5-IODO-6-METHYLPYRIMIDIN-4-OL

Product Name: 5-IODO-6-METHYLPYRIMIDIN-4-OL
CAS No.: 7752-74-1
Chemical Name: 5-IODO-6-METHYLPYRIMIDIN-4-OL
Synonyms: 5-IODO-6-METHYLPYRIMIDIN-4-OL;5-Iodo-6-MethylpyriMidin-4(1H)-one;4(3H)-Pyrimidinone, 5-iodo-6-methyl-;5-IODO-6-METHYLPYRIMIDIN-4-OL ISO 9001：2015 REACH
CBNumber: CB4460158
Molecular Formula: C5H5IN2O
Formula Weight: 236.01
MOL File: 7752-74-1.mol

More

Less

5-IODO-6-METHYLPYRIMIDIN-4-OL Property

Melting point:: 238-239 °C
Boiling point:: 245.5±43.0 °C(Predicted)
Density: 2.19±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 7.92±0.50(Predicted)
Appearance: Yellow to brown Solid

More

Less

Safety

HS Code: 2933599590

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

AK Scientific

Product number: Y5104
Product name: 5-Iodo-6-methylpyrimidin-4-ol
Packaging: 100mg
Price: $200
Updated: 2021/12/16

Ambeed

Product number: A417841
Product name: 5-Iodo-6-methylpyrimidin-4(1H)-one
Purity: 95+%
Packaging: 100mg
Price: $23
Updated: 2021/12/16

Ambeed

Product number: A417841
Product name: 5-Iodo-6-methylpyrimidin-4(1H)-one
Purity: 95+%
Packaging: 250mg
Price: $34
Updated: 2021/12/16

Ambeed

Product number: A417841
Product name: 5-Iodo-6-methylpyrimidin-4(1H)-one
Purity: 95+%
Packaging: 1g
Price: $74
Updated: 2021/12/16

Acrotein

Product number: UT02307
Product name: 5-Iodo-6-methyl-1H-pyrimidin-4-one
Purity: 97%
Packaging: 1g
Price: $111.47
Updated: 2021/12/16

More

Less

5-IODO-6-METHYLPYRIMIDIN-4-OL Chemical Properties,Usage,Production

Synthesis

3524-87-6

7752-74-1

General procedure for the synthesis of 5-iodo-6-methylpyrimidin-4(1H)-one using 6-methylpyrimidin-4(3H)-one as starting material: 127 g (0.56 mol) of N-iodosuccinimide (NIS) was added in batches to an acetic acid solution containing 70 g (0.64 mol) of 6-methylpyrimidin-4(3H)-one at room temperature, and the addition process lasted 15 minutes. The reaction mixture was stirred at room temperature until thin layer chromatography (TLC) monitoring showed complete consumption of the feedstock (about 30 hours). Upon completion of the reaction, the mixture was diluted with water and the precipitated solid product was collected by filtration. Subsequently, the solid was washed with aqueous sodium thiosulfate to remove residual iodine. Finally, the product was dried under vacuum to give 90 g of the target compound in 60% yield.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 6, p. 1601 - 1606
[2] Synthesis, 1984, # 3, p. 252 - 254
[3] Patent: WO2012/101184, 2012, A1. Location in patent: Page/Page column 50
[4] Patent: WO2012/101186, 2012, A1. Location in patent: Page/Page column 47
[5] Patent: EP2546249, 2013, A1. Location in patent: Paragraph 0177; 0178

5-IODO-6-METHYLPYRIMIDIN-4-OL Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

5-IODO-6-METHYLPYRIMIDIN-4-OL Suppliers

China 38 Germany 1 India 1 The Netherlands 1 United Kingdom 1 United States 1 Global 43

Chemfun Medical Technology(Shanghai) Co., Ltd.

Tel: 021-67220633 021-54824098
Fax: +86-21-54824069
Email: chemfun@chemfun.net
Country: China
ProdList: 491
Advantage: 58

ShangHai AmK Pharmaceutical Technology Co., Ltd.

Tel: 微信 17321281695 18019252918
Fax: 17321281695
Email: sale@amkchem.com
Country: China
ProdList: 15136
Advantage: 55

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 0512-0512-52358471 17715136450
Fax: 05125235 6881
Email: sales@shiyabiopharm.com
Country: China
ProdList: 12127
Advantage: 58

Hubei Chuangliankangcheng Pharmaceutical Co., Ltd.

Tel: 027-65388397 18164111589
Fax: 027-65388397
Email: 3321478047@qq.com
Country: China
ProdList: 2007
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Shanghai Rlavie Technology Co., Ltd.

Tel: 21-67759270 17717059219
Fax: QQ：1479352695
Email: sales@rlavie.com
Country: China
ProdList: 1620
Advantage: 55

Sichuan BaiPeng Biotechnology Co., Ltd.

Tel: 028-65791793 18140026355
Fax: QQ568470422
Email: 568470422@qq.com
Country: China
ProdList: 9997
Advantage: 58

Wuxi AppTec

Tel: 022-59987777 13552403979
Email: jia_guoqiang@wuxiapptec.com
Country: China
ProdList: 22345
Advantage: 58

SuZhou Medinoah Co.,LTD.

Tel: 0512-69561983 13914027025
Fax: 0512-69561982
Email: zhang_q@medinoah.com
Country: China
ProdList: 3811
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Shanghai Baoyisheng Biotechnology Co., LTD

Tel: 15221020695
Email: 502277408@qq.com
Country: China
ProdList: 459
Advantage: 58

Nantong Kaisheng Biotechnology Co., Ltd.

