ChemicalBook > CAS DataBase List > N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE

N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE

Product Name
N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE
CAS No.
5317-89-5
Chemical Name
N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE
Synonyms
AURORA 2940;N-(4-Acetylphenyl);4'-ACETYLMETHANESULFONANILIDE;4'-Acetylmethanesulfonanilide;N-(4-ethanoylphenyl)methanesulfonamide;Methanesulfonamide, N-(4-acetylphenyl)-;N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE
CBNumber
CB4461135
Molecular Formula
C9H11NO3S
Formula Weight
213.25
MOL File
5317-89-5.mol
More
Less

N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE Property

Melting point:
150-152 °C
Boiling point:
369.4±44.0 °C(Predicted)
Density 
1.320±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
7.16±0.10(Predicted)
Appearance
White to light yellow Solid
More
Less

Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

TRC
Product number
N497065
Product name
N-(4-Acetylphenyl)methanesulfonamide
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
N497065
Product name
N-(4-Acetylphenyl)methanesulfonamide
Packaging
500mg
Price
$110
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA114576
Product name
N-(4-Acetylphenyl)methanesulfonamide
Packaging
250mg
Price
$57.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA114576
Product name
N-(4-Acetylphenyl)methanesulfonamide
Packaging
500mg
Price
$100
Updated
2021/12/16
Matrix Scientific
Product number
030126
Product name
N-(4-Acetylphenyl)methanesulfonamide
Packaging
500mg
Price
$86
Updated
2021/12/16
More
Less

N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE Chemical Properties,Usage,Production

Synthesis

99-92-3

124-63-0

5317-89-5

Cooled 4-aminoacetophenone (10 mmol) was dissolved in pyridine (10 mL) at 0 °C and methanesulfonyl chloride (15 mmol) was added slowly. The reaction mixture was stirred at room temperature for 2 hours. After completion of the reaction, the reaction mixture was diluted with H2O and extracted with ethyl acetate (EtOAc) several times. The organic layers were combined, washed sequentially with H2O and saturated brine and dried over anhydrous magnesium sulfate (MgSO4). After filtration, the filtrate was concentrated under reduced pressure. The residue was purified by rapid column chromatography on silica gel, the eluent being a mixed solvent of ethyl acetate:hexane to afford N-(4-acetylphenyl)methanesulfonamide (Compound 13-5, LJO-298). The yield was 95% and the melting point was 161 °C. 1H NMR (CDCl3) δ: 7.97 (dd, 2H, J = 2.0, 6.8 Hz), 7.26 (dd, 2H, J = 2.0, 6.8 Hz), 6.87 (bs, 1H), 3.10 (s, 3H), 2.59 (s, 3H).

References

[1] Journal of Enzyme Inhibition and Medicinal Chemistry, 2014, vol. 29, # 6, p. 846 - 867
[2] Organic Process Research and Development, 1998, vol. 2, # 2, p. 71 - 77
[3] Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 18, p. 6043 - 6053
[4] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 12, p. 2685 - 2688
[5] Patent: WO2005/3084, 2005, A1. Location in patent: Page 79

