methyl 3-(hydroxymethyl)-4-nitrobenzoate

Product Name: methyl 3-(hydroxymethyl)-4-nitrobenzoate
CAS No.: 201932-92-5
Chemical Name: methyl 3-(hydroxymethyl)-4-nitrobenzoate
Synonyms: methyl 3-(hydroxymethyl)-4-nitrobenzoate;Benzoic acid, 3-(hydroxymethyl)-4-nitro-, methyl ester
CBNumber: CB43147311
Molecular Formula: C9H9NO5
Formula Weight: 211.17
MOL File: 201932-92-5.mol

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methyl 3-(hydroxymethyl)-4-nitrobenzoate Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

AK Scientific

Product number: 8915CX
Product name: Methyl3-(hydroxymethyl)-4-nitrobenzoate
Packaging: 100mg
Price: $95
Updated: 2021/12/16

AK Scientific

Product number: 8915CX
Product name: Methyl3-(hydroxymethyl)-4-nitrobenzoate
Packaging: 1g
Price: $220
Updated: 2021/12/16

Ambeed

Product number: A147033
Product name: Methyl3-(hydroxymethyl)-4-nitrobenzoate
Purity: 97%
Packaging: 100mg
Price: $20
Updated: 2021/12/16

Ambeed

Product number: A147033
Product name: Methyl3-(hydroxymethyl)-4-nitrobenzoate
Purity: 97%
Packaging: 250mg
Price: $39
Updated: 2021/12/16

Ambeed

Product number: A147033
Product name: Methyl3-(hydroxymethyl)-4-nitrobenzoate
Purity: 97%
Packaging: 1g
Price: $119
Updated: 2021/12/16

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methyl 3-(hydroxymethyl)-4-nitrobenzoate Chemical Properties,Usage,Production

Synthesis

148625-35-8

201932-92-5

The general procedure for the synthesis of methyl 3-(hydroxymethyl)-4-nitrobenzoate from methyl 3-formyl-4-nitrobenzoate was as follows:(RS-3-49) Methyl 3-formyl-4-nitrobenzoate (1.20 g, 5.73 mmol) was dissolved in methanol (10 mL) and the solution was cooled to 0 °C. Sodium borohydride (69 mg, 1.72 mmol) was added all at once under stirring and the reaction mixture continued to be stirred at 0 °C for 20 min. Upon completion of the reaction, the reaction was quenched with 1N hydrochloric acid (10 mL) followed by evaporation under reduced pressure to remove methanol. The remaining aqueous phase was extracted with dichloromethane (3 x 10 mL) and the organic phases were combined, dried over anhydrous sodium sulfate and concentrated to afford the crude product methyl 3-(hydroxymethyl)-4-nitrobenzoate (1.06 g), which could be used in the subsequent reaction without further purification.

References

[1] Patent: WO2014/131023, 2014, A1. Location in patent: Page/Page column 138
[2] Journal of Medicinal Chemistry, 2016, vol. 59, # 10, p. 4812 - 4830

methyl 3-(hydroxymethyl)-4-nitrobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from methyl 3-(hydroxymethyl)-4-nitrobenzoate manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: methyl 3-(hydroxymethyl)-4-nitrobenzoate 201932-92-5
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-10

201932-92-5, methyl 3-(hydroxymethyl)-4-nitrobenzoateRelated Search:

methyl 3-(hydroxymethyl)-4-nitrobenzoate

Benzoic acid, 3-(hydroxymethyl)-4-nitro-, methyl ester

201932-92-5