3-METHYL-7-AZAINDOLE

Product Name: 3-METHYL-7-AZAINDOLE
CAS No.: 5654-93-3
Chemical Name: 3-METHYL-7-AZAINDOLE
Synonyms: 7-Azaskatole;3-METHYL-7-AZAINDOLE;3-METHYL-7-AZAINDOLE(LR);3-Methylpyrrolo[2,3-b]pyridine;3-methyl-1H-pyrrolo[2,3-b]pyridine;1H-Pyrrolo[2,3-b]pyridine, 3-methyl-;3-Methyl-1H-pyrrolo[2,3-b]pyridine 98%;Methanone,[5-(hydroxymethyl)phenyl]phenyl-
CBNumber: CB4382735
Molecular Formula: C8H8N2
Formula Weight: 132.16
MOL File: 5654-93-3.mol

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3-METHYL-7-AZAINDOLE Property

Melting point:: 130.5-133 °C
Boiling point:: 352.8±15.0 °C(Predicted)
Density: 1.17±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 8.01±0.20(Predicted)
Appearance: Off-white to yellow Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M288665
Product name: 3-Methyl-7-azaindole
Packaging: 1g
Price: $1100
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: CAPOM13839
Product name: 3-Methyl-1H-pyrrolo[2,3-b]pyridine
Packaging: 250mg
Price: $155
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-1-AJ
Product name: 3-Methyl-7-azaindole
Packaging: 250mg
Price: $175
Updated: 2021/12/16

AK Scientific

Product number: W7016
Product name: 3-Methyl-7-azaindole
Packaging: 100mg
Price: $92
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM1052147
Product name: 3-METHYL-1H-PYRROLO[2,3-B]PYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $452.98
Updated: 2021/12/16

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3-METHYL-7-AZAINDOLE Chemical Properties,Usage,Production

Uses

An azaindole derivative as CRTH2 receptor antagonist.

Synthesis

2402-77-9

107-11-9

5654-93-3

（Synthesis of (a) 3-methyl-1H-pyrrolo[2,3-b]pyridine: The intermediate was prepared by the method described by Jensen et al. (Angew. Chem. Int. Ed. 2008, 47, 888-890). Toluene (5 mL), 2,3-dichloropyridine (300 mg, 2.03 mmol), tris(dibenzylideneacetone)dipalladium (Pd2dba3, 2 mg, 0.0025 mmol), 1,1'-bis(diphenylphosphino)ferrocene (dppf, 6 mg, 0.01 mmol), sodium tert-butoxide (NaOtBu, 487 mg , 5.07 mmol) and allylamine (0.15 mL, 2.03 mmol). The reaction tube was sealed and heated at 140 °C for 20 h, followed by stirring for 24 h at room temperature. The reaction mixture was washed sequentially with water and brine, dried over anhydrous sodium sulfate (Na2SO4) and adsorbed on silica gel. Initial purification was carried out using a gradient elution of dichloromethane-hexane (0 to 60%) followed by ethyl acetate-hexane (80%) to give an orange solid product (100 mg, 37% yield).

References

[1] Angewandte Chemie - International Edition, 2008, vol. 47, # 5, p. 888 - 890
[2] Patent: WO2010/132615, 2010, A1. Location in patent: Page/Page column 111
[3] Patent: WO2013/114332, 2013, A1. Location in patent: Page/Page column 92; 93
[4] Patent: US2014/371204, 2014, A1. Location in patent: Paragraph 0718

3-METHYL-7-AZAINDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-METHYL-7-AZAINDOLE Suppliers

Canada 1 China 78 Germany 2 India 3 United Kingdom 1 United States 11 Global 96

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View Lastest Price from 3-METHYL-7-AZAINDOLE manufacturers

Career Henan Chemical Co

Product: 3-METHYL-7-AZAINDOLE 5654-93-3
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

5654-93-3, 3-METHYL-7-AZAINDOLERelated Search:

7-AZAINDOLE-3-CARBOXALDEHYDE METHYL 7-AZAINDOLE-3-GLYOXYLATE 1-(2,9-diazabicyclo[4.3.0]nona-2,4,7,10-tetraen-7-yl)-N,N-dimethyl-methanamine FMOC-DL-7-AZATRYPTOPHAN 1H-Pyrrolo[2,3-b]pyridine, 2,3-dimethyl- BOC-DL-7-AZATRYPTOPHAN 7-AZATRYPTOPHAN MONOHYDRATE L-745,870 TRIHYDROCHLORIDE 2-Propenamide, 2-cyano-3-(1H-pyrrolo[2,3-b]pyridin-3-yl)- 3-([4-(4-CHLOROPHENYL)PIPERAZIN-1-YL]METHYL)-1H-PYRROLO(2,3-B)PYRIDINE HYDROCHLORIDE Ethanone, 2,2,2-trifluoro-1-(1H-pyrrolo[2,3-b]pyridin-3-yl)- 1H-Pyrrolo[2,3-b]pyridine, 3-(phenylmethyl)- ETHYL A-ACETAMIDO-A-CARBETHOXY-B-(7-AZA-3-INDOLYL)PROPIONATE 1-(1-ETHYL-1H-PYRROLO[2,3-B]PYRIDIN-3-YL)-2,2,2-TRIFLUORO-1-ETHANONE 6,7,8,9-TETRAHYDRO-5H-PYRIDO[2,3-B]INDOLE ETHYL 2-(1-[(4-METHOXYPHENYL)SULFONYL]-1H-PYRROLO[2,3-B]PYRIDIN-3-YL)-2-OXOACETATE 2,2,2-TRIFLUORO-1-(1-[(4-METHOXYPHENYL)SULFONYL]-1H-PYRROLO[2,3-B]PYRIDIN-3-YL)-1-ETHANONE 2,2,2-TRIFLUORO-1-(1-[3-(TRIFLUOROMETHYL)BENZYL]-1H-PYRROLO[2,3-B]PYRIDIN-3-YL)-1-ETHANONE

3-METHYL-7-AZAINDOLE

3-Methylpyrrolo[2,3-b]pyridine

7-Azaskatole

3-methyl-1H-pyrrolo[2,3-b]pyridine

1H-Pyrrolo[2,3-b]pyridine, 3-methyl-

3-Methyl-1H-pyrrolo[2,3-b]pyridine 98%

3-METHYL-7-AZAINDOLE(LR)

Methanone,[5-(hydroxymethyl)phenyl]phenyl-

5654-93-3

Amines

Heterocycles

Indole Derivatives

Intermediates & Fine Chemicals

Pharmaceuticals

Azaindoles