N-(2-nitrophenyl)-2-fluoroaniline

Product Name: N-(2-nitrophenyl)-2-fluoroaniline
CAS No.: 28898-02-4
Chemical Name: N-(2-nitrophenyl)-2-fluoroaniline
Synonyms: 2-Fluoro-2'-nitrodiphenylamine;N-(2-nitrophenyl)-2-fluoroaniline;N-(2-fluorophenyl)-2-nitroaniline;2-Fluoro-N-(2-nitrophenyl)aniline;2-[(2-Fluorophenyl)amino]nitrobenzene;Benzenamine, 2-fluoro-N-(2-nitrophenyl)-;2-[(2-Fluorophenyl)amino]nitrobenzene 98%;2-FLUORO-2'-NITRODIPHENYLAMINE ISO 9001：2015 REACH;2-Fluoro-N-(2-nitrophenyl)aniline, 2-Fluoro-2'-nitrodiphenylamine
CBNumber: CB4501121
Molecular Formula: C12H9FN2O2
Formula Weight: 232.21
MOL File: 28898-02-4.mol

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Safety

HS Code: 2922290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F621943
Product name: 2-Fluoro-2''-nitrodiphenylamine
Packaging: 500mg
Price: $75
Updated: 2021/12/16

TRC

Product number: F621943
Product name: 2-Fluoro-2''-nitrodiphenylamine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4655-3-22
Product name: 2-Fluoro-2'-nitrodiphenylamine
Purity: 98%
Packaging: 5G
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: PC3545
Product name: 2-[(2-Fluorophenyl)amino]nitrobenzene
Purity: 98%
Packaging: 5g
Price: $87
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4655-3-22
Product name: 2-Fluoro-2'-nitrodiphenylamine
Purity: 98%
Packaging: 25g
Price: $195
Updated: 2021/12/16

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N-(2-nitrophenyl)-2-fluoroaniline Chemical Properties,Usage,Production

Synthesis

348-54-9

1493-27-2

28898-02-4

GENERAL METHOD: Suspend NaH (75 mmol) in DMF (60 mL) at 0°C and slowly add o-fluoroaniline (50 mmol). After maintaining 0°C and stirring for 30 min, a solution of 1-fluoro-2-nitrobenzene (60 mmol) in DMF (30 mL) was added dropwise. The reaction mixture was gradually warmed to room temperature and stirred continuously for 16 hours. Upon completion of the reaction, the mixture was carefully poured into stirred saturated NH4Cl solution (500 mL) to quench the reaction. The precipitate was collected by filtration, the filter cake was washed with water and finally purified by recrystallization from methanol to afford the target product 2-fluoro-N-(2-nitrophenyl)aniline (15j). The product was a red solid with a yield of 74.1% and a melting point of 74.4-75.8 °C. 1H NMR (400 MHz, DMSO-d6) δ 9.28 (s, 1H), 8.14 (d, J = 8.0 Hz, 1H), 7.51 (m, 2H), 7.35 (m, 3H), 6.90 (m, 2H); MS (ESI) m/z (%). 231.1 [M-H]-.

References

[1] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 16, p. 4475 - 4486
[2] Molecules, 2015, vol. 20, # 1, p. 1712 - 1730
[3] Archiv der Pharmazie, 1997, vol. 330, # 11, p. 353 - 357
[4] Patent: WO2008/73459, 2008, A1. Location in patent: Page/Page column 95
[5] Journal of Medicinal Chemistry, 2010, vol. 53, # 11, p. 4511 - 4521

N-(2-nitrophenyl)-2-fluoroaniline Preparation Products And Raw materials

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Preparation Products

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View Lastest Price from N-(2-nitrophenyl)-2-fluoroaniline manufacturers

Career Henan Chemical Co

Product: 2-FLUORO-2'-NITRODIPHENYLAMINE 28898-02-4
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-03

28898-02-4, N-(2-nitrophenyl)-2-fluoroanilineRelated Search:

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N-(2-nitrophenyl)-2-fluoroaniline

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28898-02-4

C12H9FN2O2

Fluorine series