(3-Methoxy-5-methylphenyl)methanol
- Product Name
- (3-Methoxy-5-methylphenyl)methanol
- CAS No.
- 119650-44-1
- Chemical Name
- (3-Methoxy-5-methylphenyl)methanol
- Synonyms
- 3-Methoxy-5-methylbenzyl alcohol;3-methoxy-5-methylBenzenemethanol;Benzenemethanol, 3-methoxy-5-methyl-
- CBNumber
- CB43062919
- Molecular Formula
- C9H12O2
- Formula Weight
- 152.19
- MOL File
- 119650-44-1.mol
(3-Methoxy-5-methylphenyl)methanol Property
- storage temp.
- Sealed in dry,Room Temperature
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M333203
- Product name
- (3-Methoxy-5-methylphenyl)methanol
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 3394AA
- Product name
- (3-Methoxy-5-methylphenyl)methanol
- Packaging
- 250mg
- Price
- $170
- Updated
- 2021/12/16
- Product number
- 3394AA
- Product name
- (3-Methoxy-5-methylphenyl)methanol
- Packaging
- 1g
- Price
- $350
- Updated
- 2021/12/16
- Product number
- CHM0389252
- Product name
- (3-METHOXY-5-METHYLPHENYL)METHANOL
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.3
- Updated
- 2021/12/16
- Product number
- 3394AA
- Product name
- (3-Methoxy-5-methylphenyl)methanol
- Packaging
- 5g
- Price
- $950
- Updated
- 2021/12/16
(3-Methoxy-5-methylphenyl)methanol Chemical Properties,Usage,Production
Synthesis
106116-42-1
119650-44-1
General procedure for the synthesis of (3-methoxy-5-methylphenyl)methanol from 1-(bromomethyl)-3-methoxy-5-methylbenzene: To a solution of 1-(bromomethyl)-3-methoxy-5-methylbenzene (2.14 g) in acetone (80 mL) was added sodium bicarbonate (1.05 g) and water (50 mL), the mixture was heated and refluxed for 18 hours. Upon completion of the reaction, the reaction mixture was extracted with ethyl acetate, the organic layers were combined and washed with saturated sodium chloride solution. The organic layer was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography (eluent: ethyl acetate/hexane) to afford the target compound as a yellow oil (1.22 g).1H NMR (400 MHz, CDCl3) δ 2.35 (3H, s), 3.82 (3H, s), 4.64 (2H, s), 6.68 (1H, s), 6.75 (1H, s), 6.79 (1H, s).
References
[1] Journal of the American Chemical Society, 2012, vol. 134, # 30, p. 12402 - 12405
[2] Synthesis, 2007, # 1, p. 65 - 74
[3] Tetrahedron Letters, 2000, vol. 41, # 17, p. 3007 - 3010
[4] Journal of the American Chemical Society, 2011, vol. 133, # 39, p. 15686 - 15696
[5] RSC Advances, 2014, vol. 4, # 61, p. 32241 - 32248
(3-Methoxy-5-methylphenyl)methanol Preparation Products And Raw materials
Raw materials
Preparation Products
(3-Methoxy-5-methylphenyl)methanol Suppliers
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