7-BENZYLOXY-4-CHLOROQUINOLINE

Product Name: 7-BENZYLOXY-4-CHLOROQUINOLINE
CAS No.: 178984-56-0
Chemical Name: 7-BENZYLOXY-4-CHLOROQUINOLINE
Synonyms: 102579;4-chloro-7-(phenylMethoxy;4-chloro-7-benzoxyquinoline;4-chloro-7-phenoxy-quinoline;7-BENZYLOXY-4-CHLOROQUINOLINE;4-chloro-7-phenylmethoxyquinoline;Quinoline, 4-chloro-7-(phenylmethoxy)-;7-BENZYLOXY-4-CHLOROQUINOLINE ISO 9001：2015 REACH
CBNumber: CB4420424
Molecular Formula: C16H12ClNO
Formula Weight: 269.73
MOL File: 178984-56-0.mol

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7-BENZYLOXY-4-CHLOROQUINOLINE Property

Boiling point:: 414.1±30.0 °C(Predicted)
Density: 1.263±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 3.86±0.27(Predicted)
Appearance: White to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B700273
Product name: 7-(Benzyloxy)-4-chloroquinoline
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 072748
Product name: 7-(Benzyloxy)-4-chloroquinoline
Purity: 95+%
Packaging: 250mg
Price: $231
Updated: 2021/12/16

AK Scientific

Product number: W3897
Product name: 7-(Benzyloxy)-4-chloroquinoline
Packaging: 5g
Price: $419
Updated: 2021/12/16

Matrix Scientific

Product number: 072748
Product name: 7-(Benzyloxy)-4-chloroquinoline
Purity: 95+%
Packaging: 1g
Price: $500
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: PXT0001159
Product name: 7-(BENZYLOXY)-4-CHLOROQUINOLINE
Purity: 95.00%
Packaging: 250MG
Price: $631
Updated: 2021/12/16

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7-BENZYLOXY-4-CHLOROQUINOLINE Chemical Properties,Usage,Production

Synthesis

749922-34-7

178984-56-0

Step 3) Synthesis of 7-(benzyloxy)-4-chloroquinoline: 7-(benzyloxy)quinolin-4-ol (72 g, 287 mmol) was suspended in toluene (134 mL), and phosphorus trichloride (44 g, 287 mmol, source: Tianjin FuChen Chem. Co. Ltd.) was added. The suspension was heated to 120 °C and maintained for 1 hour. After completion of the reaction, the mixture was cooled to 70 °C and diluted with EtOAc (600 mL). The resulting mixture was stirred in an ice bath for 30 min and cooled to 15 °C. Subsequently, the mixture was neutralized with 3M NaOH aqueous solution to pH 7~8, keeping the solution temperature below 20°C during the process. The aqueous layer was separated and the organic layer was extracted with EtOAc. The combined organic layers were washed with brine (200 mL), dried over anhydrous Na2SO4, and concentrated in vacuum to give 7-benzyloxy-4-chloroquinoline as a light yellow solid (70.8 g, 91.6% yield). Mass spectrum (ESI, positive ion mode) m/z: 270.1 [M + 1]; 1H NMR (400 MHz, DMSO-d6) δ: 5.31 (s, 2H), 7.35 (t, 1H), 7.42 (t, J = 7.2Hz, 2H), 7.47 (dd, J = 2.8Hz, J = 9.2Hz, 1H), 7.52 (d, J = 7.6 Hz, 2H), 7.13 (t, J = 4.8 Hz, 2H), 8.11 (d, J = 9.6 Hz, 1H), 8.75 (d, J = 4.8 Hz, 1H).

References

[1] Patent: US2012/219522, 2012, A1. Location in patent: Page/Page column 20

7-BENZYLOXY-4-CHLOROQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-BENZYLOXY-4-CHLOROQUINOLINE Suppliers

China 69 Germany 2 India 1 United States 7 Global 79

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Jiaxing Novartis Chemical Co., Ltd.

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View Lastest Price from 7-BENZYLOXY-4-CHLOROQUINOLINE manufacturers

Career Henan Chemical Co

Product: 7-BENZYLOXY-4-CHLOROQUINOLINE 178984-56-0
Price: US $6.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-05-23

178984-56-0, 7-BENZYLOXY-4-CHLOROQUINOLINERelated Search:

λ-Cyhalothrin 4-Chloroquinoline 6-(benzyloxy)-4-chloroquinoline-3-carbonitrile 7-BENZYLOXYQUINOLINE 4-Chloro-7-hydroxyquinoline 4-Chloro-6-methoxy-7-(phenylmethoxy)-3-quinolinecarboxylic acid ethyl ester 4-Chloro-7-methoxyquinoline 7-BENZYLOXY-4-CHLOROQUINOLINE

7-BENZYLOXY-4-CHLOROQUINOLINE

4-chloro-7-benzoxyquinoline

4-chloro-7-(phenylMethoxy

4-chloro-7-phenoxy-quinoline

4-chloro-7-phenylmethoxyquinoline

102579

Quinoline, 4-chloro-7-(phenylmethoxy)-

7-BENZYLOXY-4-CHLOROQUINOLINE ISO 9001：2015 REACH

178984-56-0