Tel: 13951303301
Email: 2084934672@qq.com
Country: China
ProdList: 634
Advantage: 58

Shanghai Rlavie Technology Co ltd

Tel: +86-021-67759270 +8617717059219
Fax: 021-67759270
Email: sales@rlavie.com
Country: China
ProdList: 1030
Advantage: 58

Dideu Industries Group Limited

Tel: +86-29-89586680 +86-15129568250
Email: 1026@dideu.com
Country: China
ProdList: 20284
Advantage: 58

KARMEL TECHNOLOGY (HK) CO.,LIMITED

Tel: +8618795957998
Email: karmelhk@126.com
Country: CHINA
ProdList: 2886
Advantage: 58

Shanxi Xuanran Import and Export Trade Co., Ltd.

Tel: +8617735180244
Email: mike_yan@xuanranglobal.com
Country: CHINA
ProdList: 4017
Advantage: 58

Hubei xin bonus chemical co. LTD

Tel: 86-13657291602
Fax: 027-59338440
Email: linda@hubeijusheng.com
Country: CHINA
ProdList: 22963
Advantage: 58

Chongqing Chemdad Co., Ltd

Tel: +86-023-6139-8061 +86-86-13650506873
Email: sales@chemdad.com
Country: China
ProdList: 39927
Advantage: 58

Shanghai Kaiwei Chemical Technology Co., Ltd.

Tel: 021-58461859 15821823057
Email: service@aiviche.com
Country: China
ProdList: 49312
Advantage: 58

career henan chemical co

Tel: +86-0371-86658258 +8613203830695
Fax: 0086-371-86658258
Email: factory@coreychem.com
Country: China
ProdList: 29798
Advantage: 58

Henan Weitesi Chemical Technology Co. LTD

Tel: 0371-0371-55135753 18003832934
Fax: QQ：2853979818
Email: 2853979818@qq.com
Country: China
ProdList: 9991
Advantage: 58

Shanghai UCHEM Inc.

Tel: 18939844854
Fax: QQ3004479448
Email: sales6@myuchem.com
Country: China
ProdList: 4996
Advantage: 58

TCI (Shanghai) Chemical Trading Co., Ltd.

Tel: 021-61109150
Fax: 021-61105897
Email: sales@tcisct.com
Country: China
ProdList: 29668
Advantage: 58

Nantong Hi-Future Biotechnology Co., Ltd

Tel: 18051384581
Email: sales@chemhifuture.com
Country: China
ProdList: 2998
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

Nanjing Puruida Pharmaceutical Technology Co., Ltd.

Tel: 15905142898
Email: sales@prdchem.com
Country: China
ProdList: 966
Advantage: 58

Shaanxi Didu New Material Co., Ltd

Tel: 029-81145920 17391631969
Email: 1046@dideu.com
Country: China
ProdList: 9996
Advantage: 58

Beijing Solarbio Science & Tecnology Co., Ltd.

Tel: 010-50973130 17801761073
Email: Gsiyu@solarbio.com
Country: China
ProdList: 50464
Advantage: 58

Suzhou Qihang Biotechnology Co., Ltd

Tel: 18151111370
Email: 1046215251@qq.com
Country: China
ProdList: 8718
Advantage: 58

Abosyn

Tel: 0512-69561983 13914027025
Email: he_qf@medinoah.com
Country: China
ProdList: 3001
Advantage: 58

Xinxiang Anqi Biotechnology Co., Ltd

Tel: 15036601220
Email: 877180706@qq.com
Country: China
ProdList: 50
Advantage: 58

Shanghai meikai technology co., ltd

Tel: 021-68689288 15300790979
Fax: wechat 18721550091
Email: info@mkbio.com.cn
Country: China
ProdList: 5000
Advantage: 58

Hebei Yaocheng Pharmaceutical Technology Co. Ltd

Tel: 18033875090
Email: yc-eliu@yaochengph.com
Country: China
ProdList: 5489
Advantage: 58

DAYANG CHEM (HANGZHOU) CO.,LTD

Tel: +86-88938639 +86-17705817739
Email: info@dycnchem.com
Country: China
ProdList: 53899
Advantage: 58

Shanxi Tihondan Pharmaceutical Technology Co., Ltd

Tel: +8618235132063
Email: sales@tihondan.com
Country: China
ProdList: 3767
Advantage: 58

Nantong HI-FUTURE Biology Co., Ltd.

Tel: +undefined18051384581
Email: sales@chemhifuture.com
Country: China
ProdList: 3135
Advantage: 58

More

Less

View Lastest Price from 5-IODO-6-METHYLPYRIMIDIN-4-OL manufacturers

Dideu Industries Group Limited

Product: 5-IODO-6-METHYLPYRIMIDIN-4-OL 7752-74-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-08

Career Henan Chemical Co

Product: 5-IODO-6-METHYLPYRIMIDIN-4-OL 7752-74-1
Price: US $6.68/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2020-01-10

7752-74-1, 5-IODO-6-METHYLPYRIMIDIN-4-OLRelated Search:

5-IODO-6-METHYLPYRIMIDIN-4-OL 4-[(5-IODO-2,6-DIMETHYL-4-PYRIMIDINYL)OXY]BENZENECARBONITRILE 5-IODO-2-ISOPROPYL-6-METHYL-PYRIMIDIN-4-OL 2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE 5-IODOOROTIC ACID 1-(4-CHLOROPHENYL)-2-[(5-IODO-2,6-DIMETHYL-4-PYRIMIDINYL)OXY]-1-ETHANONE 2-AMINO-4-HYDROXY-5-IODO-6-PHENYLPYRIMIDINE

5-IODO-6-METHYLPYRIMIDIN-4-OL

5-Iodo-6-MethylpyriMidin-4(1H)-one

4(3H)-Pyrimidinone, 5-iodo-6-methyl-

5-IODO-6-METHYLPYRIMIDIN-4-OL ISO 9001：2015 REACH

7752-74-1