N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE Suppliers

Austria 1 Belgium 1 China 51 France 2 Germany 1 India 2 Ukraine 2 United Kingdom 2 United States 9 Global 71
Nanjing Chalf-Pharm Technology Co., Ltd.
Tel
025-57018978 18251899859
Fax
025-57018008
Email
sales@chalf-pharm.com
Country
China
ProdList
5674
Advantage
50
Cool Pharm, Ltd
Tel
021-60455363 18019463053
Fax
50966098
Email
sales@coolpharm.com
Country
China
ProdList
12346
Advantage
58
Chizhou Kailong Import and Export Trade Co., Ltd.
Tel
Fax
-
Email
xg01_gj@163.com
Country
China
ProdList
9484
Advantage
50
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
Shanghai Chaolan Chemical Technology Center
Tel
021-QQ：65489617 15618227136
Fax
21-5161 9052
Email
Sales@ATKchemical.com
Country
China
ProdList
9125
Advantage
58
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Yantai ShengKailun Chemical Technology Co., Ltd.
Tel
13356901049
Fax
QQ：1025383091
Email
3119594100@qq.com
Country
China
ProdList
7964
Advantage
55
Amatek Scientific Co. Ltd.
Tel
0512-56316828
Fax
0512-56316826
Email
info@amateksci.com
Country
China
ProdList
28785
Advantage
58
Aikon International Limited
Tel
025-58851090 15955137747
Fax
(6)02557626880
Email
sales01@aikonchem.com
Country
China
ProdList
15949
Advantage
58
Zhengzhou Ruke Biological Co., Ltd.
Tel
15981811963
Fax
QQ：1410472904
Email
1410472904@qq.com
Country
China
ProdList
5825
Advantage
58
Shanghai Jizhi Biochemical Technology Co. Ltd.
Tel
4009004166/18616739031 18616739031
Email
3007523370@qq.com
Country
China
ProdList
52687
Advantage
58
CD Chemical Group Limited
Tel
+8615986615575
Fax
0086-13651442114
Email
info@codchem.com
Country
China
ProdList
20342
Advantage
58
Shanghai Lanle Bird Industrial Co., Ltd.
Tel
15021845385
Email
765325601@qq.com
Country
China
ProdList
3609
Advantage
58
Henan Weitesi Chemical Technology Co. LTD
Tel
0371-0371-55135753 18003832934
Fax
QQ：2853979818
Email
2853979818@qq.com
Country
China
ProdList
9991
Advantage
58
Energy Chemical
Tel
021-58432009 400-005-6266
Fax
021-58436166
Email
marketing@energy-chemical.com
Country
China
ProdList
44918
Advantage
58
Hubei Co-prosperity Medicine Technonlogy Co., Ltd
Tel
2383948258 19172820304
Email
2383948258@qq.com
Country
China
ProdList
12987
Advantage
58
Beijing Jin Ming Biotechnology Co., Ltd.
Tel
010-60605840 15801484223;
Email
psaitong@jm-bio.com
Country
China
ProdList
29757
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
40000
Advantage
58
Hefei Mokai Pharmaceutical Technology Co., Ltd
Tel
18130062233
Email
3362556465@qq.com
Country
China
ProdList
8100
Advantage
58
Bide Pharmatech Ltd.
Tel
400-1647117 13681763483
Email
product02@bidepharm.com
Country
China
ProdList
59936
Advantage
58
Bide Pharmatech Ltd.
Tel
400-6005915
Email
sales@picasso-e.com
Country
China
ProdList
39653
Advantage
58
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
18621169109
Email
market03@meryer.com
Country
China
ProdList
27987
Advantage
58
Beijing FYF Chemicals Co., Ltd
Tel
010-57903446 15869909019
Email
168931144@qq.com
Country
China
ProdList
4965
Advantage
58
Beijing Solarbio Science & Tecnology Co., Ltd.
Tel
010-50973130 17801761073
Email
Gsiyu@solarbio.com
Country
China
ProdList
50464
Advantage
58
Liaocheng Lebote Biopharmaceutical Technology Co., Ltd
Tel
0635-893290 18663513896;
Email
28698871@qq.com
Country
China
ProdList
8022
Advantage
58
Yantai Shengkailun Chemical Technology Co., Ltd.
Tel
13356901049
Email
mark@sklnchem.cn
Country
China
ProdList
9993
Advantage
58
Pushan Industry (Shaanxi) Co., Ltd
Tel
029-81310890 18165209495
Email
2929288192@qq.com
Country
China
ProdList
9729
Advantage
58
Shandong Libixi Biopharmaceutical Technology Co., Ltd.
Tel
15318973357; 15318973357
Email
1460285141@qq.com
Country
China
ProdList
8064
Advantage
58
Tianjin Rongshen Chemical Co., Ltd
Tel
18317763565; 18317763565
Email
18317763565@163.com
Country
China
ProdList
9516
Advantage
58
Merck KGaA
Tel
21-20338288
Email
ordercn@merckgroup.com
Country
China
ProdList
6394
Advantage
58
Shanghai Macklin Biochemical Co.,Ltd.
Tel
021-50706066 15221275939
Email
shenlinxing@macklin.cn
Country
China
ProdList
14580
Advantage
58
Santa Cruz Biotechnology Inc
Tel
021-60936350
Email
scbt@scbt.com
Country
China
ProdList
6594
Advantage
58
ATK CHEMICAL COMPANY LIMITED
Tel
+undefined-21-51877795
Fax
+86 21 5161 9052/ 5187 7796
Email
ivan@atkchemical.com
Country
China
ProdList
33024
Advantage
60
SHANGHAI KEAN TECHNOLOGY CO., LTD.
Tel
+8613817748580
Fax
021-50175322
Email
cooperation@kean-chem.com
Country
China
ProdList
40066
Advantage
58
SUZHOU SENFEIDA CHEMICAL CO.,LTD
Tel
+86-0512-83500002 +8618662433356
Email
3899766280@qq.com
Country
China
ProdList
26362
Advantage
58
Shanghai Acmec Biochemical Technology Co., Ltd.
Tel
+86-18621343501; +undefined18621343501
Email
product@acmec-e.com
Country
China
ProdList
33337
Advantage
58
Hangzhou MolCore BioPharmatech Co.,Ltd.
Tel
+86-057181025280; +8617767106207
Fax
0571-85806285
Email
sales@molcore.com
Country
China
ProdList
49734
Advantage
58
Guangzhou Sanxu Biotechnology Co., Ltd.
Tel
15989179426
Country
CHINA
ProdList
156
Advantage
58
Guangzhou Zhenhao Biotechnology Co., Ltd.
Tel
13430395027
Country
CHINA
ProdList
115
Advantage
58
Absin Bioscience Inc.
Tel
--
Fax
--
Email
chenjw@absin.cn
Country
CHINA
ProdList
6208
Advantage
58
Shanghai Hao Zhun Biological Technology Co., Ltd.
Tel
--
Fax
--
Email
info@zzsrm.com
Country
CHINA
ProdList
6650
Advantage
58
Shanghai Qincheng Biological Technology Co., Ltd.
Tel
--
Fax
--
Email
shqcsw01@163.com
Country
CHINA
ProdList
6821
Advantage
58
Shanghai Shize Biological Technology Co., Ltd.
Tel
--
Fax
--
Email
shizezjp@163.com
Country
CHINA
ProdList
6174
Advantage
58
Rhenbo (Shanghai) Biochemical Technology Co., Ltd.
Tel
--
Fax
--
Country
CHINA
ProdList
6333
Advantage
58
Beijing Luyuan Bird Biotechnology Co., Ltd.
Tel
--
Fax
--
Email
15810802415@139.com
Country
CHINA
ProdList
6750
Advantage
58
Shanghai Machine Pure Industrial Co., Ltd.
Tel
--
Fax
--
Email
3245176082@qq.com
Country
CHINA
ProdList
6800
Advantage
58
Shanghai Wowu Biological Technology Co., Ltd.
Tel
--
Fax
--
Email
shhebio@126.com
Country
CHINA
ProdList
6137
Advantage
58
Shanghai yiji industries Co., Ltd.
Tel
--
Fax
--
Email
yiji01@foxmail.com
Country
China
ProdList
6021
Advantage
50
Shanghai Caiyou Industrial Co., Ltd.
Tel
--
Fax
--
Email
15821073967@163.com
Country
CHINA
ProdList
6748
Advantage
58
Shanghai Jingke Chemical Technology Co., Ltd.
Tel
--
Fax
--
Email
jingkehuaxue@163.com
Country
CHINA
ProdList
6141
Advantage
58

