3,4-Diethoxyaniline
- Product Name
- 3,4-Diethoxyaniline
- CAS No.
- 39052-12-5
- Chemical Name
- 3,4-Diethoxyaniline
- Synonyms
- AKOS BBS-00001416;3,4-DIETHOXYANILINE;3,4-DIETHOXYBENZENAMINE;3,4-diethoxy-phenylamine;Benzenamine, 3,4-diethoxy-;3,4-Diethoxyaniline ISO 9001:2015 REACH
- CBNumber
- CB4351229
- Molecular Formula
- C10H15NO2
- Formula Weight
- 181.23
- MOL File
- 39052-12-5.mol
3,4-Diethoxyaniline Property
- Melting point:
- 48°C
- Boiling point:
- 314.35°C (rough estimate)
- Density
- 1.0918 (rough estimate)
- refractive index
- 1.5200 (estimate)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 4.89±0.10(Predicted)
- color
- Light yellow to Brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D5478
- Product name
- 3,4-Diethoxyaniline
- Purity
- >98.0%(GC)(T)
- Packaging
- 1g
- Price
- $109
- Updated
- 2025/07/31
- Product number
- D5478
- Product name
- 3,4-Diethoxyaniline
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $327
- Updated
- 2025/07/31
- Product number
- D442015
- Product name
- 3,4-Diethoxyaniline
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FD151688
- Product name
- 3,4-Diethoxyaniline
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FD151688
- Product name
- 3,4-Diethoxyaniline
- Packaging
- 1g
- Price
- $101
- Updated
- 2021/12/16
3,4-Diethoxyaniline Chemical Properties,Usage,Production
Chemical Properties
Pink Solid
Uses
3,4-Diethoxyaniline can be used as an intermediate for the fungicide ethofluthrin.
Synthesis
4992-63-6
39052-12-5
The general procedure for the synthesis of 3,4-diethoxyaniline from 3,4-diethoxynitrobenzene was as follows: 3,4-diethoxynitrobenzene (6.30 g, 29.9 mmol), 10% palladium-carbon catalyst (600 mg), and anhydrous ethanol (300 mL) were added to a reaction flask, and the reaction was stirred for 6 hours under hydrogen atmosphere. Upon completion of the reaction, the insoluble palladium-carbon catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to afford 3,4-diethoxyaniline as an oily product in a yield of 5.02 g (92.9% yield). The product was characterized by 1H-NMR (CDCl3) with chemical shifts δ: 1.34 to 1.46 (6H, m), 3.94 to 4.08 (4H, m), 6.21 (1H, d, J = 2.8,8.4 Hz), 6.30 (1H, d, J = 2.6 Hz), 6.73 (1H, d, J = 8.4 Hz).
References
[1] Patent: EP1437344, 2004, A1. Location in patent: Page 37
[2] Yuki Gosei Kagaku Kyokaishi, 1959, vol. 17, p. 166,169
[3] Chem.Abstr., 1959, p. 11280
3,4-Diethoxyaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,4-Diethoxyaniline manufacturers
- Product
- 3,4-Diethoxyaniline 39052-12-5
- Price
- US $30.00/kg
- Min. Order
- 1kg
- Purity
- 0.99
- Supply Ability
- 100 tons
- Release date
- 2024-08-08
- Product
- 3,4-Diethoxyaniline 39052-12-5
- Price
- US $9.90/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-11-27
- Product
- 3,4-Diethoxyaniline 39052-12-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-08