXY-N-METHYLBUTANAMIDE
Packaging: 5g
Price: $425.6
Updated: 2021/12/16

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4-Chloro-N-Methoxy-N-MethylbutyraMide Chemical Properties,Usage,Production

Synthesis

6638-79-5

4635-59-0

64214-66-0

To a solution of 4-chlorobutanoyl chloride (50.0 g, 355 mmol) and N-methoxy-N-methylamine hydrochloride (34.6 g, 355 mmol) in dichloromethane (DCM, 709 mL) was slowly added triethylamine (TEA, 109 mL, 780 mmol) at 0 °C, the addition process lasted 30 min. The reaction mixture was continued to be stirred at 0 °C for 3 hours. Upon completion of the reaction, it was quenched by the addition of water (250 mL). The organic layer was separated, washed with saturated brine, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to afford 4-chloro-N-methoxy-N-methylbutyramide (55.0 g, 94% yield) as a yellow oil, which could be used for the subsequent reaction without further purification.1H-NMR (CDCl3, Varian, 400 MHz) δ: 2.12 ( 2H, quintuple peak, J = 6.4 Hz), 2.63 (2H, triple peak, J = 7.2 Hz), 3.19 (3H, single peak), 3.64 (2H, triple peak, J = 6.4 Hz), 3.71 (3H, single peak).

References

[1] Patent: CN104672121, 2017, B. Location in patent: Paragraph 0038-0040
[2] Patent: WO2005/37197, 2005, A2. Location in patent: Page/Page column 104
[3] Patent: WO2005/37197, 2005, A2. Location in patent: Page/Page column 104
[4] Patent: US2016/168156, 2016, A1. Location in patent: Paragraph 0195; 0197; 0198
[5] European Journal of Medicinal Chemistry, 2018, vol. 158, p. 353 - 370

4-Chloro-N-Methoxy-N-MethylbutyraMide Preparation Products And Raw materials

Raw materials

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4-Chloro-N-Methoxy-N-MethylbutyraMide Suppliers

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View Lastest Price from 4-Chloro-N-Methoxy-N-MethylbutyraMide manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4-Chloro-N-Methoxy-N-Methylbutyramide 64214-66-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4-Chloro-N-Methoxy-N-Methylbutyramide 64214-66-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

Hebei Miaobian Biotechnology Co., Ltd

Product: 4-Chloro-N-Methoxy-N-MethylbutyraMide 64214-66-0
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99.99
Supply Ability: 10Ton
Release date: 2020-09-27

64214-66-0, 4-Chloro-N-Methoxy-N-MethylbutyraMideRelated Search:

4-Chloro-N-Methoxy-N-MethylbutyraMide

4-Chloro-N-methoxy-N-methylbutanamide

N-Methyl-N-methoxy-4-chlorobutanamide

Butanamide, 4-chloro-N-methoxy-N-methyl-

4- Chloro-N-methoxy-N-methyl butyl

2- Chloro - N - Methoxy - N - Methylbutyramide

N-methoxy-N-methyl-4-chloroprene amide

3-N-Methoxy-N-methyl-4-chlorobutyramide

64214-66-0