5317-89-5, N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDERelated Search:

Iguratimod 4-[(4-Mesylamino)phenyl]-4-oxobutyric acid Flosulide N-[4-(2-CHLOROACETYL)PHENYL]METHANESULFONAMIDE N-(4-ACETYL-PHENYL)-4-METHYL-BENZENESULFONAMIDE N-[4-[[1-[2-(6-METHYL-2-PYRIDINYL)ETHYL]-4-PIPERIDINYL]CARBONYL]PHENYL]METHANESULFONAMIDE DIHYDROCHLORIDE FK-3311 2-CHLORO-1-[1-(METHYLSULFONYL)-2,3-DIHYDRO-1H-INDOL-5-YL]ETHANONE N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE E-4031 N-(4-ACETYL-PHENYL)-4-CHLORO-BENZENESULFONAMIDE 4-AMINO-N-(4-BENZOYL-PHENYL)-BENZENESULFONAMIDE N-(4-acetylphenyl)butane-1-sulfonamide N-(4-acetylphenyl)thiophene-2-sulfonamide AKOS BBS-00004803 N-(4-acetylphenyl)ethanesulfonamide N-(4-ACETYL-PHENYL)-4-AMINO-BENZENESULFONAMIDE N-[4-(2-CHLOROPROPANOYL)PHENYL]METHANESULFONAMIDE

  • AURORA 2940
  • N-(4-ACETYL-PHENYL)-METHANESULFON-AMIDE
  • N-(4-ethanoylphenyl)methanesulfonamide
  • N-(4-Acetylphenyl)
  • Methanesulfonamide, N-(4-acetylphenyl)-
  • 4'-Acetylmethanesulfonanilide
  • 4'-ACETYLMETHANESULFONANILIDE
  • 5317-89-5